Failure Analysis For Dummies
Failure Analysis For Dummies
Failure Analysis For Dummies
It is developed into three mains sections, each one with a dedicated chapter:
• In the chapter 1, the basic concepts are presented. They are of wide use, independently for the considered
technology or application. It will be provided too a standard template for the failure analysis report.
• In the chapter 2, a more detailed example is provided of its application to a specific component technology: the
electromechanical micro relay. This electric component is of quite wide use. The analyzed samples specifically
come from TLC applications.
• In the chapter 3, it will be shown how the lessons learned from the failure analysis experiences could be used
to build up a set of criteria to proactively assess the production process of the part ‘s manufacturer, both to
supplier quality assurance and process control purposes.
Index
Chapter 1 - The Structure of a Failure Analysis
Chapter 2 - Example: The Electromechanical micro Relay
Chapter 3 - From Failure to Prevention
Chapter 4 - Glossary
Chapter 5 - Bibliography
2
Chapter 1
The Structure of a Failure Analysis
Failure Technological
Field Failure Root Cause Reporting
Confirmation Cause
3
Introduction
In the chapter 1, the basic concepts are presented. They are of wide use, independently for the considered
technology or application. It will be provided too a standard template for the failure analysis report.
Sketch 1:
Failure Analysis
Level 1 Level 2
Failure Technological
Field Failure Root Cause Reporting
Confirmation Cause
Chapter Index
i) Field Failure or the Level 1 Failure Analysis
ii) Lab Failure Confirmation or the Phase 1 of the Level 2 Failure Analysis
iii) Technological Analysis or the Phase 2 of the Level 2 Failure Analysis
iv) Root Cause Hypothesis or the Phase 3 of Level 2 Failure Analysis
v) Reporting of the Level 2 Failure Analysis
4
Field Failure
or the Level 1 Failure Analysis
General Guideline
A component is supposed failed “in field”, after a malfunctioning of a system or a failed manufacturing test for
some of its sub assembly.
The failure analysis that can be done “in field” is quite limited in capacity and generates some hypothesis about
the identity of the component/s supposed to be the cause of the system/ sub assembly failure.
The suspected component/s are more properly “probably failed”: that is the main output of this Level 1 of the
Failure Analysis.
Good Practices
• The majority of these components are analyzed in greater detail, initiating a Level 2 analysis, to have a
confirmation of the fail, in particular when they are discarded with an high frequency.
This can assure that the right cause of the “in field” system/ sub assembly failures are identified, possibly
addressing the right corrective or improvement action (manufacturer action, sub assembly redesign, test
review, etc.).
• Statistics about these probably failed components are maintained, with evidence of their correlation with main
test failed by the system/ sub assembly.
• When a component is submitted to a Level 2 Failure Analysis, it must be assured its handling is adequate (to
avoid to introduce new damages, for example during the dismounting of the component from the sub assembly
and during the transportation to the testing lab).
In addition, an adequate report must be prepared about the sample: how and when was made the hypothesis
of fail, regarding what sub assembly, what where the treatment of the component received before arriving to
the lab (for example: the system/ assembly was subject to reliability o stress test; how the component was
mounted/ dismounted from the sub assembly; etc.)
5
Failure Confirmation
or the Phase 1 of the Level 2 Failure Analysis
General Guideline
The probably failed component entering the Level 2 of a Failure Analysis, first of all is subject to functional tests to
have a confirmation about the failure.
These confirmation tests usually are electrical in nature and are focused to check the component compliance with
its specifications.
Each possible parameter/ performance non compliant with the specifications must be checked for coherence with
the declared system/ assembly failure. To this purpose could be needed the support of the system/ assembly
design engineers.
If the failure is confirmed, it’s strongly suggested to proceed with the Phase 2 of the Level 2 Failure Analysis: the
Technological Analysis (TA), to the purpose to identify the technological cause of the evidenced failure.
Good Practices
• The confirmation tests it’s opportune that are made following the applicable standards, to assure the alignment
with measure performed in different times, laboratories etc.
• All the measurement instruments (electrical, mechanical, etc.) must be done having assured their metrological
referring chain against golden samples, controlled by certified bodies to this purpose, and with adequate
frequency (usually specified by the applicable standards or by the instrument’s manufacturers).
• In case of custom components, or custom tests, the confirmation tests must be agreed with the supplier/
manufacturer. Off course, this agreement must be met before to initiate the component supply for the
customer production.
• In case of not confirmed failure for the analyzed components, it’s highly suggested to evaluate if proceed any
case to the Phase 2 (TA). As a matter of fact, some functional failure couldn’t be permanent, but the
technological signs still are detectable.
6
Technological Analysis
or the Phase 2 of the Level 2 Failure Analysis
General Guideline
To the purpose to execute a TA, a set of minimum requirements are applied:
i. less destructive analysis must be preferred. This is true for electrical tests too: too high energies could
destroy the technological evidences;
ii. At each step of the TA, apply with priority the applicable and pertinent not destructive tests;
iii. Assure to have a complete documentation for each step;
iv. In case of found anomaly, first of all verify its pertinence with the confirmed electrical failure before to
evaluate if proceed to another TA step.
v. The TA is terminated once the right technological defect is identified (a defect clearly correlated with the
functional confirmed failure).
Good Practices
• If the right technological defect is identified, the TA is terminated to assure the integrity of the remaining
component (in particular in case of joint assessments with component’s manufacturers or with our system/
assembly customers)
7
Notes on the General Guidelines
Minimum Notes
Requirement
i /ii – not The sample under analysis must be preserved as much as possible.
destructive tests Less destructive tests are those who release to it les energy, who require less dismounting of its parts.
• Less energy released: temperature around normal component operating temperature, lower I*V, limited
shocks, measurement repeated less it’s possible, testing time dynamic near the characteristic time of
the component technology, etc.
• Dismounting: at each TA step identify the test techniques that leave as is the component. For example
X-Ray inspection on closed packages instead of visual inspection of the interior; SEM without carbon
coating (for conductive samples) instead of coated,...
iii - documentation The TA must be implemented with great care, assuring a complete documentation of the component
status at each step of the analysis. The sample we have is unique. The documentation is all what will
remain after a step completion: remember that, from a certain point of the TA, the sample will be
inevitably and progressively dismounted if not destroyed.
General Guideline
Once identified the highly possible technological cause of the confirmed functional failure, it’s opportune to try to
identify the related root cause that generated the technological defect.
First of all, the root cause could be due to the manufacturer process or to the customer processes (component
assembling, handling, testing).
In addition, in case of root case attributed to the manufacturer, its knowledge could help to assess the adequacy
of the correction/ improvement actions that the manufacturer will propose/ present.
Last but not least, this knowledge will help to design a list of check points for the site visits performed during the
supplier qualification activity (see Chapter 3)
Good Practices
• See Chapter 3
9
Reporting
of the Level 2 Failure Analysis
General Guideline
Each Failure Analysis (FA) must be closed storing a Report, also if not distributed or if the FA target isn’t meet (in
particular in this case !).
The FA Report has a written and standard form (see an example below)
Good Practices
• The FA target is opportune it’s shared with the people requiring the analysis
• See below an example of the FA Report template:
11
Introduction
In the chapter 2, a more detailed example is provided for the failure analysis application to a specific component
technology: the electromechanical micro relay.
Why the relay? This electric component is of quite wide use. In addition, it’s a quite simple electric component,
easy to be provided and analyzed by a beginner in a self made home lab, with few tools, an optical stereo
microscope, some simply test circuit also for reliability test, possibly an oven.
The analyzed samples specifically come from TLC applications in a ten years of failure analysis activity in 80s/90s.
Chapter Index
The Table 1 (next page) anticipates the experimental relationships found during my activity between
technological defect and electrical failure modes. They have only qualitative value: they haven’t any statistical
validity being related to a limited number of cases (some hundreds of pieces analyzed, not all failed) against
tens of millions of pieces assembled on printed circuit boards (pcb) in the same period.
12
Table 1: Anticipation of the found correlations between defined technological defects and electrical failure modes.
It could happens that a defect with clear potential to generate electrical failure don’t appear correlated to
them in practice, due to effective manufacturers controls.
Contacts Springs Armature/Core Coil
Electrical failure (A) (D) (B) (C ) (E) (F) (G1) (G2) (H) (I) (J)
Erosion Cold Brown Insulating Melting Assembli Deformati Break Sticking Coating Wire
mode Sticking Powder Film Spots ng on Damage Break
No Switch X X X X X
Contact Resistance X X X X X
Dropout Voltage X X
Pickup Voltage X X X X
Pickup Time
Coil Resistance X
Bounce Time
Dielectric Strength
Insulation Resistance
Dropout Time
No Electrical Failure X X X X X
Contact erosion, in my experience could cause the below electrical failure modes:
• high contact resistance (bad contact quality);
• low dropout voltage (non – permanent sticking between normally open contacts);
• loosed switching (permanent sticking between normally open or closed contacts);
• high pick-up voltage (non – permanent sticking between normally closed contacts).
A. Inspection Methods
The erosion is visible by internal visual inspection (destructive analysis) through optical stereo microscope.
Sometimes (extreme cases) through X-ray inspection (non – destructive analysis) .
The phenomena could be confirmed detecting the materials of the second contact layer (base metals), mixed with
those of the precious metal layer, using the EDS/ SEM microanalysis.
B. Technological Causes
The detection of the two layers’ material mix means an electrical/ mechanical wear out.
This wear out is caused by the contacts’ inadequacy (thickness, kind o materials) to fulfil with the requirements of
the expected application (frequency, number, and energy of the switching).
14
Technological Defect:
A) Erosion of the contacts’ precious metal layer (2/3)
Photo 1, 2
C. The photos
Into the Photo 1 it’s clearly visible the contact’s erosion with a
material transport, from the moving contact (upper contact), on the
surface of fixed contact (bottom contact)
15
Technological Defect:
A) Erosion of the contacts’ precious metal layer (3/3)
Photo 3, 4
The resulting lack of material from the surface of the upper contact
(the movable contact) is shown into the Photo 3.
16
Technological Defect:
B) Brown Powder Between and Around the Contacts (1/3)
The presence of brown powder around the contacts, in my experience could generate the following electrical
failure mode:
• high contact resistance (due to the poor quality of contact resistance impaired by the moisture) .
Electrically the technological defect could be confirmed repeating a certain number of contact resistance
measurements and observing a trend of resistance value decreasing, due to the progressive mechanical cleaning
of the contacts (see Figure 1).
Warning: until black powder isn’t confirmed by internal visual inspection, it’s important to use low voltage
measurement technique to avoid to damage / destroy possible presence of contact surface insulating films (see
section C for details about this technological defect).
17
Technological Defect:
B) Brown Powder Between and Around the Contacts (2/3)
Photo 5
A. Inspection Methods
The brown powder is visible by internal visual inspection
(destructive analysis) through optical stereo microscope.
If the EDS/ SEM microanalysis on the contact surface is used, it
shows a relevant presence of carbon (C ) .
B. Technological Causes
Notwithstanding the degassing, due to the low quality of used
materials (organic molecules in particular), or some process
contaminants (finger traces for examples, or silicon, oil products),
the internal atmosphere could promote the brown powder
formation during the arching produced with high load switching
(breakdown arcs)
C. The photos
Photo 5 shows the presence of powder in the moving contact area:
• on the walls around;
• on the contacts;
• between them.
The EDS microanalysis of the brown powder shows presence of the
cupper (Cu) of the contact springs and carbon (C )
18
Technological Defect:
B) Brown Powder Between and Around the Contacts (3/3)
19
Technological Defect:
C) Insulating Film on the Contact Surface (1/2)
Electrically the technological defect could be confirmed repeating a certain number of contact resistance
measurements and observing that the resistance values are highly unstable, sometime till 100% change, resulting
in an average high resistance value (see Figure 2).
Warning: the only detection method is electrical (see below), it’s important to use low voltage measurement
technique to avoid to damage / destroy it.
A. Inspection Methods
These insulating films aren’t detectable using visual inspection
EDS/SEM analysis is typically is not applicable due to the very thin deposit
B. Technological Causes
The cause of insulating films on the contact surfaces is the internal parts plastic material degassing and its deposit
facilitated by relay operations without high load (the breakdown arching destroy these films)
C. Photo
No photo are available
20
Technological Defect:
C) Insulating Film on the Contact Surface (2/2)
Figure 2
21
Technological Defect:
D) Sticking Between Contacts’ Gold Surface Flash (1/4)
If present, the cold sticking is detected on new devices (less than 1000 switching).
As a consequence, a possible incoming test could be designed to test supplier materials:
• 20pieces every 100.000 or smaller lots:
• 0 defects allowed;
• Ultrasonic exposure (47 KHz,60W, isopropyl alcohol 25 cc glass breaker, temperature [30; 35]^C, 10 seconds
exposure);
• Electrical test of the pick up voltage (coil voltage manually applied: 0,03 V steps starting from 0 volts)
22
Technological Defect:
D) Sticking Between Contacts’ Gold Surface Flash (2/4)
A. Inspection Methods
The cold sticking is visible by internal visual inspection (destructive analysis) through optical stereo microscope.
It could be detected too by X-ray inspection.
Both cases applying step by step coil voltage. Using X-ray the sticking must be checked through electrical test of the
suspected contacts.
Using the EDS/ SEM microanalysis on the contact surface to confirm this defect, no contact erosion must result (no
base metal).
B. Technological Causes
The causes of cold sticking are mechanical shocks or vibrations. Relevant contacts’ technological parameters tu put
under control this phenomena are:
• surface hardness (higher it’s lower the sticking susceptibility);
• surface morphology (higher roughness, lower susceptibility);
• contact shape (flatness, lower the susceptibility);
• contact force (lower, lower susceptibility).
Some parameter has influence on contract resistance, stability and reliability. Unfortunately isn’t possible to obtain
both at the same time: good contact resistance (low, stable and reliable) and low cold sticking susceptibility
23
Technological Defect:
D) Sticking Between Contacts’ Gold Surface Flash (3/4)
Photo 6,7,8
C. The photos
Photo 6 shows a fixed contact with the presence of a cold sticking
area (left side)
24
Technological Defect:
D) Sticking Between Contacts’ Gold Surface Flash (4/4)
Photo 9, 10
C. The photos
A technique to avoid the cold sticking is to increase the roughness of
the contact surfaces.
25
Technological Defect:
E) Small Surface Melting Area (1/4)
It’s possible to reproduce small melting areas by the application of a capacitor discharge during the switching of
the contacts:
• at least 10- 12 V:
• peak time 3 µ seconds minimum;
• more than 20 discharges.
A. Inspection Methods
Possible small melting area is visible by internal visual inspection (destructive analysis) through optical stereo
microscope, but confirmed by SEM (morphologic analysis of the single melting spots) .
B. Technological Causes
The cause of small melting area on contact surface is the application of electrical discharges to burn possible
insulating films, due to the degassing of internal plastic parts after the relay package sealing. If the discharge
energy level is sufficiently low, it’s possible to burn the film without to deeply melt the surfaces (no base metal).
This “low cost” on-line process is concurrent with the more reliable and generally used off-line “backing “ process
(degassing of internal plastic parts, before or after the assembling, always before the packaging, at [120; 139]^C,
in controlled atmosphere, minimum 8 hours).
26
Technogical Defect:
E) Small Surface Melting Area (2/4)
Photo 11
C. The photos [follow]
Photo 11 shows the presence of an original small melting area on
each contact
27
Technogical Defect:
E) Small Surface Melting Area (3/4)
Photo 13, 14
C. The photos [continue]
Photo 13 shows another original melting spot. This is 10 µm only of
diameter.
[follow]
28
Technogical Defect:
E) Small Surface Melting Area (4/4)
Photo 15, 16
C. The photos [continue]
29
Technological Defect:
F) Contacts’ Assembling Mechanical Defects (1/3)
A. Inspection Methods
This kind of defects is generally visible by internal visual inspection through optical stereo microscope . In some
special case, the SEM could be needed
B. Technological Causes
Contacts’ assembling process not completely under control
30
Technogical Defect:
F) Contacts’ Assembling Mechanical Defects (2/3)
Photo 17, 18
C. The photos
Defective assembly phase: contact welding
[follow]
31
Technogical Defect:
F) Contacts’ Assembling Mechanical Defects (3/3)
Photo 19, 20
C. The photos [continue]
Defective assembly phase: contact punching
32
Technological Defect:
G) Contact Spring Mechanical Defects (1/6)
G1) Spring Deformation - it could generate the following electrical failure mode:
• high contact resistance (poor quality of contact caused by lower contact force).
G2) Spring fracture - it could generate the following electrical failure modes:
• loosed switching (air gap so high to avoid any electrical contact);
• high pick up voltage (higher air gap between fixed and movable normally open contacts );
• high contact resistance (poor quality of the contact caused by lower contact force);
• low drop out voltage (higher air gap between fixed and movable normally closed contacts) .
33
Technogical Defect:
G) Contact Spring Mechanical Defects (2/6)
G1) Spring Deformation
Photo 21
A. Inspection Methods
The spring deformation is visible by internal visual inspection
through the optical stereo microscope (sometimes by non
destructive X-ray inspection: see for example Photo 22).
B. Technological Causes
The cause of the spring deformation are a not adequate supplier’s
assembly process (handling during pins bending, case marking, etc.)
or the customer’s assembly process (mechanical shocks during
electrical test or part pick up and place): generally speaking, any
mechanical shock due to a not adequate handling. To this purpose,
some manufacturer suggest to avoid any shock equivalent to a
vertical fall of more than 0,3 meters.
In Photo 23 a very unusual case !
C. The photos
Photo 21 shows a clear air gap between two movable contacts, due
to their spring deformation.
[follow]
34
Technogical Defect:
F) Contacts’ Assembling Mechanical Defects (3/6)
G1) Spring Deformation
Photo 22
C. The photos [continue]
[follow]
35
Technogical Defect:
F) Contacts’ Assembling Mechanical Defects (4/6)
G1) Spring Deformation
C. The photos [continue] Photo 23
36
Technogical Defect:
G) Contact Spring Mechanical Defects (5/6)
G2) Spring Fracture
Photo 24, 25
A. Inspection Methods
The spring fracture visible is visible by internal visual inspection
through the optical stereo microscope (sometimes through X-ray
inspection: see Photo 25).
B. Technological Causes
The cause of the spring fracture is the mechanical wear (usually
after more than 1 million switches) or poor springs’ laser welding
process.
C. The photos
Photo 24 shows the detail of a spring fracture.
[follow]
37
Technogical Defect:
F) Contacts’ Assembling Mechanical Defects (6/6)
G2) Spring Fracture
Photo 26, 27
C. The photos [continue]
38
Technological Defect:
H) Armature and Core Sticking (1/1)
Impact of the technological defect on the electrical measurements
The presence of armature and core sticking, in my experience could electrical failure modes:
• loosed switching (sticking avoid that switching happens);
• high pick up time(1...5 seconds, when sticking force is lower than the magnetic force: initially there is a lock of
the armature movement and later the switching happens).
A. Inspection Methods
The armature and core sticking generally isn’t permanent and the electrical test could destroy it.
It could be confirmed through FTIR analysis of the contact area armature/ core surfaces.
B. Technological Causes
The defect is due to the activation at temperatures higher tan 50^C of the washing process residuals.
This washing compound is generally made of paraffin (used as lubricant for moulded parts or for coil wire during
winding), carboxylic acid salt (residual of the chemical nickel coating process or the armature and the core),
mechanical wear out residuals of the armature and core. There is evidence that this kind of compound generates
sticking also without paraffin.
Usual corrective actions are to avoid paraffin and to improve washing process, for example using ultrasonic
equipment for nickel plated parts.
C. Photos
No photos are available 39
Technological Defect:
I) Armature/ Core Coating Mechanical Damage (1/2)
A. Inspection Methods
The armature/core coating damage is visible by internal visual inspection through optical stereo microscope
It could be confirmed through EDS/ SEM microanalysis.
B. Technological Causes
The defect is due to the mechanical wear caused by the interference between armature and core.
It can generate an erosion of the plating or “smear” of the organic coating (parylen), used by the manufacturer.
The function of this coating is to avoid that the erosion residuals move free inside the relay impairing the
electrical characteristics.
40
Technological Defect:
I) Armature/ Core Coating Mechanical Damage (2/2)
Photo 28
C. The photos
Photo 28 shows one of the core poles of a relay that operated 2
millions of times. The picture shows two area (circled) with evidence
of the core coating damage. They are the contact points with the
moving armature (not showed in the picture).
41
Technological Defect:
J) Wire Coil Break (1/2)
A. Inspection Methods
The defect generally could be detected by internal visual inspection through optical stereo microscope.
It could be confirmed also by EDS/ SEM micro analysis, detecting the cloride (Cl) of the aggressive chemicals used
by the welding / washing processes.
B. Technological Causes
The defect is due mechanical stress during winding/ welding of the coil.
In alternative it could be caused by internal corrosion.
The aggressive chemicals could come from the residuals of the internal coil welding.
Or they are due to lack of package sealing, with possibility that the residuals come in from the washing process,
after the component mounting on the printed circuit board.
42
Technological Defect:
J) Wire Coil Break (2/2)
Photo 29, 30
C. The photos
43
Technological Defect:
K) Residuals from Laser Welding (1/1)
A. Inspection Methods
The defect generally could be detected by internal visual inspection through optical stereo microscope.
It could be confirmed also by the EDS/ SEM micro analysis of the laser welding residuals.
B. Technological Causes
The defect is due to the poor cleaning after the laser welding.
C. Photos
No photos are available
44
Technological Defect:
L) Environmental Pollution (1/2)
The presence of pollution from the manufacturing environment inside a relay, in my experience could generate
these electrical failure modes:
• loosed switching (no magnetic field is generated by the coil);
• high contact resistance;
• low drop out (due to pollution impairment of the armature movement);
• loosed switching (pollution between contacts that avoid electrical contact).
A. Inspection Methods
The defect generally could be detected by internal visual inspection through optical stereo microscope.
It could be confirmed also by EDS/ SEM micro analysis.
B. Technological Causes
The pollution is due to the poor cleaning of the relay’s manufacturing environment (here we are considering
environmental pollutants, different from welding residual, internal plastic parts degassing etc.)
45
Technological Defect:
L) Environmental Pollution (2/2)
Photo 29, 30
C. The photos
46
Technological Defect:
M) Magnet Assembling (1/1)
The presence of magnet assembling defects, in my experience could generate the electrical failure modes:
• loosed switching (magnet circuit defect which cause not sufficient magnetic field).
A. Inspection Methods
The defect generally could be detected by internal visual inspection through optical stereo microscope.
For example in case of lack of adhesion due to gluing defects, lack of mechanical stability due to moulding slot
defects)
B. Technological Causes
The defect is due to the poor manufacturing process or lack of incoming materials control-
C. Photos
No photo available
47
Technological Defect:
N) Fulcrum Wear (1/4)
A. Inspection Methods
The defect generally could be detected by internal visual inspection through optical stereo microscope.
B. Technological Causes
The defect is due to the not optimized design of the fulcrum, that for example aloud excess of friction during the
move due to wipe.
To reduce the friction, sometime a lubricant is used (generally teflon).
Other causes could be: fulcrum assembling, or mechanical wrong handling of the component (for example during
the relay assembling on the PCB).
48
Technological Defect:
N) Fulcrum Wear (2/4)
Photo 31, 32
C. The photos
Photo 31 shows the body block, the coil block and the magnet.
The circle area highlights two spots of residuals.
The relay switched 2 millions times.
[follow]
49
Technological Defect:
N) Fulcrum Wear (3/4)
Photo 33, 34
C. The photos [continue]
Photo 34 shows the armature block with the movable contacts, the
moulding that join them and how the moulding leave free the
fulcrum area .
The circle highlights the fulcrum area
[follow]
50
Technological Defect:
N) Fulcrum Wear (4/4)
Photo 35, 36
C. The photos [continue]
Photo 35 shows a detail of the fulcrum The arrows indicate the two
wear points corresponding to the deposits on the magnet (Photo 31
and 32).
Photo 36 shows a detail of the left point: the original round profile is
flattened and eroded due to the mechanical wear.
51
Technological Defect:
O) Internal Mouldings Defects (1/4)
O1) other Damages- The internal moulded parts could be damaged by many different processes during the relay
assembling. Below (O2 and O3) will be detailed the main moulding process defects (burrs and fractures). Here are
gathered all other causes. In my ten years experience it happened only one time, generating an electrical failure
mode:
• loosed switching (due to the armature lock).
A. Inspection Methods
The moulded part defects are visible by internal visual inspection through the optical stereo microscope.
52
Technogical Defect:
O) Internal Mouldings Defects (2/4)
O1) Other Damages
Photo #
B. Technological Causes
The only case of moulded parts defect different from burrs/
fractures that I experienced was due to bad soldering process of the
coil wire with consequent moulded parts thermal deformation till
the complete blocking of the armature move.
C. The photos
No available photos.
53
Technogical Defect:
O) Internal Mouldings Defects (3/4)
O2) Burrs
Photo 37, 38
B. Technological Causes
Burrs are due to poor moulding process control and can cause
electrical defects by mechanical interference with moving parts and
after some wear to generate residuals that can impair electrical
contacts (permanently or temporary).
C. The photos
Photo 37 shows the armature block with the movable part of
armature moulded with the movable springs.
Some burrs are evidently covering the fulcrum (white arrows).
54
Technogical Defect:
O) Internal Mouldings Defects (4/4)
O3) Fractures
Photo 39, 40
B. Technological Causes
Moulding fractures are due to poor moulding process control and
can cause electrical defects if not properly cleaned generating
residuals that can impair electrical contacts (permanently or
temporary).
C. The photos
Photo 39 shows a detail of the armature block near the fulcrum: the
white arrows indicate a fracture of the moulding.
55
Technological Defect:
P) Case Defects (1/4)
P1) Venting Hole Defects – The venting hole is case moulding injection point and the last access to the internal
of the relay before to be sealed. It’s also used to inject a neutral atmosphere (usually N2). A process not
completely under control could leave at it a hole.
P2) Other Moulding Defects - Usually they are located near the pins or the case bottom corners.
P3) Deformation - In my experience, for this kind of defect I have evidence of a correlation with electrical failure
only in case of deformation till case fracture.
Deformation could happen due a not correct soldering on PCB process (thermal shock that cause dilatation of the
internal N2 atmosphere without a proper cooling profile). If present on new pieces coming from the supplier, the
deformation could be due to a not correct sealing process. No photos are available.
A. Inspection Methods
The moulded part defects are visible by internal visual inspection through the optical stereo microscope.
The sealing defects (O1 and O2) are usually detected through the standard Gross Leak Test (bubble test).
56
Technogical Defect:
P) Case Defects (2/4)
P1) Venting Hole
Photo 41, 42
B. Technological Causes
Venting hole defects are due to poor moulding process. They are
controlled through the Gross Leak Test applied 100% to every
production batch.
C. The photos
Photo 41 shows a bottom of a relay. The arrows highlight the
venting hole that appears not sealed.
57
Technogical Defect:
P) Case Defects (3/4)
P2) Other Moulding Defects
Photo 45
B. Technological Causes
All the moulding defects are due to poor moulding process. They
are controlled through the Gross Leak Test applied 100% to every
production batch.
C. The photos
Photo 43 shows a bottom of a relay. The arrows highlight the sealing
defect at the case corner (white square)
[follow]
58
Technogical Defect:
P) Case Defects (4/4)
P2) Other Moulding Defects
Photo 45, 46
59
Technological Defect:
Q) Pin Cleaning (1/2)
The presence of pin cleaning defects, in my experience isn’t correlated with electrical failure.
A. Inspection Methods
The defect generally could be detected by internal visual inspection through optical stereo microscope.
The nature of the poor cleaning could be analyzed with SEM/EDS microanalysis.
B. Technological Causes
The defect is due to the poor manufacturing process (cleaning of finished parts, moulding process, etc.)
60
Technological Defect:
Q) Pin Cleaning (2/2)
Photo 47, 48
C. The photos
Photo 47 shows a bottom of a relay. The circle highlights one of the
not cleaned pins, in this case due to a poor moulding process.
61
Chapter 3
From Failure to Prevention
62
Introduction
In the chapter 3, it will be shown how the lessons learned from the failure analysis experiences could be used
to build up a set of criteria to proactively assess the production process of the part ‘s manufacturer, both to
supplier quality assurance and process control purposes.
With lower priority, will placed for site assessment the check points related to technological defects not
resulting to us correlated with confirmed functional failure (Table 2, lower rows).
63
Table 2
Contacts
Electrical (A) (D) (B) (C ) (E) (F)
Erosion Cold Sticking Brown Insulating Melting Assembling
failure mode Powder Film Spots
NO NA 1 Contact
"assembling"
YES (g1) Spring NA 2 (h) Washing * (j1) Coil (l) (k) Cleaning of (m) Magnet
Assembling process of wire Manufacturing Laser Welding assembing
the relay welding area general
parts * (j2) Coil cleaning
assembling
NO Interference
control
Armature/
Core
[follow]
64
NA 2: The root cause, in our experience, ies related to the wear out during component
functional aging (after 2 millions switches)
[continue]
Fulcrum Internal Mouldings Case Pins
Electrical (N) (O1) (O2) (O3) (P1) (P2) Other (P3) (Q)
Mechanical Other Burrs Fractures Venting Moulding Deformation Cleaning
failure mode Wear Damages Hole
Just for an example, the priority check points are placed into the theoretical simplified process flow of
the next page (Sketch 2)
65
Sketch 2: Theoretical simplified relay manufacturing process flow, with priority check points mapping (red labels,
see also Table 2)
l) on the overall manufacturing area
Contacts
Case top
cover b)
Venting
p3) p3) p3) Electrical Bubble p3) Relay p1) hole Degassing
Storage Packaging test test Marking closing + N2
66
Chapter 4
Glossary
67
1. Parts of a relay
The Sketch 3 shows the basic principles of the functioning of an electromechanical relay, like those
analyzed into Chapter 2. The coil is energized through the pins # 1, 10 (left).
When the coil is at rest, the movable spring is in the position shown into the sketch, and the left
movable/ fixed contact (pin #9) are closed. This is one of the two Normally Closed (NC) contacts. The
second, not showed into the sketch, is at pin #1.
The second contact of the spring, at pin #7, is open: this is one of the two Normally Open contacts. The
second is at pin # 4.
Sketch 3
68
When the coil is energized, it generate a magnetic field that attract the armature (not shown into the
Sketch 3: see Sketch 4). The armature is moulded with the spring of the movable contacts: its
movement, due to the energized coil, pulls the spring that, rotating around the fulcrum (pin# 8), open
the NC contact (pin #9) and close the NO contact (pin #7).
This movement and the related change of closed contact (from #9 to # 7) is the so called switching.
The voltage sufficient to terminate this contact change is the so called Pick up voltage.
The same, in parallel happens for the contacts at pins #2 and #4 (not showed into the sketch).
When the coil return at rest (applied voltage below the so called Drop out voltage), the armature is
released and it returns to its original at rest position, moving in the same way the spring of the movable
contacts. In this way the NO contact return to open status, and the NC contact to its original closed
status.
Movable Armature
Coil
Core
69
2. Electrical Parameters of a relay and their measurement methods
Pick up and Dropout voltage
The voltage applied to the coil has a triangular shape: profile named A into the Sketch 5.
The relay output voltage profile is named B into the same sketch.
The Pick up voltage is the voltage applied to the coil when the NO contact voltage appears permanently
closed.
The Drop out voltage is the voltage applied to the coil when the NC contact voltage appears to return
closed.
The step shown in the left of the B voltage profile is due to a relevant difference (0,3 ... 0,5 Volts)
between the voltage required to open the NC contact and the voltage needed to close the NO contact. A
relay with this characteristic is named “tri-state-rely”. This step, sometimes it’s also shown during the
decrease of the coil voltage.
Sketch 5
70
To perform these measurements, I used the circuit specified by the standard IEC 255/ 7 . Of course it’s required
the availability of an oscilloscope..
Some manufacturer prefers to apply a pulse wave to the coil (height equal to the maximum pick up and
minimum drop out voltage): this is fine for a “Go – No Go” (Pass/ Fail) test, but it’s not sufficient to perform the
component performance characterization during a failure analysis.
71
A test equipment without control, particularly on spikes lower than ground level, can cause serious
measurements misinterpretations and problems about test correlation with the manufacturer.
For example, spikes lower than the ground level, with very high voltage values (100... 200 volts), also if very
short in time (few µsec), cause measurement of Drop out Time lower about 1,5 ... 2 msec than the correct
value. To avoid the spikes I suggest to use a “fast diode” in parallel with the coil, or to use a pulse generator to
energize the coil.
Sketch 6
72
Contact Resistance
The contact resistance measurement is a “four points” measurement.
The most used methods are two: low voltage ac; 100 mA dc.
Low voltage method use instruments that assure (IEC 257/7) that voltage peak is minor than 20 mV. This
is the method to be used when there is the suspect of non conductive films formation between
contacts.
“Four points” measurement is done applying a dc test current fixed at 100 mA directly to the socket pins
of the relay.
With reference to the Sketch 3, whatever the methods used, the resistances are measured at the pins:
C1, C2, C3, C4.
Sketch 3
73
3. Instruments
EDS/SEM microanalysis
Energy Dispersive X-ray Spectrometry (EDS), or Energy
Dispersive X-ray Analysis (EDX) is an analytical method
that employ the X ray emissions of an electron excited
sample to identify the sample’s atomic species.
It’s very useful for solid samples.
Each atomic specie, once excited, return to a not-excited
state releasing photons of energies very specific for this
kind of atom. The on board SW of the EDS detector has a
data base of these energy emissions and in this way it
identify the kind of atoms on the surface of the sample.
For detail about the functioning of the SEM and SEM/ EDS,
see at Wikipedia.
FTIR
The Infrared (IR) Spectroscopy in Fourier Spectrum is an
analytical thecnique wide used to identify mainly organic
materials.
75
Bubble Test (Leak Test)
To have an idea how it could function a bubble test, see the
video at https://www.youtube.com/watch?v=ta53DwOJdhw
Please consider that, for failure analysis purposes, you don’t
have to add colorants to the test liquid.
In this case it’s opportune to have a lateral view of the
vessel containing the liquid and the sample to better identify
possible bubbles emerging from the component under test (sign
of a leaking and of its position on the component’s body).
In addition the liquid test can’t be water. It has to not corrosive
liquids.
The test could be done also without vacuum application (gross
Leak).
Oscilloscope
There are different kind of oscilloscope, from portable to highly sophisticated (their price is proportional to
their functional complexity and completeness). See at Wikipedia for details about its functioning.
76
Chapter 5
Bibliography
77
Chapter 2
1. “Physical Processes in Contact Erosion”, LH Germer, July 58, Journal of All.Ph., Vol 29, nr.7, pg. 1067
2. “Fundamental Processes of Fast Arc”, JL Smith, WS Boyle, March 59, BSTJ, pg 537
3. “Arching of Electrical Contacts in Telephone Switching Circuits”, MM Atolla, BSTJ, Parts I, II, III, IV, ,
September 57 pg 1231, November pg 1493, May 54 pg 535, January 55 pg 203
4. “Dynamic Model of Stationary Contacts Based on Random Variations of Surface Features”, RF Malucci, June
92, IEEE Trans. CHMT 15, nr 3, pg 339
5. The Formation of Insulating Silicon Compounds on Switching Contacts”, A Eskes, March 88, IEEE Trans.
CHMT 11, nr 1, pg 78
6. “A Reliability Study of Relay Suitable for Surface Mount Process Usinh High- Temperature– Resistant
Plastics”, M. Ohba, K. Kuzukawa, K Ozawa, March 88, IEEE Trans CHMT 11, nr 1, pg 85
7. “Organic Deposits on Precious Metal Contacts”, HW Hermance, May 58, BSTJ pg 739
8. “Wear and Contamination of Electroplated Gold Films in Line Contact”, Zhuan-ke Chen, May 92, IEEE Trans
CHMT 15, nr 3, pg 378
9. “Extraneous Metal Deposits from Production Processes on Contact Materials”, CHA Haque, July 54, BSTJ, pg
807
10. “Fundamental Relay technology”, Phoenix Contact Application Note 105396-en-00, 2012, at
https://www.phoenixcontact.com/assets/downloads_ed/global/web_dwl_technical_info/105396_en_00.pdf
Chapter 4
1. “Effect of Measurement Conditions on Low-level Contact Resistance”, J Muniesa, JY Mousson, March 84,
IEEE Trans CHMT 7, nr 1, pg 81
78
L’autore
Domenico Famà è HR Business Partner dal 2004 ed ha ricoperto questo ruolo in diverse aziende multinazionali, dopo aver cominciato a
lavorare nella funzione HR nel 2000. In precedenza ha svolto attività tecniche, dopo una laurea in Fisica all’Università di Pisa nel 1986.
Domenico è un utente appassionato di social networks, di cui cerca di esplorare le potenzialità, compatibilmente coi limiti di tempo di una
vita sola.
Appassionato dei temi del lavoro nelle organizzazioni e nella società, cerca di seguire affannosamente la sua evoluzione sempre più veloce.
In particolare dedicandosi ad alcune tematiche: etica ed innovazione della cultura manageriale; inclusione delle diversità e relazioni
interculturali; auto-orientamento nelle transizioni di vita-lavoro.
Con lo scopo di diffondere una cultura manageriale innovativa ed etica, supporta attivamente alcune associazioni no profit, ad esempio
l’European Foundation for Quality Management: www.efqm.org per cui svolge opera volontaria di Assessor per le aziende che desiderano
impegnarsi in un percorso per l’Eccellenza.
Sulle tematiche dell’inclusione delle differenze e delle relazioni interculturali, interviene volentieri ad incontri e seminari ed ha pubblicato,
con A.Cilona, il capitolo sulla gestione della Diversity (“Diversity: Prospettive e Criticità”) in “Persone, Organizzazioni e Lavoro”, Franco
Angeli 2009, curato dal Prof. A Cocozza della LUISS.
In tema di orientamento nelle transizioni di vita-carriera, per giovani in fase di inserimento nel mondo del lavoro o per profili più senior, ha
spesso collaborato in partnership con Fondazioni come quelle di Adecco o ATM, nell’ambito delle attività di Citizenship delle aziende in cui
lavora.
Coltiva (nel senso più proprio del termine) un sogno: avviare una attività di trasformazione agroalimentare, sviluppando un piccolo fondo di
proprietà seguendo criteri di sostenibilità (ambientale, sociale), di biodiversità (salvaguardia di specie native), di innovazione tecnologica
(micro agricoltura) e di accoglienza di eccellenza, dando corpo nel suo piccolo al detto “dalle stelle alle stalle” (dalla fisica all’agricoltura)
79