MenAMI Silica 03

AMI Silica
Version 6.20 and higher
Operator’s Manual
A-96.250.671 / 150517
Customer Support
SWAN and its representatives maintain a fully trained staff of technical specialists
around the world. For any technical question, contact your nearest
SWAN representative, or the manufacturer:
SWAN ANALYTISCHE INSTRUMENTE AG
Studbachstrasse 13
8340 Hinwil
Switzerland
Internet: www.swan.ch
E-mail: [email protected]
Document Status
Title: Monitor AMI Silica Operator’s Manual
ID: A-96.250.671
Revision Issue
00 Nov. 2011 First Edition
01 Nov.2013 Main board V2.4, Update to Firmware Release 5.40
02 Okt. 2014 Update to Firmware Release 5.41, description of

installation of option 2nd Sample Stream in chap. 3.
03 June 2016 Main board V2.5, Update to Firmware Release 6.00
© 2016, SWAN ANALYTISCHE INSTRUMENTE AG, Switzerland, all rights reserved
subject to change without notice

.
AMI Silica
Table of Contents
1. Safety Instructions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
1.1 Warning Notices . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
1.2 General Safety Regulations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
1.3 Restrictions for use . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
2. Product Description . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.1 Instrument Specification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
2.2 Instrument Overview. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
3. Installation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
3.1 Installation Check List. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
3.2 Mounting of Instrument Panel. . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
3.3 Install the Constant Head . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
3.4 Connect Sample and Waste . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
3.4.1 Sample Inlet . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
3.4.2 Sample Outlet . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
3.5 Install the 2nd Sample Stream Option . . . . . . . . . . . . . . . . . . . . . 21
3.6 Install the AMI Sample Sequencer . . . . . . . . . . . . . . . . . . . . . . . . 24
3.6.1 Sample connection with 2nd sample stream. . . . . . . . . . . . . . . 25
3.7 Electrical Connections . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26
3.7.1 Connection Diagram . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28
3.7.2 Power Supply . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
3.8 Relay Contacts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
3.8.1 Input . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
3.8.2 Alarm Relay. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
3.8.3 Relay 1 and 2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
3.9 Signal Outputs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
3.9.1 Signal output 1 and 2 (current outputs) . . . . . . . . . . . . . . . . . . . 33
3.10 Interface Options . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
3.10.1 Signal Output 3 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34
3.10.2 Profibus, Modbus Interface . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34
3.10.3 HART Interface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
3.10.4 USB Interface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
4. Instrument Setup . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36
4.1 Activate the Peristaltic pump . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36
4.2 Prepare reagents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36
4.3 Establish Sample Flow . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37
4.4 Programming . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38
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AMI Silica
5. Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39
5.1 Function of the Keys . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39
5.2 Measured Values and Symbols on the Display . . . . . . . . . . . . . . 40
5.3 Software Structure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42
5.4 Changing Parameters and Values . . . . . . . . . . . . . . . . . . . . . . . . 43
5.5 Grab Sample Measurement . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44
6. Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
6.1 Maintenance Schedule . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
6.2 Stop of Operation for Maintenance . . . . . . . . . . . . . . . . . . . . . . . . 45
6.3 Refill or replace Reagents. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
6.4 Verification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49
6.5 Calibration. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50
6.6 Cleaning the Flow Cell . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51
6.6.1 Disassemble the Constant Head . . . . . . . . . . . . . . . . . . . . . . . . 51
6.7 Cleaning the Photometer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
6.8 Cleaning the solenoid valve . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54
6.9 Tube Replacement . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 56
6.9.1 Replace the Pump Tubes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 56
6.9.2 Tube Numbering . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58
6.10 Fill or Flush Reagent System . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
6.11 Check Outputs and Relays . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
6.12 Replacing Fuses . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 60
6.13 Longer Stop of Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61
7. Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
7.1 Slope Error . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
7.2. Grab Sample. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 64
7.3. Error List . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65
8. Program Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69
8.1 Messages (Main Menu 1) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69
8.2 Diagnostics (Main Menu 2) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 70
8.3 Maintenance (Main Menu 3) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71
8.4 Operation (Main Menu 4) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72
8.5 Installation (Main Menu 5). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72
9. Program List and Explanations . . . . . . . . . . . . . . . . . . . . . . . . . 74
1 Messages. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74
2 Diagnostics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74
3 Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 76
4 Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 78
2 A-96.250.671 / 150517
AMI Silica
5 Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 79
10. Material Safety Data sheets . . . . . . . . . . . . . . . . . . . . . . . . . . . . 95
10.1. Reagents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 95
11. Default Values. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 96
12. Index . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 98
13. Notes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 100
A-96.250.671 / 150517 3
AMI Silica
Safety Instructions
AMI Silica - Operator’s Manual

This document describes the main steps for instrument setup, oper-
ation and maintenance.
1. Safety Instructions
General The instructions included in this section explain the potential risks
associated with instrument operation and provide important safety
practices designed to minimize these risks.
If you carefully follow the information contained in this section, you
can protect yourself from hazards and create a safer work environ-
ment.
More safety instructions are given throughout this manual, at the
respective locations where observation is most important. Strictly
follow all safety instructions in this publication.
Target Operator: Qualified person who uses the equipment for its intended
audience purpose.
Instrument operation requires thorough knowledge of applications,
instrument functions and software program as well as all applicable
safety rules and regulations.
OM Location Keep the AMI Operator’s Manual in proximity of the instrument.
Qualification, To be qualified for instrument installation and operation, you must:
Training  read and understand the instructions in this manual as well as
the Material Safety Data Sheets.
 know the relevant safety rules and regulations.
4 A-96.250.671 / 150517
AMI Silica
Safety Instructions
1.1 Warning Notices

The symbols used for safety-related notices have the following sig-
nificance:
DANGER
Your life or physical wellbeing are in serious danger if such

warnings are ignored.
 Follow the prevention instructions carefully.
WARNING
Severe injuries or damage to the equipment can occur if such

warnings are ignored.
CAUTION
Damage to the equipment, minor injury, malfunctions or incor-

rect process can be the consequence if such warnings are ig-
nored.
Mandatory The importance of the mandatory signs in this manual.

Signs
Safety goggles
Safety gloves
A-96.250.671 / 150517 5
AMI Silica
Safety Instructions
Warning Signs The importance of the warning signs in this manual.
Electrical shock hazard
Corrosive
Harmful to health
Flammable
Warning general
Attention general
6 A-96.250.671 / 150517
AMI Silica
Safety Instructions
1.2 General Safety Regulations

Legal The user is responsible for proper system operation.
Requirements All precautions must be followed to ensure safe operation
of the instrument.
Spare Parts Use only official SWAN spare parts and disposables. If other parts
and are used during the normal warranty period, the manufacturer’s
Disposables warranty is voided.
Modifications Modifications and instrument upgrades shall only be carried out by
an authorized Service Technician. SWAN will not accept responsi-
bility for any claim resulting from unauthorized modification or alter-
ation.
WARNING
Electrical Shock Hazard

If proper operation is no longer possible, the instrument must be
disconnected from all power lines, and measures must be taken
to prevent inadvertent operation.
 To prevent from electrical shock, always make sure that the
ground wire is connected.
 Service shall be performed by authorized personnel only.
 Whenever electronic service is required, disconnect instru-
ment power and power of devices connected to.
– relay 1,
– relay 2,
– alarm relay
WARNING
For safe instrument installation and operation you must read

and understand the instructions in this manual.
WARNING
Only SWAN trained and authorized personnel shall perform the

tasks described in this document.
A-96.250.671 / 150517 7
AMI Silica
Safety Instructions
1.3 Restrictions for use

The sample must not contain any particles, which may block the
flow cell. Sufficient sample flow is coercive for the correct function
of the instrument.
WARNING
For safe instrument installation and operation you must read
and understand the instructions in this manual, as well as the
Material Safety Data Sheets (MSDS)
 Reagent 1: Ammoniummolybdate consists of:
– Reagent 1a: Ammonium molydate Tetrahydrate
– Reagent 1b: Sodium hydroxide pellets
 Reagent 2: Sulfuric acid 25%
 Reagent 3: Oxalic acid
 Reagent 4: Ammonium Ferrous Sulfate consists of:
– Reagent 4a: Sulfuric acid 25%
– Reagent 4b: Ammonium iron (II) sulfate hexahydrate
 Silica Standard 100ppm 100ml
Download The current Material Safety Data Sheets (MSDS) for the above list-
MSDS ed Reagents are available for downloading at www.swan.ch.
8 A-96.250.671 / 150517
AMI Silica
Product Description
2. Product Description
Application The AMI Silica is a complete monitoring system for the automatic,
Range continuous measurement of the silica content in water of power
plants or demineralizer plants.
Silica The determination of silica is done by the photometric analysis of
Measurement molybdate blue at 810 nm.
Silica and ortho-phosphates react at low pH with ammonium mo-
lybdate to the yellow colored silico molybdic acid respectively phos-
pho molybdic acid. The phospho molybdic acid is destroyed with
oxalic acid before the silico molybdic acid is reduced with ammoni-
um iron(II) sulfate to the heteropoly-blue complex.
The required reagents are added in 3 steps to the sample in the pho-
tometer, where they allow a precise measurement of the silica con-
tent in the sample after the chemical reactions has been finished.
Grab Sample The measuring mode grab sample allows the measurement of
samples from remote locations.
Second If required the AMI Silica can be equipped with the optional second
Sample Stream sample stream module.
Sample If measurement of more than two sample streams is required, the
Sequencer AMI Silica can be connected to a Sample Sequencer which allows
to measure up to six sample streams.
Signal Two signal outputs programmable for measured values (freely scal-
Outputs able, linear or bilinear) or as continuous control output (control pa-
rameters programmable).
Current loop: 0/4–20 mA
Maximal burden: 510 
Third signal output available as an option. The third signal output
can be operated as a current source or as a current sink (selectable
via switch).
Relay Two potential-free contacts programmable as limit switches for
measuring values, controllers or timer for system cleaning with au-
tomatic hold function. Both contacts can be used as normally open
or normally closed.
Maximum load: 1 A / 250 VAC
Operating The AMI Silica can be operated in the following 3 different modes:
Modes  Internal
 External
 Fieldbus
Further information see Channel Selection, 5.1.6, p. 79.
A-96.250.671 / 150517 9
AMI Silica
Product Description
Alarm Relay One potential free contact.

Alternatively:
 Open during normal operation, closed on error and loss of
power.
 Closed during normal operation, open on error and loss of
power.
Summary alarm indication for programmable alarm values and in-
strument faults.
Input For potential-free contact to freeze the measuring value or to inter-
rupt control in automated installations (hold function or remote-off).
Safety No data loss after power failure. All data is saved in non-volatile
Features memory. Over voltage protection of in- and outputs. Galvanic sepa-
ration of measuring inputs and signal outputs.
Communica-  USB Interface for logger download
tion Interface  Third signal output (can be used in parallel to the USB interface)
(optional)  RS485 with Fieldbus protocol Modbus or Profibus DP
 HART interface
Fluidics The sample flows via the sample inlet [R] and the flow regulating
valve [Q] into the constant head [A]. Adjust the flow regulating valve
so that always a small part of the sample flows through the overflow
tube [B] into the waste [I]. This adjustment ensures a sufficient
sample flow through the measuring chamber of the photometer [F].
If no measurement takes place, the sample flows through the pho-
tometer outlet [E] where it will be aerated through air inlet [S] to
generate bubbles. Then the sample flows through the bubble
counter [H] into the waste [I].
If a measurement cycle starts, the solenoid valve [C] is activated
and the sample inlet [D] to the photometer is closed. The 6-way
valve [N] is automatically rotated to position 1 and a precisely de-
fined quantity reagent of the container [J] is pumped into the mea-
suring chamber by the peristaltic pump [O]. Immediately after that
the 6-way valve is rotated in position 2 and the reagent 2 from con-
tainer [K] is pumped into the photometer and mixed with the re-
agent 1 and the sample by the magnetic stirrer [G]. This procedure
is repeated with the 6-way valve in position 3 and reagent 3 [L] and
6-way valve in position 4 and reagent 4 [M].
After the measurement has been finished, the solenoid valve opens
and the measuring chamber is flushed.
Position 6 of the 6-way valve is not used.
10 A-96.250.671 / 150517
AMI Silica
Product Description
A
Level
S B
Q C
P
O
D
N 6
5 E
1 7
4 F
2 G
3
H
I
M
L
K
J
A Constant head K Reagent 2

B Overflow tube L Reagent 3
C Solenoid valve M Reagent 4
D Sample inlet photometer N 6-way valve
E Sample outlet O Peristaltic pump
F Photometer P Loop
G Magnetic stirrer Q Flow regulating valve
H Bubble counter R Sample inlet
I Waste S Air Inlet
J Reagent 1
A-96.250.671 / 150517 11
AMI Silica
Product Description
Measurement The quantities of the reagents are precisely defined by a certain

cycle number of rotations of the peristaltic pump. After the predefined
quantity of a reagent has been sucked from the container, the
6-way valve is rotated to position 5, where sample from the pho-
tometer is sucked into the loop [P]. With the sample in the tube the
reagents are pumped into the photometer.
The measurement of the sample is carried out as follows:
The sample flows via constant head through the photometer. If a
measuring cycle starts:
1 The sample inlet is closed by activation of the solenoid valve [C].

A zero measurement is performed.
2 6-way valve in position 1:
the reagent 1 is sucked from the container [J].
the reagent 2 is sucked from the container [K].
sample is sucked into the loop, the whole quantity of the re-
agents is pushed into the photometer.
5 The reagents are mixed with the magnetic stirrer, the first reac-
tion starts.
After 150 sec: 6 6-way valve in position 3:
the reagent 3 is sucked from the container [L].
agent is pushed into the photometer.
8 The reagents are mixed with the magnetic stirrer, the second re-
action starts.
After 90 sec: 9 6-way valve in position 4:
the reagent 4 is sucked from the container [M].
agent is pushed into the photometer.
11 The reagents are mixed with the magnetic stirrer, the third reac-
tion starts.
After 90 sec: 12 The sample measurement is performed.
13 The sample inlet is opened by deactivation of the solenoid
valve.
The measuring cell of the photometer is flushed.
12 A-96.250.671 / 150517
AMI Silica
Product Description

The reagent inlet tube is flushed with sample.
The peristaltic pump rotates for a certain time. The reagent
free sample in the photometer is sucked into the reagent
pipe and then via loop pumped back into the photometer.
A measuring cycle takes 10 minutes.

The diagram below shows the process of a measuring cycle in the
time axis.
1
2 150 sec
Y 3 90 sec
4 90 sec
5
6 X
1 2 3 4 5 6 7 8 9 10 11 12 13 14
7.5 min 2.5 min
X Measuring steps on time axis Reagent 2

Y 6-way valve position Reagent 3
Solenoid valve closed Reagent 4
Solenoid valve open Loop
Zero point measurement Reaction time
Sample measurement Flush loop
Reagent 1
A-96.250.671 / 150517 13
AMI Silica
Product Description
2.1 Instrument Specification
Power Supply Voltage: 100–240 VAC (± 10%)

50/60 Hz (± 5%)
or 24 VDC (± 10%)
Power consumption: max. 30 VA
Electronics Aluminium with a protection degree of IP 66 / NEMA 4X
housing Ambient temperature: -10 to +50 °C
Limit range of operation: -25 to +65 °C
Storage and transport: -30 to +85 °C
Humidity: 10–90% rel., non condensing
Display: backlit LCD, 75 x 45 mm
Sample Flow rate: min. 10 l/h
requirements Sample pressure inlet: 0.15–2 bar (2–28 PSI)
Temperature: up to 50 °C (122 °F)
NOTICE: No oil, no grease, no sand.
Silica Measuring method: colorimetric, molybdosilicat method

measurement Measuring range: 1 to 5’000 ppb
Reproducibility: ± 1 ppb or ± 5% whichever is greater
Max. PO4 concentration: < 10 ppm
On-site The analyzer site must permit connections to:
requirements Sample inlet: Tube 4 x 6 mm
1 Drain: Tube 15 x 20 mm
(1/2”) hose nozzle which must end in
pressure free waste of sufficient capacity.
14 A-96.250.671 / 150517
AMI Silica
Product Description
Dimensions Panel: 400 x 850 x 160 mm

Distance between mounting holes: 374 x 824 mm
Screw diameter: 8 mm
Weight: 16.0 kg
400 mm / 15¾”
13 mm / ½”
374 mm / 14¾”
13 mm / ½”
AMI Silica
824 mm / 32 7/16”
850 mm / 33½”
4 x dia. 10 mm / 3/8”
A-96.250.671 / 150517 15
AMI Silica
Product Description
2.2 Instrument Overview
A
J
K
L
B M
C
N
D
O
E
F
G
H P
I
A Transmitter K Flow regulating valve

B Panel L Solenoid valve
C 6-way valve control box M Sample inlet with sample
D 6-way valve switch (2nd sample stream
E Peristaltic pump option)
F Reagent 1 N Photometer with magnetic
G Reagent 2 stirrer
H Reagent 3 O Bubble counter
I Reagent 4 P Waste
J Constant head
16 A-96.250.671 / 150517
AMI Silica
Installation
3. Installation
3.1 Installation Check List
Check Instrument’s specification must conform to the National Electri-

cal Code, all state and local codes, and all plant codes and stan-
dards for electrical equipment.
On-site  100 - 240 VAC ( 10%), 50/60 Hz ( 5%) or 24 DC ( 10%),

requirements isolated power outlet with ground connection and 30 VA.
Sample line with min. 10 l/h and 0.15 - 2 bar.
Waste line with atmospheric drain.
Installation  Mounting of Instrument Panel, p. 18

Install the Constant Head, p. 19
Connect Sample and Waste, p. 20
Electrical Wir- NOTICE: Do not switch on the Instrument until all electrical
ing connections are made.
 Connect all external devices like limit switches, current loops
and pumps.
 Install the 2nd Sample Stream Option, p. 21 (if available)
 Install the AMI Sample Sequencer, p. 24 (if available)
 Connect the power cord, see Power Supply, p. 29
Reagents  Prepare the reagents. Refill or replace Reagents, p. 46

 Insert suction lances, see Instrument Setup, p. 36
Power-up Perform exactly in this order:

 Activate the Peristaltic pump, p. 36.
 Prepare reagents, p. 36.
 Establish Sample Flow, p. 37.
 Switch on power.
Instrument Program all parameters for external devices (interface, record-

Setup ers, etc.). Program all parameters for instrument operation (lim-
its, alarms, measuring interval).
Run-in period Let the instrument run continuously for 1 h.
A-96.250.671 / 150517 17
AMI Silica
Installation
3.2 Mounting of Instrument Panel

The first part of this chapter describes the preparing and placing of
the system for use.
 The instrument must only be installed by trained personnel.
 Mount the instrument in vertical position.
 For ease of operation mount it so that the display is at eye
level.
 For the installation a kit containing the following installation
material is available:
– 4 Screws 8x70 mm
– 4 Dowels
– 4 Washers 8.4/24 mm
Mounting re- The instrument is only intended for indoor installation.
quirements For dimensions see Dimensions, p. 15
18 A-96.250.671 / 150517
AMI Silica
Installation
3.3 Install the Constant Head

A A Constant head cover
B Constant head tube
C Overflow tube
D O-Ring
B E Flow cell block
F Flow regulating valve
Level G Solenoid valve
E
F
1 Push the overflow tube [C] through the flow cell block [E] as far
as it ends the waste funnel.
2 Fit the constant head tube [B] into the flow cell block [E].
3 Put the constant head cover [A] onto the constant head tube.
4 Adjust the overflow tube [C] so that it is at the lower level mark.
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AMI Silica
Installation
3.4 Connect Sample and Waste
3.4.1 Sample Inlet

Use plastic tube (FEP, PA, or PE 4 x 6 mm) to connect the sample
line.
Mounting of A Screw connection
A
SERTO fitting B Compression ferrule
B C Knurled nut
D Flexible tube
C
3.4.2 Sample Outlet
A Tube from constant head

A B Tube from photometer
B C Waste funnel
D Hose nozzle
C E 1/2” tube
D
E
Connect the 1/2” tube [E] to the hose nozzle [D] and place it into a
pressure free drain with sufficient capacity.
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AMI Silica
Installation
3.5 Install the 2nd Sample Stream Option

A
B
C
D
E
F
X Level
G
N
Exit Enter
M
AMI SILICA
SiO2 Process Analyzer A
D
L
K
J
I
A Block housing I Sample stream 1

B Connecting piece J Sample stream 2
C 2 O-rings K Waste (15x20 mm)
D Blind Plug L Fixing screws
E Flow regulating valve M Solenoid valve
F Flow cell block N Sample inlet tube
G Sample inlet (Elbow union) X Detail view
H Solenoid valve cable
1 Stop operation according to Stop of Operation for Maintenance,

p. 45.
2 Close the main sample tap.
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AMI Silica
Installation
3 Unscrew and remove the flow regulating valve [E] from the flow
cell block [F].
4 Screw the blind plug [D] into the flow cell block.
5 Remove the sample inlet tube [N] from the sample inlet (elbow
union) [G].
6 Remove the elbow union from the flow cell block.
7 Put one of the O-rings [C] into the bore of the block housing [A]
and the other one into the bore of the flow cell block [F].
8 Insert the connecting piece [B] into the bore of the flow cell
block.
9 Slide the block housing [A] over the connecting piece and press
it against the flow cell block [F] while screwing the block hous-
ing with the 2 fixing screws [L] onto the panel.
10 Push a 15 x 20 mm tube [K] (not included in the installation set)
over the ½” hose nozzle of the block housing and put the end of
the tube into a pressure free drain.
11 Connect the sample stream 1 [I] and the sample stream 2 [J] to
the corresponding sample inlets of the block housing according
to section Sample Inlet, p. 20.
Connect the
solenoid valve
WARNING
Electrical shock hazard!
Before opening the AMI Transmitter switch power off.
Use one of the PG7 cable glands to feed the cable of the solenoid
valve into the AMI transmitter housing.
22 A-96.250.671 / 150517
AMI Silica
Installation
A B
1 Remove the plug [A] from the cable gland [B].

2 Open the transmitter housing.
3 Feed the cable of the solenoid valve through the cable gland [B]
into the AMI transmitter housing.
4 Connect the wires to the terminals in the AMI transmitter
according to the Connection Diagram, p. 28.
5 Close the transmitter housing and start the Instrument.
Firmware After the 2nd sample stream option is installed and connected, set
settings 2nd the firmware according to your requirements.
sample stream 1 Navigate to menu <Installation>/
Sensors 5.1.5 <Sensors>.
Ref.Verification 0.235
Standard 100 ppb 2 Navigate to <Channels> with
Blank 0.0 ppb the[ ] or[ ] key.
Meas. interval 10 Min 3 Press [Enter].
Channels 1
4 Set <Channels> to 2 with the
Sensors 5.1.5 [ ] key.
Ref.Verifikation
Save?0.235
Standard Yes 100 ppb 5 Confirm with [Enter].
Blank No 0.0 ppb 6 Press [Exit], choose <Save> “Yes”
Meas. interval 10 Min Confirm with [Enter].
Channels 2
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AMI Silica
Installation
With 2nd sample stream option the AMI Silica can be operated in
the following 3 different modes.
 internal
 fieldbus
 external
1 Navigate to menu <Installation>/
Sensors 5.1.6
Channel Selection <Sensors>.
Standard 100 ppb
Blank internal 0.0 ppb 2 Navigate to <Channel Selection>
fieldbus
Meas. interval
external 10 Min
with the [ ] or[ ] key.
Channels 2
3 Press [Enter].
Channel Selection Intern
Internal The switch over between the two sample streams is controlled by the
AMI Transmitter according to the programmed measuring interval.
Fieldbus The switch over between the two sample streams is controlled by
Profibus or Modbus.
External The switch over between the two sample streams is controlled via
an external device connected to the input.
3.6 Install the AMI Sample Sequencer

For the measurement of more than 2 sample streams, an AMI
Sample Sequencer which allows the measurement of up to 6 sam-
ple streams, can be connected to the AMI Silica.
The installation and the electrical connection of the AMI Sample
Sequencer to the AMI Silica is described in the manual of the
AMI Sample Sequencer.
Firmware After the AMI Sample Sequencer is installed and connected, set
settings the firmware according to your requirements.
AMI Sample 1 Navigate to menu <Installation/
Sequencer Sensors 5.1.5
Sensors>.
Ref.Verification 0.235
Standard 100 ppb 2 Navigate to <Channels> with
Blank 0.0 ppb the[ ] or[ ] key.
Meas. interval 15 Min
3 Press [Enter].
Channels 1
4 Set <Channels> according to the
Sensors 5.1.5 number of available channels
Ref.Verifikation
Save?0.235 (1–6) with the [ ] key.
Standard Yes 100 ppb
Blank 0.0 ppb
5 Confirm with [Enter].
No
Meas. interval 10 Min 6 Press [Exit], choose <Save> “Yes”
Channels 6 Confirm with [Enter].
24 A-96.250.671 / 150517
AMI Silica
Installation
With the AMI Sample Sequencer connected, the

AMI Silica can be operated in the following 3 different modes.
 internal
 fieldbus
 external
1 Navigate to menu <Installation/
Sensors 5.1.6 Sensors>.
Channel Selection
Standard 100 ppb
Blank internal 0.0 ppb 2 Navigate to <Channel Selection>
fieldbus with the [ ] or[ ] key.
Meas. interval
external 15 Min
Channels 2 3 Press [Enter].
Channel Selection Intern
Internal, see chap. 9, Mode Internal, p. 79

Fieldbus, see chap. 9, Mode Fieldbus, p. 80
External, see chap. 9, Mode External, p. 80
3.6.1 Sample connection with 2nd sample stream

If a Sample Sequencer is connected to an AMI Silica with a second
sample stream option [A], the sample inlet 2 will be automatically
switched off and only the sample inlet 1 is active.
Connect the sample outlet of the Sample Sequencer to the sample
inlet 1 [E] of the option second sample stream.
A Option second sample
stream
B Blind plug
C Flow regulating valve 1
D Flow regulating valve 2
A E From Sample Sequencer
F Sample inlet inactive
B
C
D
2 1
E
F
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AMI Silica
Installation
3.7 Electrical Connections
WARNING
Risk of electrical shock.

Do not perform any work on electrical components if the trans-
mitter is switched on. Failure to follow safety instructions could
result in serious injury or death.
 Always turn off AC power before manipulating electric parts.
 Grounding requirements: Only operate the instrument from
an power outlet which has a ground connection.
 Make sure the power specification of the instrument corre-
sponds to the power on site.
Cable In order to comply with IP66, use the following cable thicknesses
thicknesses
A B C
A PG 11 cable gland: cable Øouter 5–10 mm

B PG 7 cable gland: cable Øouter 3–6.5 mm
C PG 9 cable gland: cable Øouter 4–8 mm
NOTICE: Protect unused cable glands

Wire  For Power and Relays: Use max. 1.5 mm2 / AWG 14
stranded wire with end sleeves.
 For Signal Outputs and Input: Use 0.25 mm2 / AWG 23
stranded wire with end sleeves.
26 A-96.250.671 / 150517
AMI Silica
Installation
WARNING
External Voltage.
External supplied devices connected to relay 1 or 2 or to the
alarm relay can cause electrical shocks
 Make sure that the devices connected to the following con-
tacts are disconnected from the power before resuming in-
stallation.
– relay 1
– relay 2
– alarm relay
WARNING
To prevent from electrical shock, do not connect the instrument

to the power unless the ground wire (PE) is connected.
 Do not connect unless specifically instructed to do so.
WARNING
The mains of the AMI Transmitter must be secured by a main

switch and appropriate fuse or circuit breaker.
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AMI Silica
Installation
3.7.1 Connection Diagram
CAUTION
Use only the terminals shown in this diagram, and only for the
mentioned purpose. Use of any other terminals will cause short
circuits with possible corresponding consequences to material
and personnel.
28 A-96.250.671 / 150517
AMI Silica
Installation
3.7.2 Power Supply
WARNING
Risk of electrical shock

Do not perform any work on electrical components if the trans-
mitter is switched on. Failure to follow safety instructions could
result in serious injury or death.
 Always turn off AC power before manipulating electric parts.
 Installation and maintenance of electrical parts must be per-
formed by professionals.
A
B
C
A Power supply connector

B Neutral conductor, Terminal 2
C Phase conductor, Terminal 1
D Protective earth PE
NOTICE: The protective earth wire (Ground) has to be

connected to the grounding terminal.
Installation The installation must meet the following requirements.
requirements  Mains fuse 1.6 AT
 Mains cable to comply with standards IEC 60227 or IEC
60245; flammable rating FV1
 Mains equipped with an external switch or circuit-breaker
– near the instrument
– easily accessible to the operator
– marked as interrupter for AMI Silica
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AMI Silica
Installation
3.8 Relay Contacts
3.8.1 Input
NOTICE: Use only potential-free (dry) contacts.
The total resistance (sum of cable resistance and resistance of
the relay contact) must be less than 50 Ω.
Terminals 16/42
If signal output is set to hold, measurement is interrupted if input is
active.
For programming see menu 5.3.4, p. 91
Programming of the relay contacts see 5.3 Relay Contacts, p. 85
3.8.2 Alarm Relay

NOTICE: Max. load 1 A (time-lag) / 250 VAC
Alarm output for system errors.
Error codes see Troubleshooting, p. 62

Programming see menu 5.3.1, p. 85
NOTICE: With certain alarms and certain settings of the AMI

transmitter the alarm relay does not switch. The error, however,
is shown on the display.
Terminals Description Relay connection

NC1) 10/11 Active (opened) during normal 1) 11
Normally operation.
0V
Closed Inactive (closed) on error and 10
loss of power.
12
NO 12/11 Active (closed) during normal 11

Normally operation. 0V
Open Inactive (opened) on error and 10
loss of power.
12
1) usual use
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Installation
3.8.3 Relay 1 and 2

NOTICE: Max. load 1 A/250 VAC
Relay 1 and 2 can be configured as normally open or as normally
closed. Standard for both relays is normally open. To configure a
Relay as normally closed, set the jumper in the upper position.
NOTICE: Some error codes and the instrument status may
influence the status of the relays described below.
Relay Jumper
config. Terminals pos. Description Relay configuration
Normally 6/7: Relay 1 Inactive (opened) during
Open 8/9: Relay 2 normal operation and 6
loss of power.
Active (closed) when a 0V
programmed function is 7
executed.
Normally 6/7: Relay 1 Inactive (closed) during
Closed 8/9: Relay 2 normal operation and 6
loss of power.
Active (opened) when a 0V
programmed function is 7
executed.
A
B
A Jumper set as normally open (standard setting)

B Jumper set as normally closed
For programming see Menu Installation 5.3.2 and 5.3.3, p. 87
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AMI Silica
Installation
CAUTION
Risk of damage of the relays in the AMI Transmitter due to

heavy inductive load.
Heavy inductive or directly controlled loads (solenoid valves,
dosing pumps) may destroy the relay contacts.
 To switch inductive loads > 0.1 A use an AMI relay box avail-
able as an option or suitable external power relays.
Inductive load Small inductive loads (max 0.1A) as for example the coil of a power
relay can be switched directly. To avoid noise voltage in the
AMI Transmitter it is mandatory to connect a snubber circuit in par-
allel to the load.
A snubber circuit is not necessary if an AMI relaybox is used.
A A AC or DC power supply
B C B AMI Transmitter
C External power relay
D E D Snubber
E Power relay coil
Resistive load Resistive loads (max. 1A) and control signals for PLC, impulse
pumps and so on can be connected without further measures
A B A AMI Transmitter
B PLC or controlled pulse pump
C C Logic
Actuators Actuators, like motor valves, are using both relays: One relay con-
tact is used for opening, the other for closing the valve, i.e. with the
2 relay contacts available, only one motor valve can be controlled.
Motors with loads bigger than 0.1A must be controlled via external
power relays or an AMI relay box.
A A AC or DC power supply
B C B AMI Transmitter
C Actuator
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Installation
3.9 Signal Outputs
3.9.1 Signal output 1 and 2 (current outputs)

NOTICE: Max. burden 510 .
If signals are sent to two different receivers, use signal isolator
(loop isolator).
Signal output 1: Terminals 14 (+) and 13 (-)
Signal output 2: Terminals 15 (+) and 13 (-)
Programming see menu 5.2 Signal Outputs, p. 81
3.10 Interface Options

A AMI Transmitter
A B Slot for interfaces
C Screw terminals
The slot for interfaces can be used to expand the functionality of

the AMI instrument with either:
 an additional signal output
 a Profbus or Modbus connection
 a HART connection
 an USB Interface
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AMI Silica
Installation
3.10.1 Signal Output 3

Terminal 38 (+) and 37 (-).
Requires the additional board for the third signal output 0/4–20 mA.
The third signal output can be operated as a current source or as a
current sink (switchable via switch [A]). For detailed information see
the corresponding installation instruction.
NOTICE: Max. burden 510 .
A
Third signal output 0/4–20 mA PCB
A Operating mode selector switch
3.10.2 Profibus, Modbus Interface

Terminal 37 PB, Terminal 38 PA
To connect several instruments by means of a network or to config-
ure a PROFIBUS DP or a MODBUS connection, consult the PRO-
FIBUS/MODBUS manual. Use appropriate network cable.
NOTICE: The switch must be ON, if only one instrument is
installed, or on the last instrument in the bus.
OFF
ON
Profibus, Modbus Interface PCB (RS 485)

A On - OFF switch
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Installation
3.10.3 HART Interface

Terminals 38 (+) and 37 (-).
The HART interface PCB allows for communication via the HART
protocol. For detailed information, consult the HART manual.
HART Interface PCB
3.10.4 USB Interface

The USB Interface is used to store Logger data and for Firmware
upload. For detailed information see the corresponding installation
instruction.
The optional third signal output 0/4 – 20 mA PCB [B] can be
plugged onto the USB interface and used in parallel.
USB Interface
A USB Interface PCB
B Third signal output 0/4 - 20 mA PCB
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AMI Silica
Instrument Setup
4. Instrument Setup
4.1 Activate the Peristaltic pump

The occlusion frames of the peristaltic pump are opened during
transport and storage. This prevents the pump tubs from sticking
together at the pressure points.
1 Turn the occlusion frame [B] clockwise to activate the peristaltic

pump.
 The peristaltic pump is ready.
A Turn clockwise to
A activate
B Occlusion frame
B C Rotor
D Pump tube
C
D
4.2 Prepare reagents

See Refill or replace Reagents, p. 46
1 Insert the suction lances into the containers.

 Make sure that the numbers on the suction lances
correspond to the numbers on the containers.
36 A-96.250.671 / 150517
AMI Silica
Instrument Setup
4.3 Establish Sample Flow
CAUTION
Pollution of the reagents

If the occlusion frames are not closed, sample may flow into the
reagents.
 Lock the occlusion frames before establishing the sample
flow.
A Overflow tube
B Flow regulating valve
Level
1 Open the flow regulating valve [B]

2 Adjust the flow regulating valve so that a large part of the sam-
ple flows through the overflow tube [A] into the waste.
3 Switch on power.
4 Start <Fill system>, see Fill or Flush Reagent System, p. 59.
5 Check tube connections and flow cell for leaks and repair if nec-
essary.
6 Let the instrument run-in for one hour.
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AMI Silica
Instrument Setup
4.4 Programming
Programming Program all parameters for external devices (interface, recorders,
etc.) Program all parameters for instrument operation (limits,
alarms). See Program Overview, p. 69 and for explanations, see
Program List and Explanations, p. 74
Configuring Input:
NOTICE: use “hold” to interrupt measurement.

Signal The Signal Outputs 1, 2 and (optional) 3 can be used as
Outputs  process value
 continuous control.
Used as process values for:

 Temperature
 Sample flow
 Silica 1
Operating Set the operating mode according your requirements to:

Modes  Internal
 External
 Fieldbus
Further information see Channel Selection, 5.1.6, p. 79.
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AMI Silica
Operation
5. Operation
5.1 Function of the Keys
A B C D
Exit Enter
A to exit a menu or command (rejecting any changes)

to move back to the previous menu level
B to move DOWN in a menu list and to decrease digits
C to move UP in a menu list and to increase digits
to scroll the measuring values if a Sample Sequencer is
connected
D to open a selected sub-menu
to accept an entry
Program
RUN 14:10:45 Main Menu 1
Access, Exit Enter
R1 Messages
Diagnostics
R2 0.42 ppb Maintenance
Exit Operation
25.4°C 32 B/s Installation
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AMI Silica
Operation
5.2 Measured Values and Symbols on the Display

Display when
A B C D E
Operating with
one Sample
Stream
RUN 15:20:18
R1 15:10:52
F
R2 0.0 ppb
I 24.2°C 31 B/s
G
H
A RUN normal operation

HOLD input closed or cal delay: Instrument on hold
(shows status of signal outputs).
OFF input closed: control/limit is interrupted (shows
status of signal outputs).
B ERROR Error Fatal Error
C Reagent low
D Transmitter control via Profibus
E Time
F Process values with time stamp
G Sample flow in bubbles per second
H Sample temperature
I Relay status
Relay status, symbols

upper/lower limit not yet reached
upper/lower limit reached
control upw./downw. no action
control upw./downw. active, dark bar indicates control
intensity
motor valve closed
motor valve: open, dark bar indicates approx. position
timer
timer: timing active (hand rotating)
40 A-96.250.671 / 150517
AMI Silica
Operation
Display when
A B C D E
Operating with
two Sample
Streams
RUN 15:20:18
R1 15:10:52
Si1 0.0 ppb
F
15:20:52
R2
Si2 0.0 ppb ~
I 24.2°C 31 B/s
G
H
A RUN normal operation

HOLD input closed or cal delay: Instrument on hold
(shows status of signal outputs).
OFF input closed: control/limit is interrupted (shows
status of signal outputs).
B ERROR Error Fatal Error
C Reagent low
D Transmitter control via Profibus
E Time
F Process values with time stamp
Si1 sample stream 1
Si2 sample stream 2
< Channel active
~ No sample flow
n Measurement not valid (not visible in this example)
x Only visible if a Sample Sequencer is connected to the
AMI Silica.
Indicates that the sample stream is inactive.
G Sample flow in bubbles per second
H Sample temperature
I Relay status
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AMI Silica
Operation
5.3 Software Structure
Main Menu 1
Messages
Diagnostics
Maintenance
Operation
Installation
Menu Messages 1
Messages 1.1
Reveals pending errors as well as an event history
Pending Errors
(time and state of events that have occurred at an
Maintenance List
Message List earlier point of time).
It contains user relevant data.
Menu Diagnostics 2
Diagnostics 2.1
Identification Provides user relevant instrument and sample data.
Sensors
Sample
I/O State
Interface
Menu Maintenance 3
Maintenance 3.1
For instrument calibration, relay and signal output
Calibration
Service
simulation, and to set the instrument time.
Simulation It is used by the service personnel.
Set Time 01.01.05 16:30:00
Menu Operation 4
Operation 4.1
User relevant parameters that might need to be
Grab Sample
Sensors modified during daily routine. Normally password
Relay Contacts protected and used by the process-operator.
Logger Subset of menu 5 - Installation, but process-related.
Menu Installation 5
Installation 5.1
Sensors For initial instrument set up by SWAN authorized
Signal Outputs person, to set all instrument parameters. Can be
Relay Contacts protected by means of password.
Miscellaneous
Interface
42 A-96.250.671 / 150517
AMI Silica
Operation
5.4 Changing Parameters and Values

Changing The following example shows how to change the logger interval:
parameters 1 Select the parameter you want to
Logger
Sensors 5.1.2
4.4.1
change.
Sensor type
Log interval FOME
30 min
Disinf.logger Free chlorine 2 Press [Enter]
Clear no
Temperature NT5K
Standards
3 Press [ ] or [ ] key to
Logger 4.1.3
highlight the required parameter.
Log interval Interval. 30min
5 min
Clear logger no 4 Press [Enter] to confirm the selec-
10 min tion or [Exit] to keep the previous
30 min parameter).
1 Hour
 The selected parameter is

Logger 4.1.3
highlighted but not saved yet.
Log interval 10 min
Clear logger no 5 Press [Exit].
 Yes is highlighted.
Logger 4.1.3
Log interval
Save ?
6 Press [Enter] to save the new pa-
Clear logger no rameter.
Yes
No  The system reboots, the new
parameter is set.
Changing 1 Select the value you want to

values Alarm Si 1 5.3.1.1.1
change.
Alarm High 5.00 ppm
Alarm Low 0.00 ppb 2 Press [Enter].
Hysteresis 10.0 ppb 3 Set required value with [ ] or
Delay 5 Sec
[ ] key.
4 Press [Enter] to confirm the new
Alarm Si 1 5.3.1.1.1
value.
Alarm High 0.20 ppm
Alarm Low 0.00 ppb 5 Press [Exit].
Hysteresis 10.0 ppb Yes is highlighted.
Delay 5 Sec
6 Press [Enter] to save the new val-
ue.
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AMI Silica
Operation
5.5 Grab Sample Measurement

Select Menu 4.1 (Operation/Grab Sample) and follow the instruc-
tions on the display.
Relay status during grab sample measurement:
 Signal outputs are on hold
 All limits are switched off
1 Close the flow regulating valve.
Grab Sample 4.1.5
- close sample tap 2 Prepare 1 l of sample.
- prepare 1 liter of sample.
Wait for next prompt

3 Fill the flow cell with the prepared
Grab Sample 4.1.5
sample.
- Fill flow cell with Sample
<Enter> to continue
4 Wait until the measuring has been
Grab Sample 4.1.5 finished.
Wait till measuring is
completed
Progress
Grab Sample 4.1.5

Measuring completed
Wait till flow cell is empty
Press <Enter> to finish the grab sam-

Grab Sample 4.1.5
ple measurement.
Operation completed
Open sample tab
Grab Sample 0.3 ppb NOTICE: The measuring value of
the grab sample is not saved!
<Enter> to finish
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Maintenance
6. Maintenance
6.1 Maintenance Schedule
WARNING
Stop operation before maintenance.

 Stop sample flow.
 Shut off power of the instrument.
Weekly Check sample supply for dirt.

Check sample flow.
Monthly Check reagent level.
Every 6 months Exchange reagent pump tube.
By occurrence: E020, FOME dirty: Cleaning the Photometer, p. 53
E022, Reagent empty: Refill or replace Reagents, p. 46
E065, Reagents low: Refill or replace Reagents, p. 46
6.2 Stop of Operation for Maintenance

1 Put suction lances into a bucket with demineralized water.
2 Start fill system.
3 Wait until the peristaltic pump has stopped.
4 Stop sample flow.
5 Wait until the constant head is empty.
6 Put suction lances into an empty bucket
7 Shut off power of the instrument.
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AMI Silica
Maintenance
6.3 Refill or replace Reagents

The liquid level in container 4 is monitored. The following messag-
es are displayed.
Container almost Maintenance E065 - Reagents low and the
empty remaining reagent volume in % (starting at
17 % = 340 ml).
Container empty Error E022 - Reagent empty
WARNING
Health hazard
 For safe handling of the reagents you must read and under-
stand the Material Safety Data Sheets (MSDS).
 Only persons trained in handling dangerous chemicals are al-
lowed to prepare the reagents.
Canister setup A Suction lance without
A
level detector
(containers 1–3)
B B Suction lance with
level detector
(container 4)
C Level detector
D 2 L mark
E Container 1:
C Ammonium
molybdate
F Container 2:
D 2L 2L 2L 2L Sulfuric Acid
E G Container 3:
Oxalic Acid
OXYCON ON-LINE SILCA
AMI SILICA REAGENT 1
AMI SILICA REAGENT 4 H Container 4:
F Ammonium Ferrous
G Sulfate
H I Holder
I
46 A-96.250.671 / 150517
AMI Silica
Maintenance
Reagent The 2 liter reagent canister will last for 1 month of operation with
consumption default measurement interval of 10 minutes. The provided reagent
set for 3 canister fillings therefore lasts for 3 months of operation.
Duration per Duration per

Measuring interval canister reagent set
10 minute ~ 1 month 3 months
15 minutes ~ 1.5 months 4.5 months
20 minutes ~ 2 months 6 months
30 minutes ~ 3 months 9 months
NOTICE: Please consider the following two points when

preparing new reagents:
• Reagent 3, Oxalic Acid dissolves very slowly, we therefore
recommend to prepare Reagent 3 first.
• Reagent 1, add Sodium hydroxide (Reagent 1b) first.
General 1 Rinse all containers well with demineralized water.

procedure 2 Fill the container to 3/4 of its final level with demineralized water.
3 Carefully add the chemicals. See Reagent 1, p. 48,
Reagent 2, p. 48, Reagent 3, p. 48, Reagent 4, p. 48
4 Screw the cover onto the container and mix well.
5 Fill the container to its final level and mix again.
6 Put container into the holder, number 1 to 4 from left to right.
7 Insert suction lances into the containers; make sure that the
numbers on the suction lances correspond to the numbers on
the containers.
8 Lock cover.
A-96.250.671 / 150517 47
AMI Silica
Maintenance
Reagent 1 Ammonium molybdate

 Reagent 1a: Add 56 g of Ammonium molybdate Tetrahydrate
 Reagent 1b: Add 16 g of Sodium hydroxide pellets
WARNING
Sulfuric Acid is corrosive and causes severe burns.

 Read the Material Safety Data Sheets (MSDS) first.
 Only persons trained in handling dangerous chemicals are al-
lowed to prepare the reagents
 Wear suitable protective clothing, gloves and eye/face protec-
tion.
 In case of contact with eyes, rinse immediately with plenty of
water eyelid wide open, summon medical advice. In case of
accident or if you feel unwell, summon medical advice imme-
diately (show the label where possible).
Reagent 2 Sulfuric Acid

 Add 200 ml Sulfuric Acid 25% to the container.
Reagent 3 Oxalic Acid
 Add 40 g Oxalic acid dihydrate.
Reagent 4 Ammonium Ferrous Sulfate

 Reagent 4a: Add 80 ml Sulfuric acid 25%
 Reagent 4b: Add 13 g Ammonium iron (II) sulfate hexahy-
drate
All canisters
Always replace the reagent filters (included with each reagent set)
when preparing new reagents.
Insert suction lances into the containers. Make sure that the num-
bers on the suction lances correspond to the numbers on the con-
tainers.
48 A-96.250.671 / 150517
AMI Silica
Maintenance
6.4 Verification
The “Verification kit for AMI Photometer” is available as
an accessory. An optical window with a precisely deter-
mined absorbance value is placed into the light beam
of the photometer. The actual measured absorbance
will be compared to the reference value labeled on
each kit.
Relay status during verification:

Set reference Prior to performing the verification the reference value, e.g. 0.235,
value: needs to be set in menu <Installation \ Sensors \ Ref. Verification>
5.1.2*) Verification reference value.
Verification Basically follow the dialog in menu <Maintenance> \ <Service> \
procedure: <Verification> 3.2.1*)
NOTICE: Start any time, if a measuring cycle is in progress wait

for next prompt.
1 Stop sample flow by closing the flow regulating valve. Wait for
next prompt: Constant head will be drained and an automatic
zero will be defined.
2 Open cuvette of the photometer and insert the verification filter.
[Enter] to continue.
3 Adjust for minimal absorbance (see AMI Display).
4 Press [Enter] to save the verification measurement. The verifi-
cation is successful if the difference is within the limits. <Enter>
to continue.
5 Remove filter, close cuvette and open regulating valve. <Enter>
to finish and [Exit] to the main display.
Verification Can be reviewed in menu Verification History
history: <Diagnostics \ Sensors \ FOME Sensor \ Ver. History> 2.2.1.5*
A-96.250.671 / 150517 49
AMI Silica
Maintenance
6.5 Calibration
Select Menu 3.1 (Maintenance/Calibration) and follow the instruc-
tions on the display.
Relay status during calibration:
1 Close the flow regulating valve.
Calibration 3.1.1
- Close sample tap 2 Prepare 1 l of Standard.
- Prepare 1 liter of standard.

Standard: 100 ppb
3 Fill the flow cell with the prepared
Calibration 3.1.1
standard.
- Fill flow cell with
standard
<Enter> to continue
4 Wait until the calibration has been
Calibration 3.1.1 finished.
Wait till calibration is
completed
Progress
Calibration 3.1.1
Calibration completed
Wait till flow cell is empty
Press [Enter] to save the value in the

Calibration 3.1.1
calibration history or leave the menu
Operation completed
Open sample tab
with [Exit].
Slope 1.047
<Enter> to save
50 A-96.250.671 / 150517
AMI Silica
Maintenance
6.6 Cleaning the Flow Cell
CAUTION
Acrylic glass parts are fragile and scratch-sensitive.

Possible damage of acrylic glass parts due to scrubbing materi-
als.
 Never use organic solvents or scrubbing materials to clean
acrylic glass parts.
 Use soft detergent and rinse well. Eliminate lime deposits with
a common household deliming agent in standard concentra-
tion.
 Do not drop the constant head tube
6.6.1 Disassemble the Constant Head

The flow cell can be disassembled easily. Before disassemble the
flow cell, switch off the instrument according to instructions in Stop
of Operation for Maintenance, p. 45.
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AMI Silica
Maintenance
A A Constant head cover

B Constant head tube
C Overflow tube
D O-Ring
B E Flow cell block
F Flow regulating valve
Level G Solenoid valve
E
F
Cleaning 1 Remove the constant head cover [A].

2 Pull the constant head tube [B] (constant head) out of the flow
cell block [E].
3 Clean all acrylic parts with a soft brush (bottle cleaner) and
soapy water.
4 Replace all O-rings before reassembling the flow cell.
NOTICE: A film of teflon paste (e.g. Fomblin from Solvay

Solexis) on the O-rings improves tightness and life time.
Assemble the Constant Head according to Install the Constant

Head, p. 19
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AMI Silica
Maintenance
6.7 Cleaning the Photometer

Clean the photometer after indication by alarm (E020, FOME dirty).
Before opening the photometer, switch off the instrument according
to instructions in Stop of Operation for Maintenance, p. 45
Material Small brush.
Procedure A Flow regulating valve
B Photometer cover
A C Photometer
D Brush
B
1 Close the flow regulating valve [A].

2 Wait until the sample flow through the photometer has stopped
3 Unscrew the cover [B] from the photometer [C].
4 Clean the Photometer with a small brush [D].

5 Screw the cover to the photometer.
6 Open the flow regulating valve.
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AMI Silica
Maintenance
6.8 Cleaning the solenoid valve

Disassemble The solenoid valve is mounted below the constant head. The sole-
the solenoid noid valve should be disassembled if it does not switch anymore or
valve if it is clogged.
1 Switch off the instrument according to instructions in Stop of

Operation for Maintenance, p. 45
2 Loosen the nut (A).
3 Remove the solenoid coil (B) from

the valve body (C).
B
4 Loosen the fixing screws of the

valve body with a 2.5 mm allen key
(D).
54 A-96.250.671 / 150517
AMI Silica
Maintenance
NOTICE: The O-rings inside the

valve body may stick on the flow
cell and fall down if the valve body
is removed.
5 Remove the valve body from the
flow cell.
E
6 Remove the white plate (G) with a

screw driver size 0 (F).
The membrane (H) is now

visible.
7 Clean base plate (G) and mem-
H brane (H) with clean water.
Assemble Assemble the solenoid valve in reverse order.
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AMI Silica
Maintenance
6.9 Tube Replacement
6.9.1 Replace the Pump Tubes

The pump tube [D] of the peristaltic pump is exposed to a minimal
wear.
It is therefore recommended to exchange the pump tube every 6
months.
CAUTION
Pollution of reagents possible.
If the occlusion frames are opened during operation, already
mixed reagents will flow back into the reagent canisters and pol-
lute the reagents.
 Never open the occlusion frames if the instrument is in opera-
tion.
 Proceed according to Stop of Operation for Maintenance, p.
45 before opening the occlusion frames.
Overview A Pump housing

B Occlusion frame
A
closed
B C Rotor
D Pump tube
C
E Pump inlet
D F Pump outlet
56 A-96.250.671 / 150517
AMI Silica
Maintenance
Dismount The pump tube can easily be dismounted and mounted.

pump tubes Proceed as follows:
A Pump housing
B Occlusion frame open
A
C Rotor
B D Pump tube
C E Pump inlet
D F Pump outlet
E
F
1 Switch off the instrument according to instructions in Stop of

Operation for Maintenance, p. 45.
2 Relax the pump tube by turning the occlusion frame (B) count-
er-clockwise.
3 Remove the occlusion frame (B) from the rotor (C) by pulling
the complete occlusion frame out of the holder.
4 Dismount all reagent tubes from the occlusion frame.
5 Exchange the occlusion frame.
6 Install all reagent tubes.
7 Check that the occlusion frame is aligned perpendicular to the
axis of the rotor.
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AMI Silica
Maintenance
6.9.2 Tube Numbering
Level
6
5 5
1 7
6 7
4
2
3
1 2 3 4
J K L M
Tube
No. from to
1 Reagent container J 6-way valve port 1
2 Reagent container K 6-way valve port 2
3 Reagent container L 6-way valve port 3
4 Reagent container M 6-way valve port 4
5 6-way valve port 5 Photometer
6 6-way valve port 7 Peristaltic pump input
7 Peristaltic pump output Photometer reagent input
58 A-96.250.671 / 150517
AMI Silica
Maintenance
6.10 Fill or Flush Reagent System

Fill or flush the reagent tubing:
 after refilling the reagent containers,
 before a system shut-down to flush the system with demin
water until no more reagent is left in the system.
Service 3.2.2 Fill System 3.2.2.5

Verification
Enter Progress
Fill System
Manual filling
<Enter> to stop
Fill System 3.4.5
Progress
Done
Press 4 x [Exit]
6.11 Check Outputs and Relays

Terminal designations see Connection Diagram, p. 28
Check signal outputs and relay function by means of the connected
device or a multimeter.
Maintenance 3.3 Simulation 3.3.1

Calibration Alarm Relay active/inactive
Service Enter Relay 1 active/inactive
Simulation Relay 2 active/inactive
Set Time 01.06.04 16:30:00 Signal Output 1 x mA
Cleaning Signal Output 2 x mA
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AMI Silica
Maintenance
6.12 Replacing Fuses
WARNING
External Voltage.
External supplied devices connected to relay 1 or 2 or to the
alarm relay can cause electrical shocks.
 Make sure that the devices connected to the following con-
tacts are disconnected from the power before resuming in-
stallation.
– relay 1
– relay 2
– alarm relay
When a fuse has blown, find out the cause and fix it before
replacing it with a new one.
Use tweezers or needle-nosed pliers to remove the defective fuse.
Use original fuses provided by SWAN only.
A B C D E F G
A 1.6 AT/250V Instrument power supply

B 1.0 AT/250V Relay 1
C 1.0 AT/250V Relay 2
D 1.0 AT/250V Alarm relay
E 1.0 AF/125V Signal output 2
F 1.0 AF/125V Signal output 1
G 1.0 AF/125V Signal output 3
60 A-96.250.671 / 150517
AMI Silica
Maintenance
6.13 Longer Stop of Operation

1 Proceed according to chapter Stop of Operation for Mainte-
nance, p. 45.
2 Empty the measuring cell of the photometer, for example with a
pipette and dry it with a soft tissue.
3 Relax the occlusion frame of the Peristaltic pump.
See Replace the Pump Tubes, p. 56
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AMI Silica
Troubleshooting
7. Troubleshooting
This chapter provides some hints to make troubleshooting easier.
For any detailed information how to handle or clean parts please
see Maintenance, p. 45. For any detailed information how to pro-
gram the instrument please see Program List and Explanations, p.
74.
7.1 Slope Error

Slope error is a calibration error. It occurs, if the correction factor
(slope) is > 2.0 or <0.5.
NOTICE: When mixing new reagents or standard solution:

• never use water contaminated with silica.
• do not use any glass containers to mix reagents or standard
solution.
If the calibration factor is too high do the following:
1 Check the programmed standard. See chap. 9, 5.1.2, p. 79.

2 Prepare a new standard solution with demineralized water, use
SWAN stock solution only.
3 Clean all canisters and suction lances with a mix of demineral-
ized water and one percent hydrochloric acid.
4 Prepare new reagents with SWAN original reagents, see Refill
or replace Reagents, p. 46.
If the calibration factor is too low do the following:
1 Prepare a new standard solution with demineralized water, use

SWAN stock solution only.
2 Clean all canisters and suction lances with a mix of demineral-
ized water and one percent hydrochloric acid.
3 Check the pump delivery volume.
62 A-96.250.671 / 150517
AMI Silica
Troubleshooting
Check pump A low calibration factor may be caused by leaking tube connec-
delivery tions. The delivery volume of the peristaltic pump is approximately
volume 4.2 g/min.
B
6
5 5
1 7
6 7
4 C
2
3
1 2 3 4
D
2.1 g
E
J K L M
A Flow regulating valve D Beaker
B Peristaltic pump E Balance
C Tube fitting
Check the delivery volume of the peristaltic pump as follows:
1 Close the flow regulating valve [A] to stop the sample flow.
2 Put a beaker [D] onto a balance [E] and set the balance to zero.
3 Unscrew and remove the tube fitting [C] from the photometer to
disconnect tube No. 7.
 The sample contained in the photometer will flow out.
4 Put the tube into the beaker.
5 Navigate to menu <Maintenance>/<Service>/<Manual Filling>
and press [Enter].
6 Select <Position> and press [Enter].
7 Set the 6-way valve to position 1 with the [ ] or [ ] key.
 The positions 1 to 4 of the 6-way valve are assigned to the 4
canisters.
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AMI Silica
Troubleshooting
8 After the 6-way valve position has been set, select <Pump> and
press [Enter].
9 Set the pump to <on> for a half minute.
 The reagent is pumped into the beaker.
10 Read the weight on the display of the balance.
 The weight must be within 2.0 to 2.3 g.
11 Repeat step 6 to 10 and set the 6-way valve to position 2, 3,
and 4 to check the tubes of the canisters 2, 3 and 4.
If the reagent volume is below 2g:

 check the tube connections for leakage
 check if a tube is damaged (i.e. kniked)
 Replace the pump tubes of the peristaltic pump, see Tube
Replacement, p. 56
 Replace the 6-way valve, see enclosed installation instruc-
tion.
7.2. Grab Sample

The function grab sample is normally used to measure an external
sample. But it can be used for verification as well.
If the function grab sample is used for verification, the deviation to
the expected value should be less than 30%. If the deviation is
higher or lower than 30%, proceed as described in chap. “Slope Er-
ror” on page 62.
64 A-96.250.671 / 150517
AMI Silica
Troubleshooting
7.3. Error List

Error
Non-fatal Error. Indicates an alarm if a programmed value is ex-
ceeded.
Such Errors are marked E0xx (bold and black).
Fatal Error (blinking symbol)
Control of dosing devices is interrupted.
The indicated measured values are possibly incorrect.
Fatal Errors are divided in the following two categories:
 Errors which disappear if correct measuring conditions are re-
covered (i.e. Sample Flow low).
Such Errors are marked E0xx (bold and orange)
 Errors which indicate a hardware failure of the instrument.
Such Errors are marked E0xx (bold and red)
HOLD 14:10:45 Error or fatal Error

R1 Error not yet acknowledged.
Check Pending Errors 1.1.5 * and
R2 21.5 ppb
take corrective action.
23 B/s Press [ENTER].
Main Menu 1
Reagent level low
Messages Indicates the remaining reagent in per-
Diagnostics cent
Maintenance Navigate to menu Messages.
Operation Press [ENTER].
Installation
Messages 1.1 Navigate to menu Pending Errors.

Pending Errors Press [ENTER].
Maintenance List
Message List
Pending Errors 1.1.5 Press [ENTER] to acknowledge the

Error Code E002 Pending Errors. The Error is reset and
saved in the Message List.
Si1 Alarm low
* Menu numbers see
<Enter> to Acknowledge
Program Overview, p. 69
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AMI Silica
Troubleshooting
Error Description Corrective action

E001 Si 1 Alarm high – check process
– check programmed value 5.3.1.1.1, p.
85
E002 Si 1 Alarm low – check process
85
E003 Si 2 Alarm high – check process
85
E004 Si 2 Alarm low – check process
85
E007 Sample Temp. high – check process
– check programmed value
E008 Sample Temp. low – check process
– check programmed value
E009 Sample Flow high – check inlet pressure
– re-adjust sample flow
86
E010 Sample Flow low – check inlet pressure
– re-adjust sample flow
– clean instrument
86
E012 Temp. disconnected – shut off power
– check wiring of photometer, see
Connection Diagram, p. 28
E013 Case Temp. high – check case/environment temperature
– check programmed value 5.3.1.4, p. 86
E014 Case Temp. low – check case/environment temperature
– check programmed value 5.3.1.51, p.
86
66 A-96.250.671 / 150517
AMI Silica
Troubleshooting

E015 Valve defective – check valve, see Cleaning the solenoid
valve, p. 54
E017 Control Timeout – check control device or programming in
Installation, Relay contact, Relay 1/2
5.3.2 and 5.3.3, p. 87
E018 Reagent Pump – shut off power
– check wiring, see Connection Diagram,
p. 28
E019 FOME not connected – shut off power
– check wiring check wiring, see
Connection Diagram, p. 28
E020 FOME dirty – clean photometer, see Cleaning the
Photometer, p. 53
E022 Reagent empty – fill reagents,
– see Refill or replace Reagents, p. 46
E023 Sequencer – check Sample Sequencer connection
E024 Input active – See If Fault Yes is programmed in
Menu 5.3.4, p. 91
E026 IC LM75 – call service
E028 Signal output open – check wiring on signal outputs 1 and 2.
E030 I2C Rovalve – call service
E031 Calibration Recout – call service
E032 Wrong Frontend – call service
E033 Sample Flow 1 low – See operating manual Sample

(Sample Sequencer) Sequencer
– If 2nd Sample Stream option is
installed, see E010
– If 2nd Sample Stream option is
installed, see E010
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AMI Silica
Troubleshooting



E049 Power-on – none, normal status

E050 Power-down – none, normal status
E065 Reagent low – Observe the decreasing number on the
screen, indicating for how many hours
the reagent lasts. Refill reagents on
time. See Refill or replace Reagents, p.
46
68 A-96.250.671 / 150517
AMI Silica
Program Overview
8. Program Overview
For explanations about each parameter of the menus see Program
List and Explanations, p. 74.
 Menu 1 Messages informs about pending errors and mainte-

nance tasks and shows the error history. Password protection
possible. No settings can be modified.
 Menu 2 Diagnostics is always accessible for everybody. No
password protection. No settings can be modified.
 Menu 3 Maintenance is for service: Calibration, simulation of
outputs and set time/date. Please protect with password.
 Menu 4 Operation is for the user, allowing to set limits, alarm
values, etc. The presetting is done in the menu Installation
(only for the System engineer). Please protect with password.
 Menu 5 Installation: Defining assignment of all inputs and
outputs, measuring parameters, interface, passwords, etc.
Menu for the system engineer. Password strongly recom-
mended.
8.1 Messages (Main Menu 1)

Pending Errors Pending Errors 1.1.5* * Menu numbers
1.1*
Maintenance List Maintenance List 1.2.5*
1.2*
Message List Number 1.3.1*
1.3* Date, Time
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AMI Silica
Program Overview
8.2 Diagnostics (Main Menu 2)

Identification Designation AMI Silica * Menu numbers
2.1* Version V6.20-08/16
Peripherals PeriClip 1.06 2.1.3.1*
2.1.3 RoValve 1.60
Factory Test Instrument 2.1.4.1*
2.1.4* Motherboard
Operating Time Years / Days / Hours / Minutes / Seconds 2.1.5.1*
2.1.5*
Sensors FOME Sensor Current Value ppb
2.2* 2.2.1* (Raw value) V
Absorbance
Cal. History Number 2.2.1.4.1*
2.2.1.4* Date, Time
Slope
Ver. History Number 2.2.1.5.1*
2.2.1.5* Date, Time
Absorbance
Reference value
Miscellaneous Case Temp. 2.2.2.1*
2.2.2* State Machine
Sample Sample ID 2.3.1*
2.3* Temperature
Sample Flow
I/O State Alarm Relay 2.4.1*
2.4* Relay 1/2 2.4.2*
Input
Signal Output 1/2
Interface Protocol 2.5.1* (only with RS485
2.5* Baud rate interface)
70 A-96.250.671 / 150517
AMI Silica
Program Overview
8.3 Maintenance (Main Menu 3)

Calibration Calibration Progress * Menu numbers
3.1* 3.1.5*
Service Verification (Progress) 3.2.1.1*
3.2* 3.2.1*
Fill System (Progress) 3.2.2.5*
3.2.2*
Manual Filling Position 3.2.3.1*
3.2.3 Pump 3.2.3.2*
Simulation Alarm Relay 3.3.1*
3.3* Relay 1 3.3.2*
Relay 2 3.3.3*
Signal Output 1 3.3.4*
Signal Output 2 3.3.5*
Magnetic valve 1 3.3.6*
Magnetic valve 2 3.3.7*
Stirrer 3.3.8*
Set Time (Date), (Time)
3.4*
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AMI Silica
Program Overview
8.4 Operation (Main Menu 4)

Grab Sample
4.1*
Sensors Filter Time Const. 4.2.1*
4.2* Hold after Cal. 4.2.2*
Relay Contacts Alarm Relay Alarm Si 1 (Si 2) Alarm High 4.3.1.1.1*
4.3* 4.3.1* 4.3.1.1* Alarm Low 4.3.1.1.25*
Hysteresis 4.3.1.1.35*
Delay 4.3.1.1.45*
Relay 1/2 Setpoint 4.3.x.100*
4.3.2* - 4.3.3* Hysteresis 4.3.x.200*
Delay 4.3.x.30*
Input Active 4.3.4.1*
4.3.4* Signal Outputs 4.3.4.2*
Output / Control 4.3.4.3*
Fault 4.3.4.4*
Delay 4.3.4.5*
Logger Log Interval 4.4.1*
4.4* Clear Logger 4.4.2* * Menu numbers
8.5 Installation (Main Menu 5)

Sensors Ref. Veification 5.1.1* * Menu numbers
5.1* Standard 5.1.2*
Blank 5.1.3*
Meas. interval 5.1.4*
Channels 5.1.5*
Channel Selection 5.1.6*
Signal Outputs Signal Output 1/2 Parameter 5.2.1.1 - 5.2.2.1*
5.2* 5.2.1* - 5.2.2* Current Loop 5.2.1.2 - 5.2.2.2*
Function 5.2.1.3 - 5.2.2.3*
Scaling Range Low 5.2.x.40.12/10*
5.2.x.40 Range High 5.2.x.40.22/20*
Signal Sequencer Parameter 5.2.4.1*
5.2.4* Current Loop 5.2.4.2*
Function 5.2.4.3*
72 A-96.250.671 / 150517
AMI Silica
Program Overview
Scaling Range Low 5.2.4.40.10*

5.2.4.40* Range High 5.2.4.40.20*
Relay Contacts Alarm Relay Alarm Si 1(Si 2) Alarm High 5.3.1.1.1*
5.3* 5.3.1* 5.3.1.1* Alarm Low 5.3.1.1.25
Hysteresis 5.3.1.1.35
Delay 5.3.1.1.45
Sample Temp. Alarm High 5.3.1.2.1*
5.3.1.2 Alarm Low 5.3.1.2.25*
Sample Flow Flow Alarm 5.3.1.3.1*
5.3.1.3* Alarm High 5.3.1.3.2*
Alarm Low 5.3.1.3.35*
Case Temp. high 5.3.1.4*
Case Temp. low 5.3.1.51*
Relay 1/2 Function 5.3.2.1 - 5.3.3.1*
5.3.2* - 5.3.3* Parameter 5.3.2.20 - 5.3.3.20*
Setpoint 5.3.2.302-5.3.3.302*
Hysteresis 5.3.2.402-5.3.3.402*
Delay 5.3.2.50 - 5.3.3.50*
Input Active 5.3.4.1*
5.3.4* Signal Outputs 5.3.4.2*
Output/Control 5.3.4.3*
Fault 5.3.4.4*
Delay 5.3.4.5*
Miscellaneous Language 5.4.1*
5.4* Set defaults 5.4.2*
Load Firmware 5.4.3*
Password Messages 5.4.4.1*
5.4.4* Maintenance 5.4.4.2*
Operation 5.4.4.3*
Installation 5.4.4.4*
Sample ID 5.4.5*
Line Break Detection 5.4.6*
Interface Protocol 5.5.1* (only with RS485
5.5* Device Address 5.5.21* interface)
Baud Rate 5.5.31*
Parity 5.5.41* * Menu numbers
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Program List and Explanations
9. Program List and Explanations
1 Messages
1.1 Pending Errors
1.1.5 Provides the list of active errors with their status (active,
acknowledged). If an active error is acknowledged, the alarm relay
is active again. Cleared errors are moved to the Message list.
1.2 Maintenance List
1.2.5 Demands necessary maintenance, e.g. preparing new reagents.
1.3 Message List
1.3.1 Shows the error history: Error code, date / time of issue and status
(active, acknowledged, cleared). 65 errors are memorized. Then
the oldest error is cleared to save the newest error (circular buffer).
2 Diagnostics
In diagnostics mode, the values can only be viewed, not modified.
2.1 Identification
Designation: Designation of the instrument.
Version: Firmware of instrument (e.g. V6.20-08/16)
2.1.3 Peripherals:
2.1.3.1 PeriClip: Firmware of peristaltic pump (e.g. 1.06)
RoValve: Firmware of rotary valve (6-way valve) (e.g. 1.60)
2.1.4 Factory Test: Test date of the Instrument and Motherboard
2.1.5 Operating Time: Years / Days / Hours / Minutes / Seconds
2.2 Sensors
2.2.1 FOME Sensor:
Current value: Shows the actual photometer signal in ppb.
Raw value: Shows the actual photometer signal in V.
Absorbance: Process value, depends on sample.
2.2.1.4 Cal. History: Review diagnostic values of the last calibrations.
Factor (slope).
Max. 64 data records are memorized. One calibration step
corresponds to one data record:
Slope photometer: 0.5–2.0
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2.2.1.5 Ver. History: Review verifications values of the last verifications:

Absorbance: Measured absorbance of the reference kit.
Reference value: True value of the reference kit according to label.
2.2.2 Miscellaneous:
2.2.2.1 Case Temp: Shows the actual temperature in [°C] inside the
transmitter.
State Machine: Number 1–7 are assigned to the initial start up
procedure.
Number 8–23 are assigned to the measuring cycle.
Machine state 6-way valve position peristaltic pump
9 5 on
10 5 on
11 5 off
12 1 on
13 2 on
14 5 on
15 5 off
16 3 on
17 5 on
18 5 off
19 4 on
20 5 on
21 5 off
22
23
Number 24 is assigned to the manual filling function.

Number 25–31 are assigned to the calibration procedure.
Number 32–35 are assigned to the verifying procedure.
2.3 Sample
2.3.1 Sample ID: Review the programmed code. The code is defined by
the user to identify the sample point in the plant.
Temperature: Shows the Actual temperature in °C.
Sample flow: Shows the actual sample flow [B/s] (bubbles per
second). Sample flow must be above 5 B/s.
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2.4 I/O State

Shows actual status of all in- and outputs.
2.4.1 and 2.4.2
Alarm Relay: Active or inactive
Relay 1 and 2: Active or inactive
Input: Open or closed
Signal Output 1 and 2: Actual current in mA
Signal Output 3: Actual current in mA (if option is installed)
2.5 Interface
Only available if optional interface is installed.
Review programmed communication settings.
3 Maintenance
3.1 Calibration
3.1.5 Performs a calibration using the standard solution. Follow the
instruction on the screen. See Calibration, p. 50
3.2 Service
3.2.1 Verification: Performs a verification using the verification kit.
Follow the instruction on the screen. See Verification, p. 49.
3.2.2 Fill System: Activates the reagent pump and fills all tubes from the
container to the 6-way valve.
3.2.3 Manual Filling: In the menu <Manual filling> the position of the
6-way valve can be set manually and the peristaltic pump can be
switched on and off.
3.2.3.1 Position: Set the position of the 6-way valve.
Pos. 1 Reagent 1
Pos. 2 Reagent 2
Pos. 3 Reagent 3
Pos. 4 Reagent 4
Pos. 5 Loop
Pos. 6 –
3.2.3.2 Pump: Switch the peristaltic pump on or off.
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3.3 Simulation
Select the alarm relay, relay 1 and 2, signal output 1 and 2, input,
magnetic valve 1 and 2 or stirrer with the up/down keys. Then press
<Enter> to change the setting or value. After confirming the setting
with the Enter key, the value is simulated by the relay/signal output.
Alarm Relay: Active or inactive
Relay 1 and 2: Active or inactive
Input: Open or closed
Signal Output 1 and 2: Actual current in mA
Signal Output 3: Actual current in mA (if option is installed)
Magnetic valve 1 Active or inactive
Magnetic valve 2 Active or inactive
Stirrer Active or inactive
At the absence of any key activities, the instrument will switch back
to normal mode after 20 min. If you quit the menu, all simulated
values will be reset.
3.4 Set Time
Adjust date and time.
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4 Operation
4.1 Grab Sample
4.1.5 Starts a grab sample measurement. Follow the instruction on the
screen. See Grab Sample Measurement, p. 44
4.2 Sensors
4.2.1 Filter Time Constant: Used to damp noisy signals. The higher the
filter time constant, the slower the system reacts to changes of the
measured value.
Range: 5–300 Sec
4.2.2 Hold after Cal: Delay permitting the instrument to stabilize again
after calibration. During calibration, verification or grab sample plus
hold-time, the signal outputs are frozen (held on last valid value),
alarm values, limits are not active.
Range: 0–6‘000 Sec
4.3 Relay Contacts

See 5.3 Relay Contacts, p. 85
4.4 Logger
The instrument is equipped with an internal logger. The logger data
can be:
 copied to a PC with an USB stick if option USB interface is in-
stalled.
The logger can save approx. 1500 data records. Records consists
of: Date, time, alarms, measured value, temperature, flow.
Range: 1 Second to 1 hour
4.4.1 Log Interval: Select a convenient log interval. Consult the table
below to estimate the max logging time. When the logging buffer is
full, the oldest data record is erased to make room for the newest
one (circular buffer).
Event driven or interval (see table below)
Interval 1s 5s 1 min 5 min 10 30 1h Event

min min Driven
Time 25 min 2h 25 h 5d 10 d 31 d 62 d
4.4.2 Clear Logger: If confirmed with <yes>, the complete logger data is
deleted. A new data series is started.
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5 Installation
5.1 Sensors
5.1.1 Ref. Verification: Set absorbance value of verification kit according
to label.
Range: 0.200–0.600
5.1.2 Standard: Set the value in ppb of the standard you use for
calibration.
Range: 50 ppb–5 ppm
5.1.3 Blank: If the reagents contain a known amount of Silica, “Blank” can
be used to shift the zero point. The entered Blank value then is
subtracted from the measuring value.
Range: 0.0 ppb–10.0 ppb
5.1.4 Meas. Interval: The measuring interval can be set to 10, 15, 20 or
30 minutes.
5.1.5 Channels: Choose between 1 channel or 2 channel measurement.
If a Sample Sequencer is connected, up to 6 channels can be
chosen.
If 2 channels are selected, the transmitter switches automatically
between the channels after each measurement.
5.1.6 Channel Selection: The following 3 operating modes can be set:
 Internal
 Fieldbus
 External
Mode Internal In the Mode Internal, the AMI Silica works as a master.
2nd Sample Stream Option
The AMI Silica switches automatically between channel 1 and 2.
Sample Sequencer
The AMI Silica sequentially measures each single sample stream of
the Sample Sequencer.
Via an external PLC it can be defined which sample streams should
not be measured. In the example below, only the samples streams
2, 4 and 6 are measured, whereas the samples streams 1, 3 and 5
are switched off. Sample streams which are switched off are
marked with an “x” behind the measuring value on the AMI Silica
display.
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CH1 9
1 mA sink, 5 V open CH2 10
6 Inputs from PLC
CH3 11
Processor
CH4 12
CH5 13
CH6 14
GND 15
SEQUENCER
Mode Fieldbus The AMI Silica is controlled via fieldbus.
Mode External In the mode External, the AMI Silica works as a slave.
2nd Sample Stream Option
The 2nd Sample Stream Option is switched between sample
stream 1 and 2 via input, see Input 5.3.4, p. 91.
Sample Sequencer
The AMI Silica is controlled by the Sample Sequencer. The Sample
Sequencer in turn is controlled via an external PLC. Each sample
stream to be measured has to be activated by closing the respective
contact.
Example:
If sample stream 1 of the Sample Sequencer is active, the AMI Silica
measures the sample stream 1 until the Sample Sequencer changes
to the next programmed channel. In the example below, the sample
stream 3 (CH3) highlighted in green will be measured as soon as the
AMI analyzer has finished the previous measurement.The current
measurement is completed before the channel is switched.
CH1 9
CH2 10
1 mA sink, 5 V open
6 Inputs from PLC
CH3 11
Processor
CH4 12
CH5 13
CH6 14
GND 15
SEQUENCER
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5.2 Signal Outputs

5.2.1 and 5.2.2 Signal Output 1 and 2: Assign process value, the current loop
range and a function to each signal output.
NOTICE: The navigation in the menu <Signal Output 1> and
<Signal Output 2> is equal. For reason of simplicity only the
menu numbers of Signal Output 1 are used in the following.
5.2.1.1 Parameter: Assign one of the process values to the signal output.
Available values:
 Temperature
 Sample Flow
 Si 1
5.2.1.2 Current Loop: Select the current range of the signal output.
Make sure the connected device works with the same current
range.
Available ranges: 0–20 mA or 4–20 mA
5.2.1.3 Function: Define if the signal output is used to transmit a process
value or to drive a control unit. Available functions are:
 Linear, bilinear or logarithmic for process values.
See As process values, p. 81
 Control upwards or control downwards for controllers.
See As control output, p. 83
As process The process value can be represented in 3 ways: linear, bilinear or
values logarithmic. See graphs below.
[mA]
20
(0 - 20 [mA])
(4 - 20 [mA])
B A
10 12
0/4 X
0.0 0.1 0.2 0.3 0.4 0.5
A linear X Measured value

B bilinear
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[mA]
20
(0 - 20 [mA])
(4 - 20 [mA])
10 12
0/4 X
2 4 6
1 10 100 1’000 10’000
0 1 2 3 4
X Measured value (logarithmic)

5.2.1.40 Scaling: Enter beginning and end point (Range low & high) of the
linear or logarithmic scale. In addition, the midpoint for the bilinear
scale.
Parameter Temperature
5.2.1.40.10 Range low: -30 °C to + 120 °C
5.2.1.40.20 Range high: -30 °C to + 120 °C
Parameter Sample Flow
5.2.1.40.11 Range low: 0 –600 B/s
5.2.1.40.21 Range high: 0 –600 B/s
Parameter Si 1
5.2.1.40.12 Range low: 0 ppb –5 ppm
5.2.1.40.22 Range high: 0 ppb –5 ppm
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As control Signal outputs can be used for driving control units. We distinguish
output different kinds of controls:
 P-controller: The controller action is proportional to the devia-
tion from the setpoint. The controller is characterized by the
P-Band. In the steady-state, the setpoint will never be
reached. The deviation is called steady-state error.
Parameters: setpoint, P-Band
 PI-controller: The combination of a P-controller with an
I-controller will minimize the steady-state error. If the reset
time is set to zero, the I-controller is switched off.
Parameters: setpoint, P-Band, reset time.
 PD-controller: The combination of a P-controller with a
D-controller will minimize the response time to a fast change
of the process value. If the derivative time is set to zero, the
D-controller is switched off.
Parameters: setpoint, P-Band, derivative time.
 PID-controller: The combination of a P-, an I - and a D-con-
troller allows a proper control of the process.
Parameters: setpoint, P-Band, reset time, derivative time.
Ziegler-Nichols method for the optimization of a PID controller:
Parameters: Setpoint, P-Band, Reset time, Derivative time
Y
B A
X
a
A Response to maximum control output Xp = 1.2/a

B Tangent on the inflection point Tn = 2L
X Time Tv = L/2
The point of intersection of the tangent with the respective axis will
result in the parameters a and L.
Consult the manual of the control unit for connecting and
programming details. Choose control upwards or downwards.
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Control upwards/downwards
Setpoint: User-defined process value (Measured value or flow)
P-Band: Range below (upwards control) or above (downwards
control) the set-point, within the dosing intensity is reduced from
100% to 0% to reach the set-point without overshooting.
5.2.1.43 Control Parameters: Temperature
5.2.1.43.10 Setpoint: -30 °C to + 120 °C
5.2.1.43.20 P-Band: 0 °C to + 100 °C
5.2.1.43 Control Parameters: Sample Flow
5.2.1.43.11 Setpoint: 0 –600 B/s
5.2.1.43.21 P-Band: 0 –200 B/s
5.2.1.43 Control Parameters: Si 1
5.2.1.43.12 Setpoint: 0 ppb –5 ppm
5.2.1.43.22 P-Band: 0 ppb –5 ppm
5.2.1.43.3 Reset time: The reset time is the time till the step response of a
single I-controller will reach the same value as it will be suddenly
reached by a P-controller.
Range: 0–9’000 sec
5.2.1.43.4 Derivative time: The derivative time is the time till the ramp
response of a single P-controller will reach the same value as it will
be suddenly reached by a D-controller.
Range: 0–9’000 sec
5.2.1.43.5 Control timeout: If a controller action (dosing intensity) is constantly
over 90% during a defined period of time and the process value
does not come closer to the setpoint, the dosing process will be
stopped for safety reasons.
Range: 0–720 min
5.2.4 Signal Sequencer: Only visible if a Sample Sequencer is
connected.
Assign process value, the current loop range and a function to the
signal output.
5.2.4.1 Parameter: Only the parameter “Si Sequencer” is available.
5.2.4.2 Current Loop: Select the current range of the signal output.
Make sure the connected device works with the same current
range.
Available ranges: 0–20 mA or 4–20 mA
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5.2.4.3 Scaling: Define the scaling of the signal output used to transmit a
process value. Available functions are:
 Linear, bilinear or logarithmic for process values.
See As process values, p. 81
5.3 Relay Contacts
5.3.1 Alarm Relay: The alarm relay is used as cumulative error indicator.
Under normal operating conditions the contact is active.
The contact is inactive at:
 Power loss
 Detection of system faults like defective sensors or electronic
parts
 High case temperature
 Lack of reagents
 Process values out of programmed ranges.
Program alarm levels, hysteresis values and delay times for the
following parameters:
 Alarm Si 1
 Sample Temp.
 Sample Flow
 Case Temp. high
 Case Temp. low
5.3.1.1 Alarm Si 1
5.3.1.1.1 Alarm High: If the measured value rises above the alarm high
value, the alarm relay is activated and E001 (E003), is displayed in
the message list.
Range: 0.00 ppb –5.00 ppm
5.3.1.1.25 Alarm Low: If the measured value falls below the alarm low value,
the alarm relay is activated and E002 (E004) is displayed in the
message list.
Range: 0.00 ppb –5.00 ppm
5.3.1.1.35 Hysteresis: Within the hyst. range, the relay does not switch. This
prevents damage of relays contacts when the measured value
fluctuates around the alarm value.
Range. 0.00 ppb –5.00 ppm
5.3.1.1.45 Delay: Duration, the activation of the alarm relay is retarded after
the measuring value has risen above/fallen below the programmed
alarm.
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5.3.1.2 Sample Temp.: Define at which sample temperature an alarm

should be issued.
5.3.1.2.1 Alarm High: If the measured value rises above the alarm high
value, the alarm relay is activated.
Range: 30–70 °C
5.3.1.2.25 Alarm Low: If the measured value rises above the alarm high value,
the alarm relay is activated.
Range: 0–20 °C
5.3.1.3 Sample Flow: Define at which sample flow a flow alarm should be
issued.
5.3.1.3.1 Flow Alarm: Program if the alarm relay should be activated if there
is a flow alarm. Choose between yes or no. The flow alarm will
always be indicated in the display, pending error list, saved in the
message list and the logger.
Available values: Yes or no
NOTICE: Sufficient flow is essential for a correct measurement.
We recommend to program yes.
5.3.1.3.2 Alarm High: If the measuring values rises above the programmed
value E009 will be issued.
Range: 100–600 B/s
5.3.1.3.35 Alarm Low: If the measuring values falls below the programmed
value E010 will be issued.
Range: 5–80 B/s
5.3.1.4 Case Temp. high: Set the alarm high value for temperature of
electronics housing. If the value rises above the programmed value
E013 is issued.
Range: 30–75 °C
5.3.1.51 Case Temp. low: Set the alarm low value for temperature of
electronics housing. If the value falls below the programmed value
E014 is issued.
Range: -10–20 °C
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5.3.2 and 5.3.3 Relay 1 and 2: The contacts can be set as normally open or
normally closed with a jumper. See Relay 1 and 2, p. 31. The
function of relay contacts 1 or 2 are defined by the user.
NOTICE: The navigation in the menu <Relay 1> and <Relay 2>
is equal. For reason of simplicity only the menu numbers of
Relay 1 are used in the following.
1 First select the functions as:
- Limit upper/lower,
- Control upwards/downwards,
- Timer
- Fieldbus
- End of Batch (relay 2 only)
- Channel Selection (relay 2 only)
2 Then enter the necessary data depending on the selected func-
tion.
5.3.2.1 Function = Limit upper/lower:
When the relays are used as upper or lower limit switches, program
the following:
5.3.2.20 Parameter: select a process value
5.3.2.300 Setpoint: If the measured value rises above respectively falls below
the set-point, the relay is activated.
Parameter Range
Temperature -30 °C to + 120 °C
Sample Flow 0 –600 B/s
Si 1 0 ppb –5 ppm
5.3.2.401 Hysteresis: within the hysteresis range, the relay does not switch.
This prevents damage of relay contacts when the measured value
fluctuates around the alarm value.
Parameter Range
Temperature 0 °C –100 °C
Sample Flow 0 –200 B/s
Si 1 0 ppb –5 ppm
5.3.3.50 Delay: Duration, the activation of the alarm relay is retarded after
the measuring value has risen above/fallen below the programmed
alarm.
Range. 0–600 Sec
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5.3.2.1 Function = Control upwards/downwards:

The relays may be used to drive control units such as solenoid
valves, membrane dosing pumps or motor valves. When driving a
motor valve both relays are needed, relay 1 to open and relay 2 to
close the valve.
5.3.2.22 Parameter: Choose on of the following process values.
 Temperature
 Sample Flow
 Si 1
5.3.2.32 Settings: Choose the respective actuator:
 Time proportional
 Frequency
 Motor valve
5.3.2.32.1 Actuator = Time proportional
Examples of metering devices that are driven time proportional are
solenoid valves, peristaltic pumps.
Dosing is controlled by the operating time.
5.3.2.32.20 Cycle time: duration of one control cycle (on/off change).
Range: 0–600 Sec.
5.3.2.32.30 Response time: Minimal time the metering device needs to react.
Range: 0–240 Sec.
5.3.2.32.4 Control Parameters
Range for each Parameter same as 5.2.1.43, p. 84
5.3.2.32.1 Actuator = Frequency
Examples of metering devices that are pulse frequency driven are

the classic membrane pumps with a potential free triggering input.
Dosing is controlled by the repetition speed of dosing shots.
5.3.2.32.21 Pulse frequency: Max. pulses per minute the device is able to
respond to. Range: 20–300/min.
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5.3.2.32.1 Actuator = Motor valve

Dosing is controlled by the position of a motor driven mixing valve.
5.3.2.32.22 Run time: Time needed to open a completely closed valve
Range: 5–300 Sec.
5.3.2.32.32 Neutral zone: Minimal response time in % of the runtime. If the
requested dosing output is smaller than the response time, no
change will take place.
Range: 1–20 %
5.3.2.1 Function = Timer:
The relay will be activated repetitively depending on the
programmed time scheme.
5.3.2.24 Mode: Operating mode (interval, daily, weekly)
5.3.2.24 Interval
5.3.2.340 Interval: The interval can be programmed within a range
of 1–1’440 min.
5.3.2.44 Run Time: Enter the time the relay stays active.
Range: 5–32’400 Sec.
5.3.2.54 Delay: during run time plus the delay time the signal and control
outputs are held in the operating mode programmed below.
Range: 0–6’000 Sec.
5.3.2.6 Signal Outputs: Select operating mode of the signal output:
Cont.: Signal outputs continue to issue the measured value.
Hold: Signal outputs hold the last valid measured value.
Measurement is interrupted. Errors, except fatal errors,
are not issued.
Off: Signal outputs are switched off (set to 0 or 4 mA).
Errors, except fatal errors, are not issued.
5.3.2.7 Output/Control: Select operating mode of the controller output:

Cont.: Controller continues normally.
Hold: Controller continues based on the last valid value.
Off: Controller is switched off.
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5.3.2.24 daily
The relay contact can be activated daily, at any time of a day.
5.3.2.341 Start time: to set the start time proceed as follows:
1 Press [Enter], to set the hours.
2 Set the hour with the [ ] or [ ] keys.
3 Press [Enter], to set the minutes.
4 Set the minutes with the [ ] or [ ] keys.
5 Press [Enter], to set the seconds.
6 Set the seconds with the [ ] or [ ] keys.
Range: 00:00:00–23:59:59
5.3.2.44 Run Time: see Interval
5.3.2.54 Delay: see Interval
5.3.2.6 Signal Outputs: see Interval
5.3.2.7 Output/Control: see Interval
5.3.2.24 weekly
The relay contact can be activated at one or several days, of a
week. The daily starting time is valid for all days.
5.3.2.342 Calendar:
5.3.2.342.1 Start time: The programmed start time is valid for each of the
programmed days. To set the start time see 5.3.2.341, p. 90.
Range: 00:00:00–23:59:59
5.3.2.342.2 Monday: Possible settings, on or off
to
5.3.2.342.8 Sunday: Possible settings, on or off
5.3.2.44 Run Time: see Interval
5.3.2.54 Delay: see Interval
5.3.2.6 Signal Outputs: see Interval
5.3.2.7 Output/Control: see Interval
5.3.2.1 Function = Fieldbus:
The relay will be switched via the Profibus input. No further
parameters are needed.
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5.3.3.1 Function = End of Batch

This function is only available on relay 2. It is used to communicate
with canal switching instruments from third-party suppliers. The
relay closes for 1 sec. after each valid measurement. If End of
Batch is selected, no further selection is possible.
5.3.3.1 Function = Channel Selection
If the 2nd sample stream option is installed, relay 2 can be used to
indicate which channel is selected. No further parameters are
needed.
Relay 2 inactive: Channel 1 is selected
Relay 2 active: Channel 2 is selected
5.3.4 Input: The functions of the relays and signal outputs can be
defined depending on the position of the input contact, i.e. no
function, closed or open.
If <Channel Selection> in Menu < Installation>/<Sensors> is set to
“external”, the Input is set to “Active = no” and can be used to
switch the 2nd Sample Stream Option via an external device.
5.3.4.1 Active: Define when the input should be active:
The measurement is interrupted during the time the input is active.
No: Input is never active.
When closed: Input is active if the input relay is closed
When open: Input is active if the input relay is open
5.3.4.2 Signal Outputs: Select the operation mode of the signal outputs
when the relay is active:
Cont.: Signal outputs continue to issue the measured
value.
Hold: Signal outputs issue the last valid measured value.
Measurement is interrupted. Errors, except fatal
errors, are not issued.
Off: Set to 0 or 4 mA respectively. Errors, except fatal
errors, are not issued.
5.3.4.3 Output/Control: (relay or signal output):
Cont.: Controller continues normally.
Hold: Controller continues on the last valid value.
Off: Controller is switched off.
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5.3.4.4 Fault:
No: No message is issued in pending error list and the
alarm relay does not close when input is active.
Message E024 is stored in the message
list.
Yes: Message E024 is issued and stored in the mes-
sage list. The Alarm relay closes when input is
active.
5.3.4.5 Delay: Time which the instrument waits, after the input is
deactivated, before returning to normal operation.
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5.4 Miscellaneous
5.4.1 Language: Set the desired language.
Language
German
English
French
Spanish
5.4.2 Set defaults: Reset the instrument to factory default values in three
different ways:
Set defaults
no
Calibration
In parts
Completely
 Calibration: Sets calibration values back to default. All other
values are kept in memory.
 In parts: Communication parameters are kept in memory. All
other values are set back to default values.
 Completely: Sets back all values including communication
parameters.
5.4.3 Load Firmware: Firmware updates should be done by instructed
service personnel only.
Load Firmware
no
yes
5.4.4 Password: Select a password different from 0000 to prevent unau-
thorized access to the following menus:
5.4.4.1 Messages
5.4.4.2 Maintenance
5.4.4.3 Operation
5.4.4.4 Installation.
Each menu may be protected by a different password.
If you forgot the passwords, contact the closest SWAN representative.
5.4.5 Sample ID: Identify the process value with any meaning full text,
such as KKS number.
5.4.6 Line Break Detection: If activated, error message E028 is shown in
case of line break on signal outputs 1 and 2.
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5.5 Interface
Select one of the following communication protocols. Depending on
your selection, different parameters must be defined.
5.5.1 Protocol: Profibus

5.5.20 Device address: Range: 0–126
5.5.30 ID-Nr.: Range: Analyzer; Manufacturer; Multivariable
5.5.40 Local operation: Range: Enabled, Disabled
5.5.1 Protocol: Modbus RTU
5.5.31 Baud Rate: Range: 1200–115 200 Baud
5.5.41 Parity: Range: none, even, odd
5.5.1 Protocol: USB-Stick:
Only visible if an USB interface is installed. No further settings are
possible.
5.5.1 Protocol: HART
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Material Safety Data sheets
10. Material Safety Data sheets
10.1. Reagents
Catalogue No.: Part of Article No. A - 85.420. 560
Product name: OXYCON ON-LINE SILICA
Reagent 1a for AMI Silica
Ammonium heptamolybdate tetrahydrate
Reagent 1b for AMI Silica
Sodium hydroxide pellets
Reagent 2 for AMI Silica
Sulfuric acid 25 %
Reagent 3 for AMI Silica
Oxalic acid dihydrate
Reagent 4a for AMI Silica
Sulfuric acid 25 %
Reagent 4b for AMI Silica
Ammonium iron(II) sulfate hexahydrate
Catalogue No.: A85.142.400
Product name: Silica Standard 100ppm 100ml
Download The current Material Safety Data Sheets (MSDS) for the above list-
MSDS ed Reagents are available for downloading at www.swan.ch.
A-96.250.671 / 150517 95
AMI Silica
Default Values
11. Default Values

Operation:
Sensors: Filter Time Const.:..................................................................10 Sec
Hold after Cal.:.....................................................................300 Sec
Alarm Relay ...................................................................... same as in Installation
Relay 1 and 2 ...................................................................... same as in Installation
Input ...................................................................... same as in Installation
Logger Logger Interval:........................................................... Event Driven
Clear Logger: ................................................................................no
Installation:
Sensor Ref. Verification:.......................................................................0.235
Standard: .............................................................................100 ppb
Blank.....................................................................................0.0 ppb
Meas. interval ........................................................................ 10 Min
Channels.........................................................................................1
Channel Selection................................................................. internal
Signal Output 1 Parameter: ..................................................................................Si 1
Current loop: .....................................................................4 –20 mA
Function: .................................................................................. linear
Scaling: Range low: ..............................................................0.0 ppb
Scaling: Range high:..........................................................1.00 ppm
Signal Output 2 Parameter: ....................................................................Temperature
Current loop: .....................................................................4 –20 mA
Function: .................................................................................. linear
Scaling: Range low: ................................................................0.0 °C
Scaling: Range high:.............................................................50.0 °C
Alarm Relay Alarm Si 1:
Alarm high:.........................................................................5.00 ppm
Alarm low: .............................................................................0.0 ppb
Hysteresis: .............................................................................10 ppb
Delay:.......................................................................................5 Sec
Sample Temp.: Alarm High: .....................................................55 °C
Sample Temp.: Alarm Low: ........................................................5 °C
Sample Flow: Flow Alarm: .......................................................... yes
Sample Flow: Alarm High: ....................................................500 B/s
Sample Flow: Alarm Low: .........................................................5 B/s
Case temp. high:......................................................................65 °C
Case temp. low: .........................................................................0 °C
Relay1 and 2 Function: .......................................................................... limit upper
Parameter: ..................................................................................Si 1
96 A-96.250.671 / 150517
AMI Silica
Default Values
Setpoint: .............................................................................. 1.0 ppm

Hysteresis:............................................................................. 10 ppb
Delay: .................................................................................... 30 Sec
If Function = Control upw. or dnw:
Parameter:.................................................................................. Si 1
Settings: Actuator: .......................................................... Frequency
Settings: Pulse Frequency: .............................................120/min.
Settings: Control Parameters: Setpoint:......................... 1.00 ppm
Settings: Control Parameters: P-band: .............................. 10 ppb
Settings: Control Parameters: Reset time:........................... 0 Sec
Settings: Control Parameters: Derivative Time: ................... 0 Sec
Settings: Control Parameters: Control Timeout:................... 0 Min
Settings: Actuator: ................................................ Time proportional
Cycle time: ............................................................................ 60 s
Response time: ..................................................................... 10 s
Settings: Actuator ......................................................... Motor valve
Run time: ............................................................................... 60 s
Neutral zone: ........................................................................... 5%
If Function = Timer:
Mode:.................................................................................... Interval
Interval: ................................................................................ 1 min
Mode: ........................................................................................daily
Start time:........................................................................ 00.00.00
Mode:..................................................................................... weekly
Calendar; Start time: ....................................................... 00.00.00
Calendar; Monday to Sunday:.................................................. Off
Run time: ............................................................................... 10 Sec
Delay: ...................................................................................... 5 Sec
Signal output:............................................................................. cont
Output/Control: .......................................................................... cont
Input Active............................................................................ when closed
Signal Outputs ........................................................................... hold
Output/Control .............................................................................. off
Fault.............................................................................................. no
Delay ..................................................................................... 10 Sec
Miscellaneous Language:............................................................................. English
Set default: ................................................................................... no
Load firmware:.............................................................................. no
Password:........................................................... for all modes 0000
Sample ID:....................................................................... - - - - - - - -
Line break detection ..................................................................... no
Interface Protocol: ...................................................... depending on interface
A-96.250.671 / 150517 97
AMI Silica
Index
12. Index
A Interface
Alarm Relay . . . . . . . 10, 30 HART . . . . . . . . ... 35
Ammonium Ferrous Sulfate Interface Modbus . . . . ... 34
Reagent 4 . . . . . . . . 48 Interface Profibus DP . ... 34
Ammoniummolybdate Interface RS485 . . . . 34–35
Reagent 1 . . . . . . . . 48 Interface USB . . . . . . . . . 35
Application Range . . . . . . . 9 Interrupt measurement . . . 38
C L
Cable thicknesses ...... 26 Log Interval .......... 78
Calendar . . . . . . ...... 90 Logger . . . .......... 78
Changing values . ...... 43
Constant Head . . ...... 51 M
Manual Filling . . . . . . ... 76
D Measurement cycle . . ... 12
Default Values ........ 96 Measurement interval . ... 47
Messumformer . . . . . ... 16
E Mode External . . . . . ... 80
Electrical wiring . ....... 17 Mode Fieldbus . . . . . ... 80
Error List . . . . . ....... 62 Mode Internal . . . . . . ... 79
Mounting requirements ... 18
F
Fill System . . . . . . .... 76 O
Filter Time Constant . .... 78 On-site requirements . 15, 17
Fluidics . . . . . . . . .... 10 Oxalic Acid
Reagent 3 . . . . . 46, 48
G
Grab Sample ......... 44 P
Power Supply . . . . . . 14, 29
Power-up . . . . . . . . . . . 17
H Program Access . . . . . . . 39
Hold after Cal . ........ 78 Programming . . . . . . . . . 38
I R
I/O State . . . . . . . . . . . . 76 Reagent 1
Input . . . . . . . . . 10, 30, 91 Ammoniummolybdate . 48
Instrument Setup . . . . . . . 17
98 A-96.250.671 / 150517
AMI Silica
Index
Reagent 2 Signal Outputs . . . . 9, 33, 38

Sulfuric Acid. . . . . . . 48 Signal Sequencer . . . . . . 84
Reagent 3 Silica Measurement . ..... 9
Oxalic Acid . . . . . . . 48 Simulation . . . . . . . . . . 77
Reagent 4 Sulfuric Acid
Ammonium Ferrous Sulfate 48 Reagent 2 . . . . .. 46, 48
Reagent consumption . . . . 47
Reagents . . . . . . . . . . . 17 T
Relay . . . . . . . . . . . . . . 9 Terminals . 28, 30–31, 33–34
Run-in period . . . . . . . . . 17 Transmitter . . . . . . . . . . 16
S W
Safety Features ....... 10 Wire . ............. 26
Sample Flow
Establish. . ....... 37
A-96.250.671 / 150517 99
AMI Silica
Notes
13. Notes
100 A-96.250.671 / 150517

AMI Silica
Notes
A-96.250.671 / 150517 101

AMI Silica
SWAN
is represented worldwide by subsidiary companies
and distributors.
cooperates with independent representatives

all over the world.
SWAN Products
Analytical Instruments for:
High Purity Water
Feedwater, Steam and Condensate
Potable Water
Pool and Sanitary Water
Cooling Water
Waste Water and Effluents
Made in Switzerland
102 A-96.250.671 / 150517

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AMI Silica

Version 6.20 and higher

Title: Monitor AMI Silica Operator’s Manual

00 Nov. 2011 First Edition

01 Nov.2013 Main board V2.4, Update to Firmware Release 5.40

02 Okt. 2014 Update to Firmware Release 5.41, description of

03 June 2016 Main board V2.5, Update to Firmware Release 6.00

© 2016, SWAN ANALYTISCHE INSTRUMENTE AG, Switzerland, all rights reserved

subject to change without notice

AMI Silica - Operator’s Manual

1.1 Warning Notices

Your life or physical wellbeing are in serious danger if such

Severe injuries or damage to the equipment can occur if such

Damage to the equipment, minor injury, malfunctions or incor-

Mandatory The importance of the mandatory signs in this manual.

Warning Signs The importance of the warning signs in this manual.

Electrical shock hazard

1.2 General Safety Regulations

Electrical Shock Hazard

For safe instrument installation and operation you must read

Only SWAN trained and authorized personnel shall perform the

1.3 Restrictions for use

Alarm Relay One potential free contact.

A Constant head K Reagent 2

Measurement The quantities of the reagents are precisely defined by a certain

1 The sample inlet is closed by activation of the solenoid valve [C].

14 6-way valve in position 5:

A measuring cycle takes 10 minutes.

7.5 min 2.5 min

X Measuring steps on time axis Reagent 2

2.1 Instrument Specification

Power Supply Voltage: 100–240 VAC (± 10%)

NOTICE: No oil, no grease, no sand.

Silica Measuring method: colorimetric, molybdosilicat method

Dimensions Panel: 400 x 850 x 160 mm

2.2 Instrument Overview

A Transmitter K Flow regulating valve

Check Instrument’s specification must conform to the National Electri-

On-site  100 - 240 VAC ( 10%), 50/60 Hz ( 5%) or 24 DC ( 10%),

Installation  Mounting of Instrument Panel, p. 18

Reagents  Prepare the reagents. Refill or replace Reagents, p. 46

Power-up Perform exactly in this order:

Instrument Program all parameters for external devices (interface, record-

Run-in period Let the instrument run continuously for 1 h.

3.2 Mounting of Instrument Panel

3.3 Install the Constant Head

3.4 Connect Sample and Waste

3.4.1 Sample Inlet

3.4.2 Sample Outlet

A Tube from constant head

3.5 Install the 2nd Sample Stream Option

A Block housing I Sample stream 1

1 Stop operation according to Stop of Operation for Maintenance,

1 Remove the plug [A] from the cable gland [B].

3.6 Install the AMI Sample Sequencer

With the AMI Sample Sequencer connected, the

Internal, see chap. 9, Mode Internal, p. 79

3.6.1 Sample connection with 2nd sample stream

3.7 Electrical Connections