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    Nuclear Magnetic Resonance (NMR) Spectroscopy - Instrumentation - Microbe Notes

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    Nuclear magnetic resonance (NMR) spectroscopy observes local magnetic fields around atomic nuclei using electromagnetic radiation in the radio frequency region. NMR spectroscopy works by placing a sample in a magnetic field and exciting the nuclei with radio waves, which are detected by sensitive receivers. This provides detailed structural information about organic compounds and their functional groups. The instrumentation of NMR spectroscopy includes a permanent magnet, magnetic coils, a sweep generator, radio frequency transmitter and receiver, and readout systems to analyze the detected signals.

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    Nuclear Magnetic Resonance (NMR) Spectroscopy - Instrumentation - Microbe Notes

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    jimgitonga
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    Nuclear magnetic resonance (NMR) spectroscopy observes local magnetic fields around atomic nuclei using electromagnetic radiation in the radio frequency region. NMR spectroscopy works by placing a sample in a magnetic field and exciting the nuclei with radio waves, which are detected by sensitive receivers. This provides detailed structural information about organic compounds and their functional groups. The instrumentation of NMR spectroscopy includes a permanent magnet, magnetic coils, a sweep generator, radio frequency transmitter and receiver, and readout systems to analyze the detected signals.

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    Nuclear magnetic resonance (NMR) spectroscopy observes local magnetic fields around atomic nuclei using electromagnetic radiation in the radio frequency region. NMR spectroscopy works by placing a sample in a magnetic field and exciting the nuclei with radio waves, which are detected by sensitive receivers. This provides detailed structural information about organic compounds and their functional groups. The instrumentation of NMR spectroscopy includes a permanent magnet, magnetic coils, a sweep generator, radio frequency transmitter and receiver, and readout systems to analyze the detected signals.

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    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    1K views2 pages

    Nuclear Magnetic Resonance (NMR) Spectroscopy - Instrumentation - Microbe Notes

    Uploaded by

    jimgitonga
    Nuclear magnetic resonance (NMR) spectroscopy observes local magnetic fields around atomic nuclei using electromagnetic radiation in the radio frequency region. NMR spectroscopy works by placing a sample in a magnetic field and exciting the nuclei with radio waves, which are detected by sensitive receivers. This provides detailed structural information about organic compounds and their functional groups. The instrumentation of NMR spectroscopy includes a permanent magnet, magnetic coils, a sweep generator, radio frequency transmitter and receiver, and readout systems to analyze the detected signals.

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    © All Rights Reserved
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    Download as pdf or txt
    of 2

    9/20/21, 11:32 AM Nuclear Magnetic Resonance (NMR) Spectroscopy - Instrumentation - Microbe Notes

    Nuclear Magnetic Resonance (NMR) Spectroscopy


    November 12, 2018 by Sagar Aryal

    Table of Contents
    Principle of Nuclear Magnetic Resonance (NMR) Spectroscopy
    Working of Nuclear Magnetic Resonance (NMR) Spectroscopy
    Instrumentation of Nuclear Magnetic Resonance (NMR) Spectroscopy
    Applications of Nuclear Magnetic Resonance (NMR) Spectroscopy
    References

    Nuclear magnetic resonance spectroscopy, most commonly known as NMR


    spectroscopy or magnetic resonance spectroscopy (MRS), is a spectroscopic technique
    to observe local magnetic fields around atomic nuclei. 
    It is a spectroscopy technique which is based on the absorption of electromagnetic
    radiation in the radio frequency region 4 to 900 MHz by nuclei of the atoms.
    Over the past fifty years, NMR has become the preeminent technique for determining
    the structure of organic compounds.
    Of all the spectroscopic methods, it is the only one for which a complete analysis and
    interpretation of the entire spectrum is normally expected.

    Principle of Nuclear Magnetic Resonance (NMR) Spectroscopy


    1. The principle behind NMR is that many nuclei have spin and all nuclei are electrically
    charged. If an external magnetic field is applied, an energy transfer is possible between
    the base energy to a higher energy level (generally a single energy gap).
    2. The energy transfer takes place at a wavelength that corresponds to radio frequencies
    and when the spin returns to its base level, energy is emitted at the same frequency.
    3. The signal that matches this transfer is measured in many ways and processed in order
    to yield an NMR spectrum for the nucleus concerned.
    https://microbenotes.com/nuclear-magnetic-resonance-nmr-spectroscopy/ 1/2
    9/20/21, 11:32 AM Nuclear Magnetic Resonance (NMR) Spectroscopy - Instrumentation - Microbe Notes

    Working of Nuclear Magnetic Resonance (NMR) Spectroscopy


    The sample is placed in a magnetic field and the NMR signal is produced by excitation
    of the nuclei sample with radio waves into nuclear magnetic resonance, which is
    detected with sensitive radio receivers.
    The intramolecular magnetic field around an atom in a molecule changes the
    resonance frequency, thus giving access to details of the electronic structure of a
    molecule and its individual functional groups.
    As the fields are unique or highly characteristic to individual compounds, NMR
    spectroscopy is the definitive method to identify monomolecular organic compounds.
    Besides identification, NMR spectroscopy provides detailed information about the
    structure, dynamics, reaction state, and chemical environment of molecules.
    The most common types of NMR are proton and carbon-13 NMR spectroscopy, but it is
    applicable to any kind of sample that contains nuclei possessing spin.

    Instrumentation of Nuclear Magnetic Resonance (NMR)


    Spectroscopy
    1. Sample holder

    Glass tube with 8.5 cm long, 0.3 cm in diameter.


    2. Permanent magnet

    It provides homogeneous magnetic field at 60-100 MHZ 


    3. Magnetic coils

    These coils induce magnetic field when current flows through them
    4. Sweep generator

    To produce the equal amount of magnetic field pass through the sample
    5. Radio frequency transmitter

    A radio transmitter coil transmitter that produces a short powerful pulse of radio waves
    6. Radio frequency receiver

    A radio receiver coil that detects radio frequencies emitted as nuclei relax to a lower
    energy level 
    7. Read out systems

    A computer that analyses and record the data.

    https://microbenotes.com/nuclear-magnetic-resonance-nmr-spectroscopy/ 2/2

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