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    Table NMR

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    Table NMR

    Uploaded by

    karachi85
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    6 views2 pages

    Table NMR

    Uploaded by

    karachi85

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    © All Rights Reserved
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    of 2

    H-No 8a 8b 8c 8d

    Triazole C-H 7.77, s


    H-2 & H-6 7.68, d, J=
    Benzamide
    H-3 & H-5 6.96, d, J=
    Benzamide
    N-H amide 6.07, t , J =
    H-1 galactopyranose 5.47, d, J=
    5.21 (s, 2H)
    H-3 and H-6b galactopyranose 4.61, m
    H-5 galactopyranose 4.42 (dd, J= and
    H-2 galactopyranose 4.30, dd, J= 4.8 and 2.5-,
    H-4 and H-6a galactopyranose 4.15, m
    CO-CH2- amide alkyl chain 3.38 (q, J=
    CO-CH2-CH2- amide alkyl chain 1.56, pentate, J=
    CH3 x 4 isopropylidine 1.45, 1.33, 1.32, 1.25, each
    s
    amide alkyl chain CH2 x 10 1.68, 1.22, broad singlet
    alkyl chain terminal CH3 0.84 (t, J=
    13
    C-NMR (CDCl3, 125 MHz)  ppm:

    C-No 8a 8b 8c 8d
    (NH-C=O) 166.9
    Galactopyranoside
    C-1 96.2
    C-2 70.3
    C-3 70.7
    C-4 71.1
    C-5 67.2
    C-6 61.9
    Isopropylidine:
    (O-C(CH3)2-O) 109.9 ad 109.0
    CH3 x4 25.9, 25.8,
    24.8, 24.3
    Triazole:
    C-4’ 143.2
    C-5’ 128.5
    P-hydroxybenzoate:
    C-1” 160.6
    C-3” and C-5” 128.5
    C-4” 127.6
    C-2” and C-6” 114.6
    NH-CH2 50.6
    NH-CH2-CH2 40.03
    NH-(CH2)2-CH2 31.86
    NH-(CH2)3-CH2 29.7
    NH-(CH2)4-CH2 29.6
    NH-(CH2)5-CH2 29.5
    NH-(CH2)6-CH2 29.5
    NH-(CH2)7-CH2 29.5
    NH-(CH2)8-CH2 29.3
    NH-(CH2)9-CH2 26.9
    NH-(CH2)10-CH2 22.6
    - CH3 14.07

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