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The document discusses different types of gases, pressures, components of vacuum systems, and mass spectrometer leak detection testing procedures.

Absolute pressure, gauge pressure, and vacuum pressures are discussed as well as units of measurement like torr and microns of mercury.

A mass spectrometer leak detection system consists of a mass spectrometer, roughing pump, diffusion pump, and cold trap to create high vacuum and detect tracer gases.

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MASS SPECTROMETER TESTING METHOD


LEVEL I – QUESTIONAIRE

1. A vapor is best defined as :


a. water in a test system
b. a substance which, though present in the gaseous phase, exists as
a liquid at room temperature
c. a substance in the gaseous state whose temperature is above its
critical temperature
d. a substance in the liquid state whose temperature is below its
critical temperature

2. Gauge pressure is :
a. the harmonic pressure within a gage
b. atmosphere pressure plus absolute pressure
c. the difference between absolute and atmosphere pressure
d. a sum of the partial pressures of air at standard temperature and
pressure

3. All leak testing methods are dependent upon :


a. barometric pressure
b. gas or liquid flow
c. mass spectrometer analysis
d. mean free paths of helium flow

4. A type of virtual leak caused by the slow release of absorbed or


entrapped tracer gas in a helium mass spectrometer vacuum
system is a :
a. hang-up
b. condenser
c. getter
d. molecular leak

5. The sensitivity of a mass spectrometer leak detector system is the


mass flow rate of tracer gas :
a. that gives a maximum measurable signal
b. that gives a minimum measurable signal
c. at standard temperature and pressure
d. in a leak

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6. As the required sensitivity of a leak test increases, the cost of the


test :
a. Decreases
b. remains constant
c. increases
d. decreases exponentially

7. Which of the following can be considered a major class of mass


spectrometer leak testing?
a. static test
b. dynamic test
c. both a and b
d. none of the above

8. Out gassing is defined as :


a. the removing of the free gas from a system
b. the spontaneous evolution of gas from a material in a vacuum
c. the spontaneous conversion of a gas to a liquid
d. removing the vacuum

9. Vacuum bake-out is defined as the :


a. heating of a system to remove water vapor
b. degassing of a vacuum system by heating
c. use of a halide torch to boil off liquids in the system
d. heating of liquid nitrogen in the cold trap by condensable vapors

10. A material which is included in a vacuum system for removing gas by


absorption is called:
a. A getter
b. A collector
c. An orifice
d. A molecularizer

11. The diffusion pump and mechanical forepump in a MSLD system:


a. Use the same type of oil
b. Use different types of oil
c. Operate using the same motor
d. Use the same principal of operation

12. Diffusion pumps generally warm up:


a. Instantly
b. In ten to twenty minutes
c. After the system is below 1 mm mercury
d. Diffusion pumps do not require warm up

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13. When calibrating a helium mass spectrometer instrument sensitivity,


which one of the following statements is not true ?
a. the filament must be “ON”
b. the instrument must be connected to the system being tested
c. the standard leak valve must be connected to the port of the
instrument
d. the standard leak valve must be open

14. The condition of the oil in the forepump of a vacuum system is


important because:
a. The pump will not be lubricated properly
b. The limiting forepressure of the diffusion pump may be exceeded
c. The water introduced will rust the pump internals
d. All of the above

15. The helium mass spectrometer detector probe pressure test


technique is :
a. a quantitative test
b. a qualitative test
c. a semiautomatic test
d. none of the above

16. When performing a tracer probe mass spectrometer vacuum test, it is


desirable to :
a. pressure test the system first
b. have a slight draft blowing across the surface of the test objest to
distribute the tracer gas evenly
c. perform the test in a still air environment
d. rotate the vessel constantly during the test

17. In vacuum systems, a mechanical pump is used in a series with the


diffusion pump because the :
a. mechanical pump achieves a lower pressure
b. diffusion pump uses fractioning oil
c. diffusion pump will not discharge against atmospheric pressure
d. mechanical pump handles condensable vapors

18. If the HMS leak detector’s forepump belt breaks while the instrument
is in operation and unattended:
a. No damage will occur since the automatic protection system will be
activated
b. The vacuum system will stay at low vacuum as long as the cold trap
remains filled
c. Backstreaming of the diffusion pump oil vapors will occur
contaminating the system
d. The system will continue to function properly as long as the
diffusion pump is operating

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19. 300 psig is approximately equal to :


a. 101 kPa (1 atmosphere of pressure)
b. 40 kPa (300 mm Hg)
c. 2.1 MPa (21 atmospheres of pressure)
d. none of the above

20. In the normal sequence of starting up a mass spectrometer leak


detector unit with a mechanical forepump and diffusion pump, what
is the start up sequence ?
a. the diffusion pump is started first
b. the mechanical pump is started first
c. both pumps are started simultaneously
d. the starting sequence is not important

21. Increasing the length of a tube connecting the mass spectrometer


leak detector to an evacuated test object may:
a. cause a decrease in the system’s response time
b. cause an increase in the system’s response time
c. have no effect on the system’s response time
d. none of the above

22. When vacuum testing large volumes with a mass spectrometer leak
detector, the response and cleanup times depend on :
a. the volume of the system under test
b. the conductance of the connecting tubes
c. the pumping speed of the mass spectrometer leak detector unit
d. all of the above

23. Operating the mass spectrometer tube at a pressure greater than that
recommended by the manufacturer is undesirable because :
a. too many electrons will be produced
b. the spectrometer filament may burn out prematurely
c. the diffusion pump cannot handle it without wear
d. the pressure relay switches will arc

24. When connecting an auxiliary vacuum pump system to a test vessel,


the pumbing lines should be kept as short as possible because the :
a. out gassing effect will be reduced
b. conductance of the system is inversely proportional to the length of
the tubing
c. leak detector should be as close to the test system as possible
d. pumps will run smoother

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25. The minimum leakage detectable in a helium mass spectrometer leak


testing system changes when a continuous parallel vacuum auxiliary
pump is used according to the :
a. position of the pump in the system
b. ratio of the throughput of the auxiliary to that of the leak detector
c. design of the cold trap
d. type of throttle valve used

26. The accumulation technique of helium mass spectrometer leak


testing is a:
a. Semiquantitative test
b. Static quantitative test
c. Qualitative test
d. Both b and c
27. It is desirable that a system being helium mass spectrometer leak
tested should have:
a. A long response time
b. A short response time
c. A fluctuating time constant
d. None of the above

28. When performing a helium mass spectrometer detector probe test


technique, it is :
a. highest to the lowest areas in the system
b. farthest to the nearest areas from the instrument
c. most difficult to the easiest areas to test
d. lowest to the highest areas in the system

29. When using the mass spectrometer leak detector probe test
technique, it is :
a. difficult to detect small leaks that are close to large leaks
b. impossible to segregate leaks
c. desirable to have a draft blowing across the test surface
d. simple to accurately size detected leaks

30. A vessel designed to hold liquid nitrogen when inserted into a


vacuum system is called a:
a. Bell jar
b. Cold cathode tube
c. Cold trap
d. Condenser

31. A vacuum pump using a vapor jet as the pumping means is called a :
a. mechanical vacuum pump
b. cold trap
c. diffusion pump
d. fission pump

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32. The percentage of helium in air is approximately :


a. the same as nitrogen
b. 0.0004%
c. 1%
d. 21%

33. The area leak tested must be free of :


a. Oil
b. Grease
c. Paint
d. all of the above

34. Tracer gas ions in a helium mass spectrometer leak detector are
separated from the remainder of the ion beam by the :
a. ion collector
b. magnetic field
c. hot tungsten filament
d. cold trap

35. The evacuation of the test object to the point at which its volume can
be exposed to a MSLD system is called the:
a. Diffusion cycle
b. Vacuum cycle
c. Roughing cycle
d. Pressurizing cycle

36. The gage that is used to monitor the pressure in the high vacuum
section of a mass spectrometer leak detector is called a :
a. cold-cathode discharge gage
b. Bourdon pressure-vacuum gage
c. Pirani gage
d. bulk pressure gage

37. The mass spectrometer vacuum gage that is used to monitor the
pressure during the roughing cycle is called a :
a. cold-cathode discharge gage
b. thermal conductivity gage
c. Bourdon pressure meter
d. bulk pressure gage

38. Which of the following factors would affect the sensitivity of a mass
spectrometer leak detector?
a. use of a remote control system
b. the pumping speed of the mass spectrometer leak detector vacuum
system
c. design of the roughing pump
d. type of throttle valve used

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39. Background signal in a mass spectrometer leak detector testing


refers to:
a. an output signal of the mass spectrometer leak detector caused by
any reason other than leakage
b. noise level above 70 dB through the detector
c. signal created by the mechanical forepump
d. noise created by stressing the part in pressure testing

40. Which of the following is the best definition of the “torr”?


a. 133 Pa ( 1 mm Hg)
b. 1 atmosphere
c. 760 mm Hg
d. 101 kPa (14.7 psig)

41. When dynamic mass spectrometer vacuum testing:


a. The system analyzes collected samples
b. The system is in motion
c. The system is in motion
d. The system is being continually pumped
e. None of the above

42. The cold cathode pressure gauge can be damaged by:


a. An extended time at pressure below 0.01 microns
b. An extended time at pressure below 0.2 microns
c. A high output meter reading
d. A low ionization current.

43. Increasing probing speed over the area being tested will result in :
a. an increase in response time
b. an increase in test sensitivity
c. a decrease in test sensitivity
d. a decrease in instrument sensitivity

44. The scale of a mass spectrometer leak detector output meter reads in :
a. SCFM
b. micrometers (µm)
c. torr (µm Hg)
d. none of the above

45. The purpose of a mass spectrometer tube is to :


a. measure tracer gas content in the test sample
b. analyze total gas content in the test sample
c. pump tracer gas ions
d. measure the internal pressure in the system

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46. For a mass spectrometer leak detector, what is the function of the
roughing pump?
a. to evacuate the system external to the mass spectrometer leak
detector
b. to pressurize the system external to the mass spectrometer leak
detector
c. to evaluate the internal mass spectrometer leak detector high
vacuum section
d. none of the above

47. The gas having the lowest molecular weight is :


a. Helium
b. Hydrogen
c. Nitrogen
d. Oxygen

48. Helium has an atomic mass of :


a. 2
b. 3
c. 4
d. 8

49. 760 torr are approximately equal to :


a. 10 kPa ( 76 mm Hg)
b. 101 kPa ( 760 mm Hg)
c. 2 Kpa ( 14.7 mm Hg)
d. none of the above

50. When performing a detector probe helium mass spectrometer test,


the test object is :
a. blanketed in helium
b. evacuated
c. pressurized
d. immersed in water

51. When completely shutting down a helium mass spectrometer, the


cold trap should:
a. Always removed, warmed-up cleaned and replaced if cryogenic
liquid was used
b. Never be removed because of the possibility of atmospheric
contamination
c. Be left in place to clean up as the diffusion pump cools down
d. Inspected but not cleaned unless discoloration is noticed on the
cold trap

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52. When the operating diffusion pump in a helium mass spectrometer is


suddenly exposed to high pressure for an extended period of time,
the result can be :
a. cracking of the diffusion pump oil
b. backstreaming oil vapor contamination of the cold trap
c. backstreaming oil vapor contamination of the entire high vacuum
system, including the analyzer tube
d. any of the above

53. The valve in a helium mass spectrometer which makes it possible to


manually connect the instrument to a higher pressure vacuum
system for the purpose of leak testing that system is usually called
the rouging valve or:
a. Test valve
b. Throttle valve
c. Accumulator valve
d. Pump valve

54. When leakages is indicated during a helium mass spectrometer test,


the operator should :
a. mark the approximate area where the signal was received and
continue testing
b. immediately vent the system, repair the leak, retest the repair, and
continue with the test
c. retest the same area to verify that the signal was really caused by
leakage, pinpoint and mark the source of that leakage for repairs,
temporarily seal it if necessary, and continue testing
d. peen it shut to eliminate the need for later repairs, and continue
testing
55. When starting up a helium mass spectrometer, the circuit breaker
repeatedly shuts off the test manifold rouging pump. Which of the
following could be the cause?
a. Low line voltage
b. Pump oil too cool
c. Roughing pump belt too tight
d. Any of the above

56. When performing a helium mass spectrometer tracer probe test, the
probing should be conducted in a sequence from the:
a. Highest to the lowest areas in the system
b. Farthest to the nearest areas from the instrument
c. Most difficult to the easiest areas to test
d. Lowest to the highest areas in the system

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57. In a helium mass spectrometer, exposure of the filament to high


pressure for extended periods of time wall:
a. Increase the life of the filament
b. Do little or no harm to the filament
c. Cause the filament to burn out
d. Increase the sensitivity of the filament

58. The section of a helium mass spectrometer that “detects” extremely


small quantities of helium gas, indicating leakage, is known in
general terms as the:
a. Spectrometer tube
b. Amplifier element
c. Ionizer element
d. Diffusion element

59. The safest effective and economical cryogenic fluid commonly used
in cold traps is liquid:
a. Oxygen
b. Argon
c. Nitrogen
d. Hydrogen

60. In the event of power failure while operating any helium mass
spectrometer, the first thing the operator should do is:
a. Look for some other source of electrical power
b. Disconnect the power cord to the machine so that when the power
comes back “ON”, the electronics will not come “ON” before the
roughing pump
c. Close the diffusion pump isolation (accumulator) valve
d. Vent the system to atmosphere, remove the cold trap and clean it.

61. When starting up a helium mass spectrometer from total shut down,
the high vacuum system diffusion pump takes about
__________________ to begin pumping after it is turned “ON”.
a. 2 minutes
b. 20 minutes
c. 60 minutes
d. 1-1/2 hours

62. When adding cryogenic liquid to a cold trap, one should:


a. Use a funnel and pour the liquid in rapidly so less will be lost by
evaporation
b. Just pour the liquid into the opening without the use of a funnel
c. Use the funnel and pour in a small amount, wait a few minutes and
slowly pour in the rest
d. Not worry about getting freeze burns from the liquid since it
evaporates very rapidly

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63. A micron of mercury pressure is equal to which of the following?


a. 760 mm mercury
b. 10-4 Torr
c. 10-3Torr
d. 1000 mm Hg
64. An absolute pressure of 50 microns Hg is the same as:
a. 5 x10-1Torr
b. 5 x10-4 mm Hg
c. 5 x10-2Torr
d. 50 Torr

65. A pressure of .000025 mm Hg can also be written as:


a. 25 x106 mm Hg
b. 2.5 x105 mm Hg
c. 2.5 x10-5 mm Hg
d. 2.5 x10-2 microns Hg
(5 10 2 ) (5 10 3 )
66. The product of equals:
(110 2 ) ( 2.5 10  4 )
a. 1 x 104
b. 5 x 103
c. 1 x 10-3
d. 2.5 x 104

67. A pressure of 1 mm Hg is the same as:


a. 100 microns Hg
b. 1000 microns Hg
c. 10-3 microns Hg
d. 1 micron Hg

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MASS SPECTROMETER TESTING METHOD


LEVEL I – QUESTIONAIRE ANSWERS

Q.NO. ANS Q.NO. ANS Q.NO. ANS


1 B 25 B 49 B
2 C 26 B 50 C
3 B 27 B 51 A
4 A 28 D 52 D
5 B 29 A 53 B
6 C 30 C 54 C
7 C 31 C 55 D
8 B 32 B 56 A
9 B 33 D 57 C
10 A 34 B 58 A
11 B 35 C 59 C
12 B 36 A 60 C
13 B 37 B 61 B
14 B 38 B 62 C
15 B 39 A 63 C
16 C 40 A 64 C
17 C 41 C 65 C
18 C 42 C 66 A
19 C 43 C 67 B
20 B 44 D
21 B 45 A
22 D 46 A
23 B 47 B
24 B 48 C

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