Universiti Kuala Lumpur Malaysian Institute of Chemical & Bioengineering Technology

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CLB 21204 TRANSPORT PROCESS PRINCIPLE

UNIVERSITI KUALA LUMPUR


MALAYSIAN INSTITUTE OF CHEMICAL
& BIOENGINEERING TECHNOLOGY
LABORATORY REPORT COVER PAGE
Title of experiment: Experiment 1– Bubble Cap Distillation Process
Group number: Group 1 Section: L01-P1
Date of experiment: 21/4/2021 Date of submission: 30/5/2021
Name & ID No.: 1. Nur Hayati Binti Abd Halim 55217220001
2. Nur Sabrina Binti Zuhairi 55217220006
3. Nur Syahmina Afiqah Bt Amirudin 55217220009
4. Nur Zakiah Binti Roslan 55216220007
5. Ilyas Fikri Binti Mohd Said 55213220037
*Penalty:
 For any late of submission, the mark will be reduced by 5% per day.
 Plagiarism will not be tolerated and will be given ZERO.
Satisfactory Good Excellen Marks
Unacceptable Poor
Criteria (3) (4) t
(1) (2)
(5)
X1 X1 X1 X1 X1
Report format (5%)
1.Organization of the report.
X2 X2 X2 X2
X2
Summary (10%) – max 1 page
1.Brief review on the objectives of the
experiment, major findings and significant
conclusion.

Objectives (5%) X1 X1 X1 X1 X1
1.State the objectives of the experiment in
point form.
X2 X2 X2 X2
Introduction & Theory (10%) – max 2 X2
pages
1. State the background to the experiment
conducted.
2. Summary of theories including
formulations related to the experimental
work.
X2 X2 X2 X2 X2
Data & Results (10%)
1. Data are presented as deemed suitable
with complete labels and units.
X8 X8 X8 X8 X8
Analysis & Discussion (40%)
1. Explanations of the referred table and
figure are presented after the table and
figure.
2. Discuss on the findings and relations to
the theory and objective of experiment.
X1 X1 X1 X1 X1
Conclusion (5%)
1.Summary of the results to relate the
findings with the theory applicable to the
experimental (relate with objectives).
X1 X1 X1 X1 X1
Recommendation (5%)
1.Suggest improvements in apparatus or
measurement procedure, or experimental
procedures for future.
X1 X1 X1 X1 X1
References (5%)
1. Cite references in the text.
2. References taken from books, journals
and articles.
X1 X1 X1 X1 X1
Appendices (5%)
1. Put raw data (signed) and sample
calculation.
TOTAL (100%)

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CLB 21204 TRANSPORT PROCESS PRINCIPLE

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CLB 21204 TRANSPORT PROCESS PRINCIPLE

1.0 SUMMARY

2.0 OBJECTIVES

3.0 INTODUCTION & THEORY

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CLB 21204 TRANSPORT PROCESS PRINCIPLE

4.0 DATA & RESULTS

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CLB 21204 TRANSPORT PROCESS PRINCIPLE

Graph 1: Calibration Curve Graph

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CLB 21204 TRANSPORT PROCESS PRINCIPLE

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CLB 21204 TRANSPORT PROCESS PRINCIPLE

Reflux ratio = 1.0

Rotameter reading R1 (L/hr) = 1.6

Rotameter reading R2 (L/hr) = 1.6

Temperature T4 (oC) =-

Temperature T2 (oC) = 97.0

Time, t TOP PRODUCT BOTTOM PRODUCT


(min)
Refractive index Mole fraction Refractive index Mole fraction
(RI) (RI)

0 1.358 0.535 1.334 0.03

5 1.359 0.620 1.332 0.02

10 1.360 1.00 1.332 0.02

15 1.360 1.00 1.331 0.02

20 1.360 1.00 1.331 0.02

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CLB 21204 TRANSPORT PROCESS PRINCIPLE

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CLB 21204 TRANSPORT PROCESS PRINCIPLE

Graph 2: Mole Fraction of Ethanol in Vapor (Y) VS Mole Fraction of Ethanol in Liquid (X) for 1.0

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CLB 21204 TRANSPORT PROCESS PRINCIPLE

Reflux ratio = 2.0

Rotameter reading R1 (L/hr) = 2.0

Rotameter reading R2 (L/hr) = 1.0

Temperature T4 (oC) =-

Temperature T2 (oC) = 100

Time, t TOP PRODUCT BOTTOM PRODUCT


(min)
Refractive index Mole fraction Refractive index Mole fraction
(RI) (RI)

0 1.359 0.620 1.332 0.02

5 1.359 0.620 1.332 0.02

10 1.358 0.532 1.332 0.02

15 1.357 0.47 1.332 0.02

20 1.357 0.47 1.331 0.00

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CLB 21204 TRANSPORT PROCESS PRINCIPLE

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CLB 21204 TRANSPORT PROCESS PRINCIPLE

Graph 3: Mole Fraction of Ethanol in Vapor (Y) VS Mole Fraction of Ethanol in Liquid (X) for 2.0

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CLB 21204 TRANSPORT PROCESS PRINCIPLE

5.0 ANALYSIS & DISCUSSION

6.0 CONCLUSION

7.0 RECOMMENDATION

8.0 REFERENCE

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CLB 21204 TRANSPORT PROCESS PRINCIPLE

9.0 APPENDICES

9.1 DATA PROPERTIES OF ETHANOL AND WATER

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CLB 21204 TRANSPORT PROCESS PRINCIPLE

9.2 CALCULATION MOLE FRACTION OF TABLE 1 (PART A)

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