Test of Dynamic Mechanical Properties of Ambient Cured Geopolymer Concrete Using Split Hopkinson Pressure Bar by Zhijie Huang (2022)
Test of Dynamic Mechanical Properties of Ambient Cured Geopolymer Concrete Using Split Hopkinson Pressure Bar by Zhijie Huang (2022)
Test of Dynamic Mechanical Properties of Ambient Cured Geopolymer Concrete Using Split Hopkinson Pressure Bar by Zhijie Huang (2022)
Abstract: The application of geopolymer concrete (GPC) in construction could reduce a large amount of carbon dioxide (CO2 ) emission,
which is greatly beneficial to environmental sustainability. Structures made of GPC might be subjected to extreme loading such as impact
and blast loads. Therefore, a good understanding of the dynamic properties of GPC is essential to provide reliable predictions of performance
of GPC structures subjected to dynamic loading. This study presents an experimental investigation on the dynamic compressive and splitting
tensile properties of ambient-cured GPC using split Hopkinson pressure bar (SHPB), with the strain rate up to 161.0 s−1 for dynamic com-
pression and 10.3 s−1 for dynamic splitting tension. The failure mode and damage progress of GPC specimens, energy absorption, and
dynamic increase factor (DIF) were studied. Test results showed that ambient-cured GPC exhibited strain rate sensitivity. The compressive
and splitting tensile DIFs increased with the strain rate and the ambient-cured GPC with lower quasi-static compressive strength exhibited
higher DIFs under both dynamic compression and splitting tension. Empirical formulas were proposed to predict the DIF of ambient-cured
GPC. Furthermore, the specific energy absorption of ambient-cured GPC under dynamic compression increased approximately linearly with
the strain rate. DOI: 10.1061/(ASCE)MT.1943-5533.0004074. © 2021 American Society of Civil Engineers.
Author keywords: Geopolymer concrete; Split Hopkinson pressure bar (SHPB); Compression; Splitting tension; Energy absorption;
Dynamic increase factor (DIF).
Introduction these industrial by-products can also save a lot of land areas for
disposal and lead to great benefits to the environment. In the last
Climate change due to greenhouse gas emission has attracted in- years, many studies have investigated the mechanical properties of
creasing attention in recent decades. The production of ordinary GPC (Diaz-Loya et al. 2011; Ganesan et al. 2014; Noushini et al.
portland cement concrete (OPC), one of the most widely used con- 2016; Thomas and Peethamparan 2015; Xie et al. 2019). It is re-
struction materials around the world, contributes to a large amount ported that GPC could behave similarly as OPC, or even better with
of greenhouse gas emission such as carbon dioxide (CO2 ). The respect to chemical resistance, fire resistance, chloride penetration,
demand of OPC is still rising due to the booming of construction and freeze-thaw cycles (Li et al. 2019; Singh et al. 2015).
industry. Therefore, an alternative material with less CO2 emission Concrete structures may be subjected to impact and blast loads
to replace OPC is deemed necessary. Geopolymer concrete (GPC), during their service life. The failure modes and damage level of
a potential alternative to OPC, uses industrial by-products such as concrete structures are greatly affected by dynamic mechanical
fly ash and slag to replace cement as binder materials. The reuse of properties of concrete materials. Previous studies demonstrated that
1
the dynamic mechanical properties of OPC is strain rate dependent
Visiting Research Associate, Center for Infrastructural Monitoring and
(Al-Salloum et al. 2015; Grote et al. 2001; Li and Meng 2003;
Protection, School of Civil and Mechanical Engineering, Curtin Univ.,
Perth 6102, Australia; Ph.D. Student, Institute of Geotechnical Engineer- Lv et al. 2017; Trindade et al. 2020; Zhang et al. 2009). Under high
ing, Zhejiang Univ., Hangzhou 310058, China. Email: zhijie.huang@ loading rate, concrete materials exhibited a strength enhancement,
curtin.edu.au including compressive and tensile strength, which could be quan-
2
Senior Lecturer, Centre for Infrastructural Monitoring and Protection, tified by the dynamic increase factor (DIF). The strength enhance-
School of Civil and Mechanical Engineering, Curtin Univ., Perth 6102, ment of concrete at high strain rate can be explained by the
Australia (corresponding author). Email: [email protected] following reasons: (1) the Stefan effect that free water within con-
3
John Curtin Distinguished Professor, Centre for Infrastructural crete forms thin viscous films that can induce opposing viscous
Monitoring and Protection, School of Civil and Mechanical Engineering,
force to maintain the integrity of concrete (Rossi 1991a, b); (2) the
Curtin Univ., Perth 6102, Australia. Email: [email protected]
4
Graduate Civil Engineer, School of Civil and Mechanical Engineering, inertia force that counters crack initiation and propagation, leading
Curtin Univ., Perth 6102, Australia. Email: [email protected] to lateral inertial confinement that restrains the deformation of con-
5
Ph.D. Student, Centre for Infrastructural Monitoring and Protection, crete (Hao et al. 2010; Li and Meng 2003; Rossi and Toutlemonde
School of Civil and Mechanical Engineering, Curtin Univ., Perth 6102, 1996); and (3) the aggregates cleavage that cracks tend to cut
Australia. Email: [email protected] through strong aggregates with short and straight paths (Brara
6
Senior Lecturer, Centre for Infrastructural Monitoring and Protection, and Klepaczko 2006; Wang et al. 2018). Over the last decades,
School of Civil and Mechanical Engineering, Curtin Univ., Perth 6102, intensive studies have been conducted to investigate dynamic
Australia. Email: [email protected]
mechanical properties of OPC (Al-Salloum et al. 2015; Brara and
Note. This manuscript was submitted on February 4, 2021; approved
on June 14, 2021; published online on November 25, 2021. Discussion Klepaczko 2006; Chen et al. 2011; Grote et al. 2001; Kim et al.
period open until April 25, 2022; separate discussions must be submitted 2019; Li et al. 2009; Malvar and Crawford 1998; Zhang et al.
for individual papers. This paper is part of the Journal of Materials in 2009). Due to the different microstructures associated with the
Civil Engineering, © ASCE, ISSN 0899-1561. reaction processes between OPC and GPC (i.e., polymerization
50 100
Compression Splitting tension
Unit: mm
Digital record system Oscilloscope & Amplifier
on the reflected wave (εr ) and transmitted wave (εt ) as follows value of transmitted wave εt ðtÞmax and can be calculated by using
(Lindholm 1964): Eq. (4). Therefore, the stress rate σ̇ and strain rate ε̇ of the specimen
can be estimated according to Eqs. (5) and (6), respectively
A (Tedesco and Ross 1993)
σðtÞ ¼ Eb b εt ðtÞ ð1Þ
As
R2b Eb
2C ftd ¼ ε ðtÞ ð4Þ
ε̇ðtÞ ¼ − b εr ðtÞ ð2Þ Rs Ls t max
Ls
Z t f td
εðtÞ ¼ ε̇ðtÞdt ð3Þ σ̇ ¼ ð5Þ
τ
0
Voltage (V)
0.0 0.00
-0.1 -0.05
-0.2 -0.10
-0.3 -0.15
0 50 100 150 200 250 300 350 400 450 500 0 50 100 150 200 250 300 350 400 450 500 550 600
Time ( s) Time ( s)
Fig. 2. Stress equilibrium check of the dynamic compressive test. Fig. 3. Stress equilibrium check of the dynamic splitting tensile test.
C47
C55
Fig. 4. Failure modes of GPC specimens under dynamic compression at different strain rates.
98.0 s-1
63.7 s-1
C47 C55
Fig. 5. Failure progress of GPC specimens under dynamic compression at different strain rates.
140
C47: strain rate 48.4 s-1 plotted for comparison. It is found that the trend of the energy ab-
C47: strain rate 63.7 s-1 sorption of the GPC specimens in the present study agrees with the
120
C47: strain rate 79.3 s-1 test data of highly fluidized GPC by Luo et al. (2013). However,
100 C55: strain rate 84.7 s-1 less energy was absorbed by the heat-cured GPC specimens from
C55: strain rate 98.0 s-1
Stress (MPa)
Tang et al. (2020) at similar strain rate, owing to the smaller speci-
80 men size (i.e., diameter 75 mm × length 37.5 mm) as compared to
60 the GPC specimens (diameter 100 mm × length 50 mm) in the
present study. The relation of energy absorption E versus strain rate
40 in the present study is fitted and given as follows:
20 C47∶ E ¼ 25.21ε̇ − 421.73; 48.4 s−1 ≤ ε̇ ≤ 98.3 s−1 ð7Þ
0
C55∶ E ¼ 19.61ε̇ − 236.59; 66.3 s−1 ≤ ε̇ ≤ 161.0 s−1 ð8Þ
0.000 0.005 0.010 0.015 0.020 0.025 0.030
Strain
Dynamic Increase Factor of the Compressive Strength
Fig. 6. Dynamic compressive stress–strain curves of GPC specimens at
different strain rates. The DIF, defined as the ratio of the dynamic strength to the static
strength, is used to quantify the strength increment of concrete-
like materials under dynamic loads. Concrete is a heterogeneous
material, which includes mortar, aggregates, voids, and micro-
and Lv et al. (2017) and it was named as compression wave phe- cracks. As mentioned in the “Introduction” section, three factors
nomenon in Lv et al. (2017). It is more evident when strain rate is contribute to the increment of strength of concrete, one of which
relatively low since specimens experience relatively low level of is the lateral inertial confinement induced by inertia force under
damage. With the increased strain rate, this phenomenon lessens dynamic loading (Hao et al. 2010; Li and Meng 2003). The lateral
due to severe damage of specimens. Table 3 gives the dynamic inertial confinement is considered as a structural effect. Therefore,
compressive strength of all the specimens under impact loading. the contribution of lateral inertia confinement to CDIF should be
The dynamic compressive strength of GPC increases with the removed from the test data. Previous studies (Hao et al. 2010; Wang
increase of strain rate, demonstrating GPC is a highly strain rate et al. 2018) showed that the lateral inertial confinement effect is
dependent material. specimen size and density dependent. For instance, the cylindrical
The energy absorption (Li and Xu 2009a; Luo et al. 2013; Su specimens with dimensions of 75 (diameter) × 37.5 mm (length),
et al. 2014, 2016) or impact toughness (Khan et al. 2018; Ren et al. 100 × 50 mm, 100 × 100 mm, and 200 × 100 mm have the con-
2015), which is defined as the area enclosed by the stress–strain tribution of 0%–5%; 4%–13%, 13.68 %, and 16.64% to dynamic
curve, is also calculated and listed in Table 3. The relation between strength increment, respectively. With the increase of strain rate,
the energy absorption and strain rate is shown in Fig. 7. It is found it increases slowly in low strain rate range but increases sharply
that the energy absorption of C47 specimens is slightly higher than after strain rate is higher than 200 s−1 (Hao et al. 2010). Since
that of C55 specimens and both of them increased approximately the strain rate in the present study was less than 200 s−1 and the
linearly with the rising strain rate. The higher energy absorption at specimen size was 100 × 50 mm, the contribution of lateral inertial
higher strain rate was due to more microcracks and fracture surfa- confinement effect to dynamic compressive strength increment was
ces (Ma et al. 2019; Tang et al. 2020), as illustrated in Fig. 5. The adopted as 10%, which was also used in Pham et al. (2020a). The
test data from Luo et al. (2013) and Tang et al. (2020) are also CDIFs after removing the lateral inertial contribution are listed in
5000 Highly fludized GPC (43 MPa, Luo et al. 2013) 3.0 C47
heat cured GPC (37 MPa, Tang et al. 2020) Fitted curve: C47
heat cured GPC (41 MPa, Tang et al. 2020) C55
C47 (present study)
Energy absorption E (kJ/m3)
2.0
E =25.21 -421.73, 48.4 s-1 98.3 s-1
2000 R2 =0.70
0 1.0
0 50 100 150 200 50 100 150 200 250 300
Strain rate Strain rate (s-1)
Fig. 7. Relation between energy absorption and strain rate of GPC Fig. 8. Relation between CDIF and strain rate of GPC specimens.
specimens.
Fig. 10. Failure modes of GPC specimens under dynamic splitting tension at different strain rates.
C47
2.27 s-1
C47
5.50 s-1
C55
4.75 s-1
C55
9.74 s-1
Fig. 11. Failure progress of GPC specimens under dynamic splitting tension at different strain rates.
Stress (MPa)
strain rate 9.80 s-1 strain rate 9.61 s-1
15 15
10 10
5 5
0 0
-5 -5
0 50 100 150 200 250 300 0 50 100 150 200 250 300
(a) Time ( s) (b) Time ( s)
Fig. 12. Time histories of dynamic splitting tensile stress of (a) C47; and (b) C55 specimens.
similar failure characteristics. At low strain rate (e.g., 2.27 s−1 for ends caused more energy absorption by the specimens at high
C47 and 4.75 s−1 for C55), the cracks initiated in the middle of the strain rate.
specimens and could hardly be seen at 550 μs. When the time
reached 800 μs, the disintegration of the specimens could be easily
Dynamic Increase Factor of the Splitting Tensile
observed, which was characterized by a main crack in the middle of
Strength
the specimens. Finally, the specimens failed into two halves with
minor concrete crushing at both ends. As the strain rate increased, Fig. 12 shows the time histories of dynamic splitting tensile stress
the disintegration occurred earlier, which could be found at 550 μs of C47 and C55. It is obvious that the peak splitting tensile stress of
for C47 specimens at the stain rate of 5.50 s−1 and C55 specimens GPC increased with the strain rate, which confirms that the GPC is
at the strain rate of 9.74 s−1 . It should be noted that some minor strain rate dependent. Moreover, the time to achieve the peak stress
cracks initiated from the edge near both ends besides a main crack. decreased in general as the strain rate increased. The test results of
These additional minor cracks and more concrete failure at both dynamic splitting tension are given in Table 4.
The relation between TDIF and strain rate of GPC specimens is
plotted in Fig. 13. C47 has slightly higher TDIF than C55, which
supports the recommendations by Committee CEB (1993) and
Table 4. Results of dynamic splitting tensile tests
Malvar and Crawford (1998) that OPC with lower strength exhibits
Dynamic splitting tensile higher TDIF. The TDIF is nearly linearly proportional to strain rate
Samples Strain rate (s−1 ) strength (MPa) TDIF in a logarithmical manner and the fitted curve can be expressed as
T-C47-1 2.08 11.96 2.9
T-C47-2 2.25 12.57 3.0 C47∶ TDIF ¼ 4.21 logðε̇Þ þ 1.42; 2.08 s−1 ≤ ε̇ ≤ 9.80 s−1
T-C47-3 2.27 12.25 2.9 ð11Þ
T-C47-4 4.98 17.08 4.1
T-C47-5 5.08 18.74 4.5 C55∶ TDIF ¼ 4.38 logðε̇Þ þ 0.89; 3.19 s−1 ≤ ε̇ ≤ 10.33 s−1
T-C47-6 5.43 20.01 4.8
T-C47-7 5.48 19.27 4.6 ð12Þ
T-C47-8 5.50 19.32 4.6
T-C47-9 5.56 16.69 4.0
T-C47-10 5.62 19.27 4.6 9.0 C47
T-C47-11 5.89 20.70 4.9 Fitted curve: C47
T-C47-12 6.69 19.52 4.6 8.0 C55
T-C47-13 6.83 19.34 4.6 7.0 Fitted curve: C55
T-C47-14 8.49 22.57 5.4
T-C47-15 9.80 25.22 6.0 6.0 TDIF=4.21log( )+1.42, 2.08 s-1 9.80 s-1
T-C55-1 3.19 14.17 3.0 R2 =0.92
TDIF
5.0
T-C55-2 4.61 18.36 3.8
T-C55-3 4.75 18.92 3.9 4.0
T-C55-4 7.14 21.33 4.4 3.0
T-C55-5 7.20 24.12 5.0
T-C55-6 7.42 23.51 4.9 2.0 TDIF=4.38log( )+0.89, 3.19 s-1 10.33 s-1
T-C55-7 8.29 24.02 5.0 1.0 R2 =0.92
T-C55-8 8.52 23.13 4.8
T-C55-9 8.71 22.87 4.8 0.0
1 10
T-C55-10 9.32 25.31 5.3
-1
T-C55-11 9.60 23.46 4.9 Strain rate (s )
T-C55-12 9.61 25.22 5.3
T-C55-13 9.74 24.67 5.1 Fig. 13. Relation between splitting TDIF and strain rate of GPC
T-C55-14 10.33 26.18 5.5 specimens.