Filtra'on - Lecture 1: CH 2040 - Mechanical Opera'ons Basavaraj M. Gurappa Department of Chemical Engineering IIT Madras
Filtra'on - Lecture 1: CH 2040 - Mechanical Opera'ons Basavaraj M. Gurappa Department of Chemical Engineering IIT Madras
Filtra'on - Lecture 1: CH 2040 - Mechanical Opera'ons Basavaraj M. Gurappa Department of Chemical Engineering IIT Madras
Filtra'on
Filtra'onisaprocessofremovalofsolidpar'clesfromauid bypassingtheuidthroughalteringmedium,orseptum,on whichthesolidsaredeposited. Industrial ltra'on range from simple straining to highly complexsepara'ons
Valuableproduct ofltra'on
Neither
Classica'onoflters
Inanylter,uidsowthroughaltermediumbyvirtueofa pressuredieren'alacrossthemedium.
UpstreamPressure>atm Upstream
FilterMedium
FilterMedium
Downstream
DownstreamPressure=atm
UpstreamPressure=atm
Pressure above atmosphere is developed by several means by a pump or blower, centrifugalforceorbygravityforceac'ngona columnofliquid
FilterMedium
DownstreamVacuum
Mechanismsofltra'on
Cakelters
Clarifying
Crossowlters
Mechanismsofltra'on
Cake lters separate rela'vely large amounts ofsolidsascakeofcrystalsorsludge.OVenthey have provisions for washing cake or removing some of the liquid from the solids before discharge. Clarifyinglterstheseltersremovesmallamounts of solids to produce a clean gas or sparkling clear liquids. Most solids are trapped inside lter medium. Suchltersdierfromscreensinthattheporesofthe lter medium are much larger than size of the par'clestoberemoved Cross ow lters feed suspension ows under pressure at a fairly high velocity across the lter medium.Highliquidvelocitykeepsthelayerofsolids from building up. Filter medium used generally is ceramic,polymerormetalwithporessmallenoughto excludemostofthesuspendedpar'cles.Someofthe liquidpassesthroughtheltermedium,leavingmore concentratedsuspensionbehind
FilterMedia
Theltermediumormembraneinanyltermustmeetthefollowing requirements 1. It must retain the solids to be ltered, giving a reasonably clear ltrate. 2. Itmustnotplugorblind 3. It must be resistant chemically and strong enough physically to withstandprocesscondi'ons 4. Itmustpermitthecakeformedtodischargecleanlyandcompletely 5. Itmustnotbeprohibi'velyexpensive
FilterAids
Slimyorverynesolidsthatformadenseimpermeablecakequicklypluganyltermediumthat is ne enough to retain them. In prac'ce, to lter such materials, porosity of the cake is increasedtopermitthepassageoftheliquidatareasonablerate.Thisisdonebyaddinglter aidssuchaspuriedwoodcellulose,inertporoussolids,diatomaceoussilicatotheslurrybefore ltra'on. Another way of using a lter aid is by precoaCng, that is, deposi'ng a layer of it on the lter mediumbeforeltra'on.
Principlesofcakeltra'on
Filtra'onisaspecialcaseofowthroughpackedbeds. Inconven'onalpackedbeds,resistancetoowareconstant. Inltra'ontheowresistancesincreasewith'meastheltermedium becomescloggedoraltercakebuildsup.Thereforeequa'onsrela'ng ow rates and pressure drops in packed beds have to be modied to allowforthischange.
ErgunEqua'on
P 150V0 (1 ) 1.75 V (1 ) = 2 2 + 3 L s Dp s Dp 3
2 2 0
KozenyCarman
BurkePlummer
Principlesofcakeltra'on
Filtra'onisaspecialcaseofowthroughpackedbeds. Inconven'onalpackedbeds,resistancetoowareconstant. Inltra'ontheowresistancesincreasewith'meastheltermedium becomescloggedoraltercakebuildsup.Thereforeequa'onsrela'ng ow rates and pressure drops in packed beds have to be modied to allowforthischange.
ErgunEqua'on
LaminarFlow
2
TurbulentFlow
2 0
P 150V0 (1 ) 1.75 V (1 ) = 2 2 + 3 L s Dp s Dp 3
KozenyCarman BurkePlummer
P 32V0 = L D2
Solids/Par'cles
Channelsforliquidow
Deq
Totalsurfaceareaofnparallelchannels
n Deq L
S0 L (1 )
S0 L (1 ) vp
n Deq L
S0 L (1 )
S0 L (1 ) vp
Totalsurfaceareaavailablefornchannels
S0 L (1 ) sp vp
n Deq L
S0 L (1 ) sp n vp
6 = vp s Dp
6 n Deq L = S0 L (1 ) s Dp
sp
VoidVolumeinthebed=Totalvolumeofnchannels
D2 eq S0 L = n L 4
Using(1)and(2)
(2)
2 Deq = s D p 3 (1 )
V0 V=
V0
istheemptytowerorsupercialvelocity
P 32V0 (1 )2 = 1 3 4 2 2 L s Dp 9
P 72 1V0 (1 )2 = 2 3 L 2 D s p P 150V0 (1 ) = 2 2 L s Dp 3
2
1 = 2.1