5100 - Operating Instruction Manuals

NO.
378M
Parr Instrument Company
5100
Low Pressure Reactors
Operating Instruction Manual
5100 Low Pressure Reactors
Table of Contents
Preface — 4 Accessories — 13
Scope — 4 Air Motor — 13
Related Instructions — 4 Spare Parts Kit — 13
Safety Information — 5 Mantle Heaters — 13
General Specifications — 5 Variable Speed Electric Motor — 13
Explanation of Symbols — 6 Cooling Loop — 13
Environmental Conditions — 6
Provisions for Lifting and Carrying — 6 Explosion Proof Operation — 14
Intended Usage — 6
Cleaning & Maintenance — 6 Periodic Pressure Tests — 14
Users Responsibility — 7
Unpack Carefully — 7 General Maintenance Notes — 15
Installation — 8 Parts List — 16
Pressure and Temperature Limits — 8 Cylinders — 16
Heads* — 16
Assemble the Reactor — 8 Dip Tubes — 16
Assembling and Connecting the Circulator Jacket Male Connectors — 16
Hoses — 10 Cooling Loop — 16
Draining the Jacket — 10 Stirrer Support Bracket — 17
Stirrer Shaft and Impellers — 17
Identify the Valves — 11 Stirrer Shaft and Impellers — 17
Gas Inlet Valve — 11 Thermowell and Thermocouple — 18
Gas Release Valve — 11 Gaskets and Seals — 18
Liquid Sampling Valve — 11 Split Ring — 18
Relief Valve — 11 Accessories — 19
Magnetic Drive Parts (for A1120HC9 Drive) — 19
Other Vessel Head Fittings — 11 Heaters — 19
Safety Rupture Disc — 11 Product Features and Part Identification — 20
Pressure Gage — 11
Type J Thermocouple — 11 Figures
Stand for 1 - L and 1.5 L Vessels — 20
How to use the Vessel — 12 Stand for 160 - 600 mL Vessels — 21
Gas Connections — 12 5100 Stand — 22
Pressurizing the Vessel — 12 5100 Overarm — 23
Do Not Overfill the Vessel — 12 5100 Internals — 23
Releasing Pressure — 12 5100 Head Assembly — 27
Withdrawing Liquid Samples — 12 5110 Head Assembly — 28
Initial Operating Test — 12
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Preface Related Instructions

Scope The following Parr publications are also available to
further your understanding of this instrument and its
These instructions describe the installation, operation component parts:
and maintenance of Parr Series 5100 Fixed Head Bench
Top Reactors offered in six sizes from 160 mL to 1.5 L No. Description
with glass and/or metal cylinders. They cover the basic 230M Safety Precautions to be observed when
steps to be followed for installing these reactors and operating Pressure Reaction Equipment
describe the function of all standard components. They
231M Operating Instructions for Parr Safety Rupture
are intended to be used in conjunction with several
Discs
related instruction sheets listed on the previous page.
This information describes several components which 548M Operating Instructions for 4848 Reactor
are common to most Parr pressure reaction equipment, Controllers
and includes safety precautions and other related 549M 4848 Controller CD-ROM
information applicable to all reaction laboratories. The 553M Operating Instructions for A2110E Motor
users should study all of these instructions carefully Controller
before starting to use these vessels so that they will 234M Operating and Maintenance Instructions for
fully understand the capabilities and limitations of the Parr Magnetic Drives
equipment.
323M Operating Instructions for Parr Pressure Relief
Valves
201M Limited Warranty
F0042 Health & Safety Assurance Certification
Customer Service:
Questions concerning the installation or operation of this instrument
can be answered by the Parr Customer Service Department:
1-309-762-7716 • 1-800-872-7720 • Fax: 1-309-762-9453

E-mail: [email protected] • http://www.parrinst.com
4 Parr Instrument Company

Safety Information General Specifications
To avoid electrical shock, always: Electrical Ratings
1. Use a properly grounded electrical outlet of correct Controller ratings are found in the Operating
voltage and current handling capability. Instructions for the controller supplied with your
2. Ensure that the equipment is connected to electrical reactor and on the controller data plate.
service according to local national electrical codes.
Failure to properly connect may create a fire or Before connecting a controller to an electrical outlet,
shock hazard. the user must be certain that the electrical outlet has
3. For continued protection against possible hazard, an earth ground connection and that the line, load and
replace fuses with same type and rating of fuse. other characteristics of the installation do not exceed
4. Disconnect from the power supply before the following limits:
maintenance or servicing.
Voltage: Fluctuations in the line voltage should not
To avoid personal injury: exceed 10% of the rated nominal voltage shown on the
1. Do not use in the presence of flammable or data plate.
combustible materials; fire or explosion may result.
This device contains components which may ignite Frequency: Controllers can be operated from either a
such material. 50 or 60 Hertz power supply without affecting their
2. Refer servicing to qualified personnel. operation or calibration.
Current: The total current drawn should not exceed

the rating shown on the data plate on the controller by
more than 10 percent.
Thermocouple: Unless otherwise specified, all

Series 4848 Controllers operate with a Type J (iron-
constantan) thermocouple. The total resistance of the
thermocouple and the lead wires should not exceed
20 ohms. If the resistance of the thermocouple circuit
is higher, it will reduce the sensitivity of the control
system.
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Explanation of Symbols
II On position, full power heater switch
I On position, half power heater switch
O Off Position
~ Alternating Current (AC)
This CAUTION symbol may be present on the Product Instrumentation

and literature. If present on the product, the user must consult the appropri-
ate part of the accompanying product literature for more information.
This CAUTION symbol indicates that the surface may be hot.
Protective Earth (PE) terminal. Provided for connection of the Protective

Earth (green or green/yellow) supply system conductor.
Environmental Conditions Intended Usage

This instrument is intended to be used indoors. This system has been designed for use as a low pressure
reactor system. It has been designed, built, and tested
Operating: 15 ºC to 35 ºC; maximum relative humidity to strict physical and electrical standards. However,
of 80% non-condensing. Installation Category II (over it is the user's responsibility to install and operate it in
voltage) in accordance with IEC 664. conformance with local pressure and electrical codes.
Pollution degree 2 in accordance with IEC 664. If the instrument is used in a manner not specified by
Altitude Limit: 2,000 meters. Parr Instrument Company, the protection provided by
the equipment may be impaired.
Provisions for Lifting and Carrying
Cleaning & Maintenance
The Parr Series 5100 Fixed Head Bench Top Reactors
and its components are very heavy. Before moving Periodic cleaning may be performed on the exterior
ensure all cables are disconnected. Use proper and safe surfaces of the controller with a lightly dampened cloth
lifting techniques when installing or moving the Parr containing mild soap solution. All power should be
Series 5100 Fixed Head Bench Top Reactors and/ or its disconnected and the power cord should be unplugged
components. when cleaning the instrument.
There are no user serviceable parts inside the product

Caution! other than what is specifically called out and discussed
Do not use in hazardous atmospheres. in this manual. Advanced troubleshooting instructions
beyond the scope of this manual can be obtained by
calling Parr Instrument Company in order to determine
which part(s) may need to be replaced or serviced.
Ensure that any hot surfaces have had

adequate time to cool before cleaning
or maintaining the reactor and/or its
components.

Users Responsibility 2. Install and operate the equipment within a suitable
All Parr reactors and pressure vessels are designed and barricade, if required, with appropriate safety
manufactured with great care to assure safe operation accessories and in full compliance with local safety
when used within their prescribed temperature and codes and rules.
pressure limits.
3. Establish training procedures to ensure that any
But… the basic responsibility for safety when using this person handling the equipment knows how to use it
equipment rests entirely with the user; who must: properly.
1. Select a reactor or pressure vessel that has the 4. Maintain the equipment in good condition and
capability, pressure rating, corrosion resistance, establish procedures for periodic testing to be sure
and design features that are suitable for its intended the vessel remains structurally sound.
use. Parr engineers will be glad to discuss available
equipment and material options with prospective
users, but the final responsibility for selecting a
Unpack Carefully
reactor or pressure vessel that will perform to the Unpack the equipment carefully and check all the
user's satisfaction in any particular reaction or test parts against the packing list. If shipping damage is
must rest with the user - not with Parr. discovered, report it immediately to the delivering
carriers. Examine the components closely for any loose
In exercising the responsibility for the selection of
parts or shipping damage and be sure to check all layers
pressure equipment, the prospective user is often
of packing materials thoroughly so as not to overlook
faced with the choice between over- or under-
any parts which might otherwise be discarded.
designed equipment. The hazards introduced
by under-designed pressure vessels are readily
apparent, but the penalties that must be paid for
over-designed apparatus are often overlooked.
Recognizing these criteria, Parr reactors and
pressure vessels are offered in several different
styles, each designed for convenient use in daily
operation within certain temperature and pressure
limits, using gaskets, closures, and other elements
carefully selected for safe operation within the limits
specified for that design. But in order to preserve
the validity of these designs, all temperature and
pressure limits must be observed, and no attempt
should be made to increase these limits by making
alterations or by substituting components which are
not recommended by Parr Instrument Company.
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Installation Assemble the Reactor

These reactors require at least 10 inches of workspace
Pressure and Temperature Limits from walls or flammable materials on a sturdy bench,
table, or floor in a well ventilated area with convenient
The maximum working conditions for Parr vessels are access to an electric outlet, running water, and a drain.
stamped on the cylinder. No attempt should be made If the tabletop is not heat resistant it would be ideal
to increase these limits by making alterations or by to provide an insulated pad on which to set the vessel
substituting components which are not recommended when it is hot.
by the Parr Instrument Company. It must also be
understood that lower pressure and temperature limits Review the following instructions first, prior to
may be required for modified reactors and for vessels assembling the reactor.
made of special alloys. Limits for such vessels will be
determined by the physical characteristics of the vessel 1. Set the stand in the workspace.
material and will be prescribed on an individual basis.
Working temperatures up to 225 °C are permissible Bolt the stand to a workbench or to the floor
in reactors equipped with fluoroelastomer (FKM) using the holes in the base plate.
O-ring seals, such as Viton®. The higher the operating
temperature above 200 °C, the shorter the life of the
O-ring will be. Perfluoroelastomer (FFKM) O-ring
seals such as Kalrez® have a broad chemical resistance. Place the head assembly in the stand. Make sure the
Unfortunately, they are very expensive and will O-ring that seals the head and the cylinder together is
generally be reserved for unique applications. Ethylene installed in the head groove.
propylene (EP) O-rings can be used to 170 °C and are
recommended for applications where solvents such Two types of glass cylinders can be used with
as ammonia and amines which will rapidly destroy this apparatus (jacketed and non-jacketed) If a
fluoroelastomer O-rings. jacketed cylinder is being used, remove the jacket
connection hoses, if present. A pair of split rings, with
The maximum working pressure and temperature thumbscrews, is used to join the head and the cylinder
for any vessel is governed by the design of the vessel flanges. The split rings are lined at the bottom with
and the strength of the material from which it is plastic cushions that eliminate metal against glass
constructed. There is also a close relationship between contact that could result in dangerous point loading on
working pressure and temperature since the strength of the glass. Examine the plastic cushions carefully. If they
any material will normally fall off as the temperature are cracked or otherwise appear damaged, they should
is increased. Temperature and pressure limits are also be replaced.
affected by the physical properties and temperature
limits of the gaskets and seals used in the vessel, and CAUTION! Take care when handling the
by any valves, gages or other fittings attached to the glass cylinder. If any of the pressure or
vessel. Obviously, the safe operating pressure of any load bearing surfaces become chipped or
system can be no higher than that of its lowest rated scratched, the pressure rating of the cylin-
component.
der will be compromised.
All Parr reactors show the maximum safe operating
pressure and temperature imprinted on the cylinder. If a metal cylinder is also being used with this
The working pressure and temperature in these 160 apparatus, note that the split rings differ from those
mL to 1.5 L reactors must not exceed the following provided for a glass cylinder. Split rings intended for
maximum limits: sealing a metal cylinder to a metal head should not be
used with glass cylinders. A clasp system on both ends
of the split rings is used to ensure proper alignment
Pressure and Temperature Limits when assembled. Before using the split rings to mate the
Bomb Maximum Maximum head and the cylinder, make sure the three thumbscrews
Material Pressure Temperature on each half ring are backed off so that the end of the
Glass 150 psi 225 °C screw is flush with the inside of the split ring. Both sets
of split rings feature thumb screws to be installed finger-
T316 SS 1000 psi 225 °C tight.

Carefully bring the flange of the glass cylinder in Labeled connections are provided on the rear panel of
contact with underside of the reactor head. A lab jack the controller.
/ cork support is provided for 1.0 and 1.5 liter glass
reactors. When using the lab jack, bring the cylinder
flush with the O-ring in the head, ensuring no stress Parr Cooling Only:
is put on the glass. Align the major OD of the head
with the OD of the cylinder flange. If a jacketed
cylinder is being used, orient the cylinder so that the
jacket connections are oriented to either side. Hold The Parr Cooling output connector is to be used only
the cylinder carefully at the bottom with one hand, with Parr Instrument Company cooling solenoid valve
slide one of the half split rings onto the head/cylinder assemblies supplied with the appropriate cooling power
flanges, and rotate/slide around the head/cylinder cord.
flanges until the latches are facing you. Use one hand to
steady this half split ring to the head/cylinder flanges
as you attach the other half split ring from the front. Parr Heating Only:
Secure the latches. If using a lab jack, now lower it so
that cylinder hangs freely.
At this point, the glass cylinder will be held in place The Parr Heating output connector is to be used
loosely and can be rotated for proper orientation if only with Parr Instrument Company heater
needed. Tighten the six thumb screws in a criss-cross assemblies supplied with the appropriate heater
pattern rather than progressively around the circle until power cord. Note: Do not make connections to a
finger-tight and the head flange is flush with the top of Variac, Powerstat or the like to attempt to control
the cylinder flange. Do not over-tighten. the heating output. The heavy inductive load
on the primary side of such devices can destroy
CAUTION! Never use tools, such as pliers, the internal sold state relay located in the 4848
to tighten the thumbscrews. Excessive load- Controller.
ing on the cylinder flange can compromise
the pressure rating of the cylinder. Motor:
Secure the clamp on motor cord to the
controller with the provided screw next to
WARNING! Before applying pressure to the motor socket for safety purposes.
the reactor, install the transparent Lexan
safety shield onto the front of the reactor
3. The support and heater are shipped fully assembled.
stand. Failure to do so can result in serious
The heater raises and lowers on its support rod to
injury if the cylinder should break under
pressure. permit the vessel or cylinder to be removed. Lower
the heater, open the hinged retainer on the front
of the support and slide the vessel into its support.
To remove the cylinder from the head, follow the above Fixed head vessels have a square lip which fits into
procedure in the reverse order. If a jacketed cylinder is a matching groove in the support plate. Removable
being used, drain and disconnect the jacket hoses first. vessels are supported by the split rings which rest on
top of the support plate. The stirrer drive connector
2. Set the Temperature Controller near the reactor, lifts by rotating and lifting the knob above the belt
leaving a space of at least six inches between the guard. The universal joint contains a cross pin that
controller and the base of the reactor so that the slips into the groove on top of the magnetic drive.
controller will not be unduly affected by radiant
heat. Connect the reactor to the controller using 4. Connect the heater cord from the heater into the
information contained in its Instruction Manual heater socket on the rear panel of the Series 4848
548M or follow the steps below. Reactor Controller.
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5. Plug the motor cord into the motor socket on the
rear of the controller.
Assembling and Connecting the
Circulator Jacket Hoses
Secure the clamp on the motor cord with
the provided screw next to the motor CAUTION! If a jacketed vessel is being
socket for safety purposes. used, the compression fittings should be
pre-assembled onto the insulated hoses
before attaching them to the cylinder.
6. Connect the thermocouple extension wire to both
Failure to do so or tightening any of the
the thermocouple and to the controller in the
compression fittings while the hoses are
“Primary Temp Input” position on the rear panel.
attached to the cylinder will likely cause
Insert the thermocouple into thermowell.
the jacket nipple to break off.
7. Connect leads from accessory packages such as
tachometer, pressure transducer and high temp cut- Once the hoses are fixed at one end, they tend to have
off to the designated positions on the back panel of a preferred orientation. The following hose assembly
the 4848 Controller. procedure will minimize any side loading by the hoses
against the jacket connection nipples.
8. Connect cooling water to internal cooling coil if
installed. Attach the hoses to the circulating bath first and route
them through the openings at the rear of the reactor
9. Connect cooling water to the magnetic stirrer. See stand. Note that lower left connection is the jacket
Instruction Manual 234M. inlet. This should be connected to the circulator pump
discharge. Elbows are used on the cylinder end to route
10. Connect tubing to the rupture disc outlet and run to the insulated hoses down and then out the rear of the
a safely vented area. See Instruction Manual 231M. stand. With the hose in its free state and not being
twisted or rotated, tighten the elbows to the hoses in a
11. Note the voltage requirement on the controller manner that orients the open end of the elbow in line
identification label on the back panel, and then plug with the jacket nipple. This minimizes any side loading
the power cord into an appropriate outlet. Power of the hose against the nipple.
for these reactors should be drawn from a 3-slot,
grounded outlet capable of carrying up to the full
Slide the brown plastic nut onto the nipple adapter so
current rating of the system.
that the flange with the O-ring groove is recessed inside
the nut. Tighten the tube stub onto the elbow. Place the
12. Using the switch on the Temperature Controller,
turn on the motor for a short run to check the stirrer O-ring in the groove of each of the assembled adapters
drive system. and then screw the hose adapter onto the jacket nipple.
Tighten firmly, by hand only! No pliers!
This apparatus includes a safety shield Draining the Jacket

which should be used at all times. A relief
valve set to 150 psi is also provided as a To drain the jacket, first lower the temperature of the
safety precaution to prevent over-pressuriz- jacket circulating fluid to 60 °C or less.
ing the glass cylinder - this also should be
used at all times. Should this relief valve Note: Oil, used as the circulating fluid, drains much
be inadvertently removed, the glass vessel faster when it is hot.
could be over-pressurized, resulting in an
explosion. The safety shield has been de- Turn off the circulator and loosen the hose connection
signed to withstand the force of this explo- at the top of the jacket. This will allow air to enter
sion. However, in the event of an explosion, the jacket and cause to fluid to drain back into the
some glass fragments will exhaust through circulator. When the draining is complete, both hoses
the vertical slots provided in the back of the can be disconnected from the jacket. The ends of the
shield for the hoses. hoses should be supported at a level higher than that of
the circulator bath to prevent siphoning and fluid loss.

Identify the Valves Other Vessel Head

Gas Inlet Valve Fittings
The gas inlet valve is easily identified when the vessel
is open by noting that it is connected to a dip tube
Safety Rupture Disc
There is a safety rupture disc attached to the head
which extends to a point near the bottom of the vessel
which is intended to rupture and release the pressure
cylinder. This is an angle valve with an attached fitting
before it reaches a dangerous level. A metal tag wired
which provides a socket for attaching the A495HC
to the safety head identifies the burst pressure at room
pressure hose furnished with the reactor.
temperature for that particular disc. A similar tag is
furnished with each replacement disc. This tag must
Gas Release Valve remain with the apparatus at all times so that both
The gas release valve is connected to the gage adapter present and future operators will be aware of the disc
on vessels with volumes of 160 – 600 mL. The gas rating. Users should read the discussion of rupture discs
release valve is installed in a port by itself on 1 L & given in the Instruction Sheet No. 231M for a complete
1.5 L vessels. These ports do not have a threaded description of the characteristics of rupture discs and
connection on the underside of the head; they are the precautions to be observed when operating pressure
always open to the gas phase of the reactor. equipment protected by this type of safety device. The
disc is rated for 1000 psi and should remain installed for
both glass and metal cylinders.
Liquid Sampling Valve
The liquid sampling valve is attached to the same fitting
as the gas inlet valve and connected to a common dip Pressure Gage
tube. With this arrangement, incoming gas is always A pressure gage, typically 200 psi gage for glass
introduced below the surface of the liquid and the cylinders and 1000 psi gage for metal cylinders includes
operator is provided with a means for clearing the dip a T316 Stainless Steel Bourdon tube. It is mounted on
tube to be sure that any sample taken during a run will the head using attachment fittings similar to those used
be representative of the charge. This can be done by for the inlet/sampling valve assembly.
opening the upper gas inlet valve momentarily to allow
the inlet gas to force any liquid in the dip tube back
into the reactor before withdrawing a sample from the
Type J Thermocouple
A Type J thermocouple in a 1/8” diameter stainless
sampling valve.
steel sheath is furnished with the reactor. Insert this
thermocouple into the head thermowell and connect
Relief Valve it to the thermocouple socket on the rear panel of
The relief valve is connected to the gage adapter and is the temperature controller using the A470E Series
pre-set to 150 psi to ensure that the glass cylinder is not extension wire furnished with the reactor.
over-charged. When using a metal cylinder, a plug is
provided so that the relief valve can be removed (due to
higher pressure rating of metal cylinder).
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How to use the Vessel liquid in the vessel can lead to development of
dangerous pressures if sufficient space is not provided
for expansion when the liquid is heated. This hazard
is explained in greater detail in a warning statement
Gas Connections included in the Instruction Manual No. 230M.
Gas connections are dependent on applications. For
general usage, use the pressure hose furnished with the
reactor. Screw the Type “A” coned pressure fitting into Releasing Pressure
the adapter attached to the gas inlet valve and tighten Use the gas release valve to reduce the pressure in
the compression nut firmly. Do not use any thread the vessel if the reactor is accidentally overcharged
dope on the coned fining. The A495HC pressure hose when filling. Use this valve also to release any excess
is made of reinforced Nylon which can be used for all pressure during a run and to exhaust the vessel at the
noncorrosive gases at pressures up to 2500 psig. For end of a run. If the discharge gases are flammable or
operations involving corrosive gases, this hose should toxic, discharge to an exhaust hood or to any other safe
be replaced with an A490HC hose which has a PTFE release point.
lining and a braided stainless steel outer covering. Both
of these hoses have the same fittings. An A506HC all
metal hose is also available in stainless steel and other Withdrawing Liquid Samples
corrosion resistant materials. Liquid samples may be withdrawn from the sampling
valve attached to the inlet fitting whenever the vessel
is pressurized. Always close the inlet valve before
Pressurizing the Vessel withdrawing a liquid sample and open the sampling
Check all valves carefully before admitting gas into valve cautiously because liquid will be discharged with
the system. The liquid sampling valve must remain considerable force. A delivery tube may be attached
closed throughout the charging procedure. The gas to the sampling valve to discharge the liquid into an
release valve must also be closed unless the vessel is to appropriate receiver. Be particularly careful if the
be purged, or unless there is to be a continuous flow temperature of the sample is above its boiling point at
through the reactor during a run. Always make certain atmospheric pressure. If so, it will “flash” and be lost
that the pressure in the gas tank is greater than the as soon as it is released from the vessel. This problem
pressure in the vessel; otherwise, liquid will be forced can be avoided by connecting an optional metal sample
out of the vessel and into the gas tank when the inlet bottle to the valve and collecting the sample in a sealed
valve is opened. If there is any possibility that the tank container. Incoming gas can be used to clear the dip
pressure might not be high enough to force gas into the tube between liquid samples so that the next sample
reactor, install a one-way check valve (optional) in the drawn through the tube will truly be representative of
gas line to prevent any reverse flow. With the inlet valve the mixture.
open and the flow control valve on the gas tank closed,
open the main valve on the gas tank only about one-
quarter turn; then use the flow control valve or the valve Initial Operating Test
on a pressure regulator to control the flow of gas into Read all operating instructions carefully so as to be well
the vessel. After the desired pressure has been reached, acquainted with the correct procedures for handling
close the tank valves and the vessel inlet valve and the vessel and for operating the controller and other
disconnect the hose at the vessel end. accessories. An initial operating test should be made,
with only water, to check the apparatus before starting
the first experimental runs. For this initial test, fill the
Do Not Overfill the Vessel cylinder not more than half full of water and run the
Always watch the pressure gage closely when admitting temperature up to 150 ° C while checking the apparatus
gas so as not to exceed the maximum working limit. for leaks and observing the performance of the
Remember that any subsequent increase in temperature temperature controller.
will raise the pressure. Also, be sure that the amount of
liquid placed in the vessel is carefully controlled.
As a general rule, the liquid charge should not exceed

two-thirds of the capacity of the cylinder. Too much

Accessories Mantle Heaters

Mantle heaters with high temperature fabric heating
mantles housed in sturdy aluminum shells can be
Air Motor provided for any plain (non-jacketed) cylinder.
Variable stirring speeds from 100 to 2000 rpm with These heaters are designed to provide uniform heat
no spark hazard can be obtained by replacing the distribution to the walls and bottoms of these vessels.
standard motor with an air motor. This motor operates They are attached to a support rod with a spring
on compressed air which must be supplied at 40 psig steel clamp and arranged so that they can be raised
minimum pressure with at least 10CFM available at that or lowered on the rod as desired. Each mantle must
pressure. It is furnished with a speed control valve and always be used with the vessel of the size for which it
oiler, all assembled on a mounting bracket. was designed, and must always be fully attached to the
To operate reactors equipped with an air motor, vessel before heat is turned on. Similarly, a short vessel
mount the drive system firmly on the support stand must never be heated in a deep mantle. Without full
and connect the air hose to a compressed air line. Fill contact with a vessel wall, a mantle will overheat and
the oiler with SAE 10 oil and adjust the oiler to feed burn out.
one drop per minute into the air stream. For long
continuous runs at high speeds, the oiling rate should
be increased to three drops per minute. If the motor
Variable Speed Electric Motor
Reactors are normally equipped with a DC variable
becomes sluggish, flush it with a non-flammable solvent
speed motor supplied and controlled through the
in a well-ventilated area. Disconnect the air line and
Series A2110E or 4840 Controllers. Instructions for
muffler and pour a small amount of solvent into the
connecting and operating these motors are included in
inlet port. Rotate the shaft by hand in both directions
the controller’s instruction manual No. 553M or 548M.
for a few minutes; then connect the air line and run
This motor is installed in a drive system designed to
the motor until there is no further trace of solvent in
produce stirring speeds from 0 to 1700 rpm.
the exhaust. If the muffler felts are dirty, wash them
in solvent or replace them. Relubricate the motor with
a squirt of oil into the chamber and reassemble. If it Cooling Loop
becomes necessary to disassemble the motor to replace Each 5100 Reactor has a single loop cooling coil
the vanes, follow directions given in the instruction installed in the vessel (except the 160 & 215 mL units).
sheet published by the Gast Manufacturing Corp., A slow, continuous flow of cold water through a cooling
Benton Harbor, Michigan. loop proves a very effective means for controlling
temperature overshoot in these reactors, particularly
when operating at temperatures below 150 °C. Water
Spare Parts Kit flow through the loop can be controlled automatically
Parr can furnish spare parts kits for these reactors
using a solenoid valve in the cold water line, with the
which will provide a reserve supply of parts and tools
solenoid connected to the cooling socket on the rear
sufficient to handle most normal replacements and
panel of the 4840 Temperature Controller. With this
emergency repairs during a year of heavy usage.
arrangement, cold water will be admitted to the cooling
These kits contain replacement gaskets, packing,
loop whenever the controller calls for cooling.
O-rings, shafts, bearings, and rupture discs. They can
be ordered from any Parr Dealer or direct from the
Parr Instrument Company. The order must specify the
reactor size and indicate type of rupture disc, stirrer
drive and whether it has a flat-gasket or O-ring closure.
www.parrinst.com 13
4. The Wiring
Explosion Proof The wiring provided with the standard reactor systems
does not meet the standards prescribed for explosion
Operation proof operation. Optional, intrinsically safe barriers are

available.
If the local safety code requires that equipment installed

in the user’s laboratory must be explosion proof, there
are four possible ignition hazards to be considered: Periodic Pressure Tests
1. The Motor Each cylinder used in a Parr stirred reactor is tested
The standard adjustable speed motor is not explosion under hydrostatic pressure to 1.3 times its maximum
proof, yet these motors are not unduly hazardous if rating before it is released from the factory. Micrometer
operated in a well ventilated location where care is caliper measurements are taken during this test to check
taken to prevent the accumulation of explosive gases the deflection of the walls and bottom of the cylinder
or vapors. To eliminate any possible spark hazard under pressure. Excessive deflection or failure of the
originating at the motor, Parr can furnish an air motor metal to resume its original dimensions after pressure
as described previously, or the reactor can be equipped is released indicates that a cylinder is potentially unsafe
with a variable speed, explosion proof motor that is and it will be rejected. Similar tests should be made
approved for use in Class 1, Groups C & D, and Class at regular intervals during the life of each cylinder,
2, Groups E, F, & G atmospheres. Explosion proof and particularly whenever the user suspects that the
motors are furnished with a temporary power cord and equipment has been over-stressed or damaged.
plug which are not explosion proof. The user should
remove this temporary wiring and replace it with an Some laboratories maintain hydraulic test facilities and
explosion proof switch and wiring which will comply make it a rule that all pressure vessels must be tested
with the local electrical code. at regular intervals. Records are kept of deflections
at specific test pressures so that any increase in
2. The Temperature Controller deflection becomes a warning that the metal has lost
The Series 4848 Temperature Controllers furnished strength. Any cylinder which fails to return to its
with these reactors contain switches and other elements original dimensions after application of the prescribed
that are not explosion proof. The minimal spark hydrostatic test should be discarded as unsafe for further
hazard associated with these units can be resolved by use.
installing the controller in a remote location outside of
the hazardous area or by enclosing it in an approved Users who do not have pressure test facilities can return
explosion proof housing. If enclosed within a positive any Parr pressure vessel to the factory for hydrostatic
pressure, clean air housing, the discharge from the testing and overhaul. This should be done whenever
housing must be directed into a safe area. If requested, the metal shows excessive damage from corrosion or
Parr will furnish the long lead wires needed to mount whenever an over-pressure or other unusual occurrence
the controller in a remote location. If the controller is raises any safety questions. To return a vessel for
to be installed in an explosion proof housing, the user repair contact Parr Instrument Company for a return
must provide the necessary housing and installation. authorization number. Apparatus returned for testing
and overhaul should be shipped prepaid to the Parr
3. The Heater Instrument Company, 211-53rd Street, Moline, Illinois
The elements in the heater could be dangerous in an 61265. An order or letter of instructions should be
explosive atmosphere if the surface temperature of mailed to the same address, as no repair work will be
the element becomes high enough to ignite flammable started without specific instructions and a Health &
vapors. This hazard must be evaluated for each Safety Assurance Certification form (F0042) signed by a
individual installation since major modifications responsible user.
are required if the heater must be isolated from the
surrounding atmosphere. Users who consider this
a significant hazard are urged to contact the Parr
Instrument Company for further discussion and
suggestions that might be helpful.
General Maintenance metal parts, but do not place a thermocouple

probe, pressure gage, face seals or ball bearings
in an ultrasonic bath. Periodic cleaning may be
Notes performed on the exterior surfaces of the reactor
stand with a lightly dampened cloth containing mild
soap solution. All power should be disconnected
1. Periodically inspect all electrical wiring and pressure
when cleaning.
connections for excessive corrosion. Suspect parts
should be replaced by components only supplied by
9. Routinely inspect cap screws on split ring closure
Parr Instrument Company.
for lubrication and cleanliness. These screws should
not be allowed to dry because the threads will seize.
2. Always use appropriate wrenches on all fittings and
Regularly apply Parr High Temperature Anti-Seize
valves. Never use pliers or pipe wrenches.
Lubricant (Parr No. 424HC2) before this happens.
3. Head and cylinder service fixtures are available for
10. To operate reactors equipped with an air motor,
convenience and protection of components during
connect air hose to a compressed air line. For best
maintenance of your reactor.
torque and speed control the piping to the motor
should be at least 3/8” IPS or larger. Fill the oiler
4. To reinstall straight thread (NPS) fittings to the
with SAE 10 oil and adjust the oiler feed one drop
head, screw the gage or valves firmly into the
per minute into the air stream. For long continuous
adapter. Run the bushing onto the threaded stem
runs at high speeds the oiling rate should be
as far as it will go. Screw this assembly into the
increased to three drops per minute. If the motor
head until the nose of the adapter is seated; then
becomes sluggish, flush it with a non-flammable
back it off until the valve or gage is facing in the
solvent in a well ventilated area.
desired direction (no more than one full turn).
Disconnect the air line and muffler and pour a small
Hold the fitting firmly in place and close the joint
amount of solvent into the inlet port. Rotate the
by tightening the bushing. This connection can be
made and broken repeatedly without destroying shaft by hand in both directions for a few minutes;
the sealing surfaces. A light coating of thread then connect the air line and run the motor until
lubricant, such as Parr High Temperature Anti-Seize there is not further trace of solvent in the exhaust.
Lubricant, applied to the straight threads and to the If the muffler is dirty, replace it. Re-lubricate the
nose of the adapter will help to obtain a tight joint. motor with a squirt of oil into the chamber and
Note: PTFE tape should not be used on this joint. reassemble.
5. NPT (National Pipe Taper) threads should not If servicing assistance is needed, contact Parr
be disassembled any more than necessary. It will Instrument Company directly at 800-872-7720 or at the
become increasingly difficult to maintain a tight seal address shown on the back of these instructions.
with these tapered threads if the joint is made and
broken repeatedly. Grafoil tape or PTFE tape (if
temp allows) should be used on all NPT threads.
6. Do not use oil or anti-seize lubricant on threads or

fittings if the vessel is to be used with oxygen.
7. If your vessel is equipped with a loose compression

ring be sure that it is in place on the head before
attaching any head fittings. The compression ring
cannot be installed after fittings have been screwed
into the head.
8. Clean all threads and gas passages thoroughly and

remove all tape fragments when overhauling a
vessel. An ultrasonic bath is excellent for cleaning
www.parrinst.com 15
Parts List Part No. Description
*Note: Special material internal parts (not T316) will

Heads*
have a suffix designating the material: 2635HC3 Head for 160 mL - 600 mL, T316
2635HC4 Head for 160 mL - 600 mL, T316, footless
CH Alloy C-276 CA Titanium mag drive
CB Alloy Cb-20 CX Zirconium
CG Alloy B-2 HZ PTFE coated T316 2915HC2 Head for 1000 mL - 1500 mL, T316
2915HC3 Head for 1000 mL - 1500 mL, T316, foot-
(I.e.- a 300 mL Alloy C-276 dip tube would be less mag drive
832HC31CH)
Dip Tubes
Part No. Description 832HC35 Dip tube, 160 mL, T316, .75” length
832HC35HZ Dip tube, 160 mL, PTFE coated, T316
Cylinders 832HC36 Dip tube, 215 mL, 1.46” length
832HC36HZ Dip tube, 215 mL, 1.46” length, PTFE
For 160 mL - 600 mL: coated, T316
2525HC4 Cylinder, Glass, 160 mL 832HC31 Dip tube, 300 mL, T316
2525HC14 Cylinder, Glass jacketed, 215 mL 832HC31HZ Dip tube, 300 mL, PTFE coated, T316
2525HC Cylinder, Glass, 300 mL 832HC32 Dip tube, 450 mL, T316
2525HC2 Cylinder, Glass, 450 mL 832HC33 Dip tube, 600 mL, T316
2525HC3 Cylinder, Glass 600 mL 686HC19 Dip tube, 1000 mL, T316
686HC20 Dip tube, 1500 mL, T316
2630HC4 Cylinder, T316, 160 mL
686HC20HZ Dip tube, 1500 mL, PTFE coated, T316
2630HC14 Cylinder, T316 jacketed, 215 mL
2630HC Cylinder, T316, 300 mL
Male Connectors
A92HWAD Male connector, 1/4T x 1/8"NPT for dip
2630HC2 Cylinder, T316, 450 mL tube and cooling loop
2630HC3 Cylinder, T316, 600 mL A138CA Male connector, 1/4T x 1/8"NPT for
2630HC13 Cylinder, T316 jacketed, 600 mL thermowell
For 1000 mL - 1500 mL: Cooling Loop

2825HC Cylinder, Glass, 1000 mL 831HC6 Cooling loop, 300 mL, T316
2825HC11 Cylinder, Glass jacketed, 1000 mL 831HC6HZ Cooling loop, 300 mL, PTFE coated T316
2825HC2 Cylinder, Glass 1500 mL 831HC7 Cooling loop, 450 mL, T316
2825HC12 Cylinder, Glass jacketed, 1500 mL 831HC7HZ Cooling loop, 450 mL, PTFE coated T316
831HC8 Cooling loop, 600 mL, T316
2910HC3 Cylinder, T316, 1000 mL 831HC8HZ Cooling loop, 600 mL, PTFE coated T316
2910HC4 Cylinder, T316, 1500 mL 2930HC3 Cooling loop, 1000 mL, T316
2910HC14 Cylinder, T316 jacketed, 1500 mL 2930HC3HZ Cooling loop, 1000 mL, PTFE coated T316
2930HC4 Cooling loop, 1500 mL, T316
2930HC4HZ Cooling loop, 1500 mL, PTFE coated T316
Part No. Description Part No. Description
Stirrer Support Bracket 2028HC5 Gas Entrainment shaft, 300 mL, T316
A1260HC2 Stirrer bracket, 450 mL - 600 mL, for cool- 2028HC5HZ Gas Entrainment shaft, 300 mL, PTFE
ing loop, T316 coated T316
A1260HC5HZ Stirrer bracket, 450 mL - 600 mL, PTFE 2028HC6 Gas Entrainment shaft, 450 mL, T316
coated T316 2028HC6HZ Gas Entrainment shaft, 450 mL, PTFE
A1872HC Stirrer bracket, 450 mL - 600 mL, for coated T316
265HC style thermowell 2028HC7 Gas Entrainment shaft, 600 mL, T316
1261HC Bushing for stirrer bracket, 450 mL - 600 2028HC7HZ Gas Entrainment shaft, 600 mL, PTFE
mL, PTFE coated T316
2028HC8 Gas Entrainment shaft, 160 mL, T316
A1404HC2 Stirrer bracket, 1000 mL - 1500 mL, for
thermowell, T316
Stirrer Shaft and Impellers
A1404HC3HZ Stirrer bracket, 1000 mL - 1500 mL, PTFE
coated T316
For 1000 mL - 1500 mL:
299HC Bushing for stirrer bracket, 1000 mL - 1500
352HC9 Upper shaft, 1000 mL - 1500 mL, T316
mL, PTFE
A358HC5 Propeller, turbine, 1000 mL - 1500 mL,

Stirrer Shaft and Impellers T316
A358HC8 Propeller, turbine, 1000 mL - 1500 mL,
For 160 mL - 600 mL: PTFE coated T316
A837HC Propeller, turbine, T316
A837HC5HZ Propeller, turbine, PTFE coated T316 A2044HC Gas Entrainment shaft/impeller, 1000 mL,
T316
822HC33 Stirrer shaft, 160 mL, T316, 4.99” length A2044HCHZ Gas Entrainment shaft/impeller, 1000 mL,
822HC33HZ Stirrer shaft, 160 mL, PTFE coated T316, PTFE coated T316
4.99” length A2044HC3 Gas Entrainment shaft/impeller, 1500 mL,
822HC44 Stirrer shaft, 215 mL, T316, 5.69” length T316
822HC44HZ Stirrer shaft, 215 mL, PTFE coated T316, A2044HC3HZ Gas Entrainment shaft/impeller, 1500 mL,
5.69” length PTFE coated T316
822HC30 Stirrer shaft, 300 mL, T316, 6.92" length
822HC30HZ Stirrer shaft, 300 mL, PTFE coated T316, A449HC Lower shaft with coupling, 1000 mL, T316
6.92" length A449HCHZ Lower shaft with coupling, 1000 mL, PTFE
822HC31 Stirrer shaft, 450 mL, T316, 8.92” length coated T316
822HC31HZ Stirrer shaft, 450 mL, PTFE coated T316, A449HC22 Lower shaft with coupling, 1500 mL, T316
8.92” length A449HC22HZ Lower shaft with coupling, 1500 mL, PTFE
822HC32 Stirrer shaft, 600 mL, T316, 10.92” length coated T316
822HC32HZ Stirrer shaft, 600 mL, PTFE coated T316,
10.92” length
2070HC Gas Entrainment impeller, 300 mL - 600

mL, T316
2070HCHZ Gas Entrainment impeller, 300 mL - 600
mL, PTFE coated
2070HC2 Gas Entrainment impeller, 160 mL, T316
2070HC2HZ Gas Entrainment impeller, 160 mL, PTFE
coated T316
2027HC3 Gas Entrainment upper shaft, T316

www.parrinst.com 17
Thermowell and Thermocouple Gaskets and Seals

For 160 mL - 600 mL: For 160 mL - 600 mL:
A138CA Male connector, 1/4T x 1/8"NPT for 48HC Gasket for mag drive, Silver
thermowell 48HCFG Gasket for mag drive, Gold plated Silver
48HCKL Gasket for mag drive, Graphite
217VBAD Replacement nut for thermowell
218VBAD Replacement ferrule set for thermowell 2632HCJV Head seal O-ring, FKM
2632HCJK Head seal O-ring, FFKM
2943HCHZ Thermowell, 300 mL, PTFE coated T316, 2632HCJE Head seal O-ring, EP
6.86" length
2632HCJB Head seal O-ring, NBR
2943HC2HZ Thermowell, 450 mL, PTFE coated T316,
8.86" length
For 1000 mL - 1500 mL:
10.86" length 48HC Gasket for thermowell and mag drive,
Silver
4.73" length 48HCFG Gasket for thermowell and mag drive, Gold
plated Silver
5.43" length 48HCKL Gasket for thermowell and mag drive,
Graphite
A472E Thermocouple, type-J, 7 ½”, grounded

2913HCJV Head seal O-ring, FKM
A472E2 Thermocouple, type-J, 9 ½” , grounded
2913HCJK Head seal O-ring, FFKM
A472E3 Thermocouple, type-J, 11 ½”, grounded
2913HCJE Head seal O-ring, EP
A472E4 Thermocouple, type-J, 5 ½”, grounded
A490E Dual thermocouple, type-J, 7 ½”
For 1000 mL - 1500 mL:
A490E2 Dual thermocouple, type-J, 9 ½”
48HC Gasket for thermowell and mag drive,
A490E3 Dual thermocouple, type-J, 11 ½”
Silver
48HCFG Gasket for thermowell and mag drive, Gold
For 1000 mL - 1500 mL: plated Silver
48HC Gasket for thermowell, Silver 48HCKL Gasket for thermowell and mag drive,
48HCFG Gasket for thermowell, Gold plated Silver Graphite
265HC7 Thermowell, 1000 mL, T316 2913HCJV Head seal O-ring, FKM
265HC7HZ Thermowell, 1000 mL, PTFE coated T316 2913HCJK Head seal O-ring, FFKM
265HC27 Thermowell, 1500 mL, T316 2913HCJE Head seal O-ring, EP
265HC27HZ Thermowell, 1500 mL, PTFE coated T316
Split Ring
A472E2 Thermocouple, type-J, 1000 mL, grounded
A472E3 Thermocouple, type-J, 1500 mL, grounded For 160 mL - 600 mL:
A2526HC Split ring, glass and glass jacketed cylinder
A2735HC Split ring, metal cylinder
2524HC Spacer, Ultem, for A2526HC split ring

2524HCHA Spacer, PTFE, for A2526HC split ring

Heaters
For 1000 mL - 1500 mL:
A2916HC Split ring, glass cylinder For 160 mL - 600 mL:
A2912HC2 Split ring, metal cylinder A2230HCEB Electric heater, 300 mL metal or glass
cylinder, 115V
2914HC Spacer, Ultem, for A2916HC split ring A2230HCEE Electric heater, 300 mL metal or glass
2914HCHA Spacer, PTFE, for A2916HC split ring cylinder, 230V
A2230HC2EB Electric heater, 450 mL metal or glass
cylinder, 115V
Accessories A2230HC2EE Electric heater, 450 mL metal or glass
cylinder, 230V
424HC2 High temperature thread lubricant, 1oz A2230HC3EB Electric heater, 600 mL metal or glass
tube cylinder, 115V
A495HC Gas inlet hose assembly, 6-ft, 2500 psi, A2230HC3EE Electric heater, 600 mL metal or glass
Nylon cylinder, 230V
JP0025TB06 Neoprene tubing, 1/4"OD, for cooling
water
A2230HC4EB Electric heater, 160 mL metal cylinder,
TX31SK 5/16 socket screw key 115V
2925HC Lab Jack (for 1000 mL - 1500 mL glass A2230HC4EE Electric heater, 160 mL metal cylinder,
cylinders) 230V
A2230HC16EB Electric heater, 160 mL glass cylinder, 115V
A2995HC Hose assembly for circulator A2230HC16EE Electric heater, 160 mL glass cylinder, 230V
211VBAD Nut (part of A2995HC)
222VBAD Ferrule (part of A2995HC) For 1000 mL - 1500 mL:
297VBAD Union fitting (part of A2955HC) A2945HCEB Electric heater, 1000 mL metal cylinder,
2648HC Cap for hose end (part of A2995HC) 115V
2649HC Tube adapter (part of A2995HC) A2945HCEE Electric heater, 1000 mL metal cylinder,
230V
A2945HC2EB Electric heater, 1500 mL metal cylinder,
Magnetic Drive Parts (for A1120HC9 Drive) 115V
264AC4 Pin spanner wrench A2945HC2EE Electric heater, 1500 mL metal cylinder,
264AC5 Face spanner wrench 230V
1132HC Thrust washer, pk of 2
1133HC Bushings, pk of 3 A2944HCEB Electric heater, 1000 mL glass cylinder,
1137HCHA PTFE O-ring 115V
48HC Silver gasket A2944HCEE Electric heater, 1000 mL glass cylinder,
230V
1138HC Upper snap ring
A2944HC2EB Electric heater, 1500 mL glass cylinder,
1138HC2 Lower snap ring
115V
1139HC Ball bearings, pk of 2
A2944HC2EE Electric heater, 1500 mL glass cylinder,
2714HC Nipples for cooling sleeve 230V
827HC Cooling sleeve O-rings
1144HC Wave spring
See manual 234M for additional detail.
www.parrinst.com 19
Product Features and Part Identification
Stand for 1 - L and 1.5 L Vessels

Stand for 160 - 600 mL Vessels
www.parrinst.com 21
5100 LOW PRESSURE REACTORS
5100 Stand
2446HC Thumb Screw (2)
2656HC Belt Guard with

2655HC Overarm Plate
2667HC Vessel 2666HC Shield

Support Plate Top Plate
2657HC2 Encasement with

2658HC Lower Backplate 2206HC
and 2659HC Upper Vessel Retainer
Backplate
2665HC Latches (6) 2652HC2 Rear

Guard
2660HC
Support Rod (3)
A2651HC Base
2653HC2
Front Frame
Mini Stand (160 mL - 600 mL)
Note: Liter Stands (larger) can be converted to accept Mini Vessel Assemblies. Mini Stands
are for Mini Vessel Assemblies only.

5100 Overarm
857HC4 Driven Pulley A1001E6 Tach 1564HC Optical Wheel 1700 rpm
(Flip over when using 850 max rpm) Sensor Assembly 1564HC2 Optical Wheel 850 rpm
2663HC Hinge
A1120HC9
Magnetic Drive
2634HC Drive Adapter 847HC10 Drive Belt 1700 rpm 2661HC (1/8 HP Motor) Pulley 2 Stage
847HC9 Drive Belt 850 rpm 2662HC (1/4 HP Motor) 2 Stage
857HC7 (Air Motor)
Common for all 5100 Reactors
5100 Internals
Internals for 1 L & 1.5 L Glass Vessels
www.parrinst.com 23
Internals for 300 mL - 600 mL Glass Vessels

Internals for 160 mL - 215 mL Glass Vessels

www.parrinst.com 25
Internals for 160 mL - 215 mL Vessels

5100 Head Assembly
Head Assembly for 160 mL - 600 mL Vessels

www.parrinst.com 27
5110 Head Assembly
Head Assembly for 1 L & 1.5 Vessels

5120 Circulator (optional)
A2650HC 288VBAD
155VB Street Tee
Hose Assemblies (2) Male Connectors (2)
A472E4 Thermocouple A833HC Male Connector 504HCAA Adapter Reducer
www.parrinst.com 29
Parr Instrument Company
211 53rd Street
Moline, Illinois 61265 USA
Phone: 1-309-762-7716 or 1-800-872-7720
Fax: 1-309-762-9453
E-mail: [email protected]
http://www.parrinst.com
Revision 04/06/10

5100 - Operating Instruction Manuals

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Parr Instrument Company

Preface Related Instructions

1-309-762-7716 • 1-800-872-7720 • Fax: 1-309-762-9453

4 Parr Instrument Company

Current: The total current drawn should not exceed

Thermocouple: Unless otherwise specified, all

This CAUTION symbol may be present on the Product Instrumentation

This CAUTION symbol indicates that the surface may be hot.

Protective Earth (PE) terminal. Provided for connection of the Protective

Environmental Conditions Intended Usage

There are no user serviceable parts inside the product

Ensure that any hot surfaces have had

6 Parr Instrument Company

Installation Assemble the Reactor

8 Parr Instrument Company

This apparatus includes a safety shield Draining the Jacket

10 Parr Instrument Company

Identify the Valves Other Vessel Head

As a general rule, the liquid charge should not exceed

12 Parr Instrument Company

Accessories Mantle Heaters

Operation proof operation. Optional, intrinsically safe barriers are

If the local safety code requires that equipment installed

General Maintenance metal parts, but do not place a thermocouple

6. Do not use oil or anti-seize lubricant on threads or

7. If your vessel is equipped with a loose compression

8. Clean all threads and gas passages thoroughly and

Parts List Part No. Description

*Note: Special material internal parts (not T316) will

For 1000 mL - 1500 mL: Cooling Loop

A358HC5 Propeller, turbine, 1000 mL - 1500 mL,

2070HC Gas Entrainment impeller, 300 mL - 600

2027HC3 Gas Entrainment upper shaft, T316

Thermowell and Thermocouple Gaskets and Seals

A472E Thermocouple, type-J, 7 ½”, grounded

2524HC Spacer, Ultem, for A2526HC split ring

18 Parr Instrument Company

See manual 234M for additional detail.

20 Parr Instrument Company

Stand for 160 - 600 mL Vessels

2446HC Thumb Screw (2)

2656HC Belt Guard with

2667HC Vessel 2666HC Shield

2657HC2 Encasement with

2665HC Latches (6) 2652HC2 Rear

Mini Stand (160 mL - 600 mL)

22 Parr Instrument Company

Internals for 1 L & 1.5 L Glass Vessels

Internals for 300 mL - 600 mL Glass Vessels

Internals for 160 mL - 215 mL Glass Vessels

Internals for 160 mL - 215 mL Vessels

Head Assembly for 160 mL - 600 mL Vessels

Head Assembly for 1 L & 1.5 Vessels

A472E4 Thermocouple A833HC Male Connector 504HCAA Adapter Reducer

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