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    SKL1043 Lab 2

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    Lingesswari Nagarajan
    This laboratory report details an experiment using NMR spectroscopy to elucidate the structures of alcohols. The objective was to prepare samples for 1H NMR and 13C NMR analysis and interpret the NMR spectra of alcohols. Butanol and cyclohexanol were analyzed using deuterated chloroform as the solvent. NMR is a non-destructive technique that provides a direct relationship between measured spectra and chemical structure, making it useful for molecular structure characterization and quantitative analysis of complex mixtures.

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    SKL1043 Lab 2

    Uploaded by

    Lingesswari Nagarajan
    127 views4 pages
    This laboratory report details an experiment using NMR spectroscopy to elucidate the structures of alcohols. The objective was to prepare samples for 1H NMR and 13C NMR analysis and interpret the NMR spectra of alcohols. Butanol and cyclohexanol were analyzed using deuterated chloroform as the solvent. NMR is a non-destructive technique that provides a direct relationship between measured spectra and chemical structure, making it useful for molecular structure characterization and quantitative analysis of complex mixtures.

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    This laboratory report details an experiment using NMR spectroscopy to elucidate the structures of alcohols. The objective was to prepare samples for 1H NMR and 13C NMR analysis and interpret the NMR spectra of alcohols. Butanol and cyclohexanol were analyzed using deuterated chloroform as the solvent. NMR is a non-destructive technique that provides a direct relationship between measured spectra and chemical structure, making it useful for molecular structure characterization and quantitative analysis of complex mixtures.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    127 views4 pages

    SKL1043 Lab 2

    Uploaded by

    Lingesswari Nagarajan
    This laboratory report details an experiment using NMR spectroscopy to elucidate the structures of alcohols. The objective was to prepare samples for 1H NMR and 13C NMR analysis and interpret the NMR spectra of alcohols. Butanol and cyclohexanol were analyzed using deuterated chloroform as the solvent. NMR is a non-destructive technique that provides a direct relationship between measured spectra and chemical structure, making it useful for molecular structure characterization and quantitative analysis of complex mixtures.

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    © All Rights Reserved
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    of 4

    LABORATORY REPORT

    SKL1043
    SEM 4 2019/2020

    EXPERIMENT 2

    STRUCTURAL ELUCIDATION OF ALCOHOLS


    TITLE
    USING NMR SPECTROMETER

    STUDENT’S 1)LINGESSWARI A/P NAGARAJAN


    NAME 2)DIVYARSI A/P THELLAIVASSAN

    1) E20182022985
    MATRIC NO.
    2) E20182022971

    LECTURE
    A
    GROUP

    LECTURER
    DR. MOHAMAD IDRIS BIN SAIDIN
    NAME

    CHECKLIST Marks
    Title 4
    Introduction 10
    Objective (s) 5
    Methods 10
    Result (Worksheet) 15
    Discussion 30
    Conclusion 10
    Question (s) 10
    References 6
    TOTAL MARKS 100
    Objective

    By end of the experiment, we will be able to prepare samples for 1HNMR and
    13
    CNMR analyses and will be able to interpret the NMR spectrum of alcohols.

    Introduction

    NMR spectroscopic methods for structural elucidation in organic chemistry are


    reviewed. Detailed procedures and recommended experimental parameters are
    provided for commonly encountered scenarios.It is a non-destructive and
    non-invasive techniques that provide direct relationship between the measured spectra
    and chemical structure.This is the primary standard and routine method for molecular
    structure characterization.The capability of NMR for quantitation (qNMR) is to
    simultaneously detect a large number of compounds is a complex mixture without
    separation. It is suitable to be used in the analysis of natural products including
    food,fruit juices and alcoholic beverages.The principle of nuclear magnetic resonance
    is based on the spins of atomic nuclei.The magnetic measurements depend upon the
    spin of unpaired electron whereas nuclear magnetic resonance measures magnetic
    effect caused by the spin of protons and neutrons.Both nucleons have intrinsic angular
    spins which act as elementary magnet.The existence of nuclear magnetism is revealed
    in the hyper fine structure of spectral lines.If the nucleus with a certain magnetic
    moment is placed in the magnetic field,we can observe the phenomenon of space
    quantization where the direction will be slightly different energy level.

    The Table below shows principle components of NMR


    Material & Apparatus

    Chemicals:

    1. Butano

    2. Cyclohexanol

    3. Deuterated chloroform, CDCl 3


    Apparatus

    1. NMR tube

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