Designation: A1038 13

Standard Test Method for

Portable Hardness Testing by the Ultrasonic Contact
Impedance Method1
This standard is issued under the fixed designation A1038; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon () indicates an editorial change since the last revision or reapproval.

1. Scope* Determine the Precision of a Test Method

1.1 This test method covers the determination of compara-
tive hardness values by applying the Ultrasonic Contact 3. Terminology
Impedance Method (UCI Method). 3.1 Definitions:
1.2 The values stated in SI units are to be regarded as 3.1.1 calibrationdetermination of the specific values of
standard. No other units of measurement are included in this the significant operating parameters of the UCI instrument by
standard. comparison with values indicated by a standardized workbench
hardness tester or by a set of certified reference test pieces.
1.3 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the 3.1.2 surface finishall references to surface finish in this
responsibility of the user of this standard to establish appro- test method are defined as surface roughness (that is, Ra =
priate safety and health practices and determine the applica- average roughness value).
bility of regulatory limitations prior to use. 3.1.3 UCI hardness testa hardness testing method using a

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calibrated instrument by pressing a resonating rod with a
2. Referenced Documents defined indenter, for example, a Vickers diamond, with a fixed
2.1 ASTM Standards:2 force against the surface of the part to be tested.
A370 Test Methods and Definitions for Mechanical Testing 3.1.4 UCI methodUltrasonic Contact Impedance, a hard-
of Steel Products ness testing method developed by Dr. Claus Kleesattel in 1961
E10 Test Method for Brinell Hardness of Metallic Materials based on the measurement of the frequency shift of a resonat-
E18 Test Methods for Rockwell Hardness of Metallic Ma- ing rod caused by the essentially elastic nature of the finite area
terials of contact between the indenter and the test piece during the
E140 Hardness Conversion Tables for Metals Relationship penetration.
Among Brinell Hardness, Vickers Hardness, Rockwell
3.1.5 verificationchecking or testing the UCI instrument
Hardness, Superficial Hardness, Knoop Hardness, Sclero-
to ensure conformance with this test method.
scope Hardness, and Leeb Hardness
E177 Practice for Use of the Terms Precision and Bias in
ASTM Test Methods 4. Significance and Use
E384 Test Method for Knoop and Vickers Hardness of 4.1 The hardness of a material is a defined quantity having
Materials many scales and being dependent on the way the test is
E691 Practice for Conducting an Interlaboratory Study to performed. In order to avoid the creation of a new method
involving a new hardness scale, the UCI method converts into
common hardness values, for example, HV, HRC, etc.
1
This test method is under the jurisdiction of ASTM Committee A01 on Steel,
Stainless Steel and Related Alloys and is the direct responsibility of Subcommittee 4.2 The UCI hardness test is a superficial determination,
A01.06 on Steel Forgings and Billets. only measuring the hardness condition of the surface con-
Current edition approved Nov. 1, 2013. Published March 2014. Originally tacted. The results generated at a specific location do not
approved in 2005. Last previous edition approved in 2010 as A1038 10a. DOI:
10.1520/A1038-13. represent the part at any other surface location and yield no
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or information about the material at subsurface locations.
contact ASTM Customer Service at [email protected]. For Annual Book of ASTM
Standards volume information, refer to the standards Document Summary page on 4.3 The UCI hardness test may be used on large or small
the ASTM website. components at various locations. It can be used to make

*A Summary of Changes section appears at the end of this standard

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 A1038 13
hardness measurements on positions difficult to access, such as resonating rod. This shift is related to the size of the indent area
tooth flanks or roots of gears. (contact area of the indenter with the material). The size, in
turn, is a measure for the hardness of the test material at a given
A. GENERAL DESCRIPTION OF INSTRUMENTS modulus of elasticity, for example, HV(UCI) according to Eq
AND TEST PROCEDURE FOR UCI HARDNESS 1.
TESTING 5.3.2 Therefore, the frequency shift is relatively small for
5. Apparatus hard materials, because the indenter penetrates not very deep
into the test material leaving only a small indent.
5.1 Instruments used for UCI hardness testing generally 5.3.3 The frequency shift becomes larger if the indenter
consist of (1) a probe containing a rod with a defined indenter, penetrates deeper into the material, indicating medium
for example, a Vickers diamond, attached to the contacting end hardness, in accordance with the larger test indentations.

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per Test Method E384 (see Fig. 1), (2) vibration generating Analogously, the frequency shift becomes largest when soft
means, (3) vibration detecting means, (4) electronic means for materials are tested (see Fig. 2).
the numerical evaluation, and (5) a digital display, indicating 5.3.4 The instrument constantly monitors the resonance
the measured hardness number. frequency, calculates the frequency shift when the specified
5.2 UCI ProbesThere are different probes available for test load has been reached either after the internal switch has
UCI hardness testing. They typically cover static loads ranging triggered the corresponding measurement frequency in the case
from 1 N to 98 N. See also Appendix X1. They come also in of handheld probes or after a specific dwell time has been
different sizes with longer and shorter sensor rods for specials elapsed in the case of motor driven probes. The instrument
applications. And they are developed in two versions, that is, carries out the evaluation and calculations, and displays instan-
manually operated or equipped with a servo-motor for auto- taneously the hardness value, for example, HV(UCI).
matic testing. UCI Vickers (1)
5.3 Summary of Test MethodIn conventional workbench
F
hardness testing like Brinell or Vickers testing according to f 5 f ~ E effA ! and HV 5
A
Test Methods E10 and E384, the hardness value is determined
optically by the size of the indentation in the material generated _________________
by a certain test load, after the indenter has been removed. In
the mobile hardness test under applied load according to the 5.3.5 The frequency shift is a function of the indentation
UCI method, however, the size of the produced indents are not size of a defined indenter, for example, a Vickers diamond, at
determined optically. Instead the contact area is derived from a given modulus of elasticity of the measurement system.
the electronically measured shift of an ultrasonic resonance 5.3.6 Eq 1 describes the basic relation in comparison to the
frequency. To carry out the UCI test, a probe containing the rod definition of the Vickers hardness value: f = Frequency shift,
with the indenter is excited into a longitudinal ultrasonic A = indentation area, Eeff = effective elastic modulus (contains
oscillation of about 70 kHz by piezoelectric ceramicsthe the elastic constants of both the indenter and the test piece), HV
so-called zero frequency, which occurs when the indenter is = Vickers hardness value, F = Force applied in the hardness
vibrating in air. test.
5.3.1 A spring inside the probe applies the specified test 5.4 The Influence of the Elastic ConstantsAs can be seen
load, the vibrating tip penetrates into the material creating an in Eq 1, the frequency shift not only depends on the size of the
elastic contact, which results in a positive frequency shift of the contact area but also on the elastic moduli of the materials in
contact. To allow for differences in Youngs modulus, the

Legend:
T = Piezo Transducer
R = Receiver
O = Oscillating rod
V = indenter, for example, Vickers diamond
m = test material FIG. 2 Hardness Value versus Frequency Shift of the Oscillating
FIG. 1 Schematic Description of the UCI Probe Rod

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 A1038 13
instrument has to be calibrated for different groups of materi- 8.1.2 Penetration depth of the Vickers diamond pyramid for
als. After calibration, the UCI method can be applied to all a certain hardness (in HV) and test load (in N) id is shown in
materials, which have the corresponding Youngs modulus. Eq 2.
5.4.1 As manufactured, the UCI instrument usually has been 8.1.3 Table 1 provides the recommended minimal surface
calibrated on non-alloyed and low-alloyed steel, that is, certi- roughness for certain UCI probes that use a Vickers indenter. If
fied hardness reference blocks according to Test Method E384. surface preparation is necessary, care must be taken not to alter
Besides this, some instruments may be calibrated quickly, also the surface hardness by overheating or cold working. Any
at the test site, for metals such as high-alloyed steels, aluminum paint, scale or other surface coatings shall be completely
or titanium. removed. Failure to provide adequate surface finish will
produce unsteady readings. Coarse finishes will tend to lower
6. Calibration to Other Materials the measured value.
6.1 A test piece of the particular material is needed. The 8.2 Minimum ThicknessThin coatings or surface layers on
hardness value should then be determined with a standardized bulk material must have a minimum thickness of at least ten
workbench hardness tester like one for Vickers, Brinell or times of the indentation depth of the indenter used (see Fig. 3
Rockwell according to Test Methods and Definitions A370. It for a Vickers indenter) corresponding to the Bueckles rule:
is recommended to take at least five readings and calculate the Smin = 10 h.
average hardness value. Now carry out a set of at least five 8.3 Minimum Wall ThicknessDistinct reading variations
single UCI measurements on your test material according to may especially occur with a specimen thickness of less than
instructions in 10.6, adjust the displayed average value to the about 15 mm if the test material is excited to resonance or
before measured hardness of the material and thus find the sympathetic oscillations (for example, thin blocks, tubes, pipes,
calibration value which is necessary for further measurements etc.). Most disturbing are flexural vibrations excited by the
on this particular material in the desired hardness scale and vibrating tip. These should be suppressed by suitable means.
range. Sometimes attaching the test piece to a heavy metal block by
6.1.1 Some instruments allow storing all calibration data means of a viscous paste, grease or oil film suffices to quench
and adjustment parameters for hardness testing of different the flexural waves. Nevertheless, a minimum wall thickness of
materials. They can be recalled to the instrument as needed. 2 to 3 mm is recommended.
7. Comparison with Other Hardness Testing Methods 8.4 Influence of the OscillationThe UCI method is based
on measuring a frequency shift. Parts less than about 300 g can
7.1 As opposed to conventional low load hardness testers,
go into self-oscillating causing erroneous or erratic readings.
the UCI instruments do not evaluate the indentation size
Test pieces of weights less than the minimum or pieces of any
microscopically but electronically according to the UCI
weight with sections less than the minimum thickness require
method. The UCI method yields comparative hardness mea-
rigid support and coupling to a thick, heavier non-yielding
surements when considering the dependency on the elastic
surface to resist the oscillation of the UCI probe. Failure to
modulus of the test piece.
provide adequate support and coupling will produce test results
7.2 After removing the test force, an indentation generated lower or higher than the true hardness value.
by the UCI probe using a Vickers diamond as indenter and
8.5 Surface CurvatureTest pieces with curved surfaces
mounted in a test stand is practically identical to a Vickers
may be tested on either the convex or concave surfaces
indentation produced by a workbench tester of the same load.
providing that the radius of curvature of the specimens is
The indentation can be measured optically according to the
matched to the appropriate probe and probe attachment in order
standard Vickers test if care is taken to apply the force
to ensure a perpendicular positioning of the probe.
according to Test Method E384 and if a Vickers indenter is
used in the UCI probe. In this case special arrangements or 8.6 TemperatureThe temperature of the test piece may
probe attachments have to be used to provide verification of the affect the results of the UCI hardness test. However, if the
actual test force of the UCI probe. probe is exposed to elevated temperature for only the time of
measurement, measurements are possible at temperatures
8. Test Piece higher than room temperature, without influencing the perfor-
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mance of the UCI instrument.

8.1 Surface PreparationThe applied test force (that is, the
selected UCI probe) must not only match the application but 9. Verification of the Apparatus
also the surface quality and roughness of the material. While
smooth, homogeneous surfaces can be tested with low test 9.1 Verification MethodPrior to each shift or work period
loads, rougher and coarse-grained surfaces require test loads as the instrument shall be verified as specified in Part B. Any UCI
high as possible. However, the surface must always be free of hardness testing instrument not meeting the requirements of
any impurities (oil, dust, etc.) and rust. Part B shall not be used for the acceptance testing of products.
8.1.1 The surface roughness should not exceed 30 % of the
penetration depth (Ra 0.3 h) with: TABLE 1 Surface Finish for Different Test Loads
Test Load 98 N 50 N 10 N 3N

h @ mm# 5 0.062 3 Force @ N #

Hardness @ HV#
(2) Ra # 15 m # 10 m # 5 m # 2.5 m

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 A1038 13

FIG. 3 Vickers Diamond Penetration Depth for Different Test Loads from 1 N to 98 N

10. Procedure 10.4 Spacing IndentationAs per Test Method E384 the
10.1 Test ProcedureTo perform a hardness test, the probe center distance between two adjacent indents in relation to the
is connected to the indicating unit and the instrument is turned mean length of the diagonals must be (1) at least 3 times the
on. The probe is held firmly (using a probe grip if needed) with amount for steel, copper and copper alloys, and (2) at least 6
its axis in a perpendicular position relative to the test piece times the amount for light metals, lead, tin and their alloys. If
surface. Hold the probe with both hands to achieve the best two neighboring indents vary in size then the mean indent
possible result. Carefully exert steady pressure against the test diagonal of the larger indent must be used for calculation of the
piece during the loading phase. Make sure that the vertical minimum distance. No point shall be measured more than
probe position is maintained as long as the load is effective. once.
Some instruments indicate the end of the measurement by an 10.5 Reading of UCI InstrumentsHardness values can be
acoustic signal and display the hardness value instantaneously. read directly off the electronic display of the instrument. On
10.2 AlignmentTo prevent errors from misalignment some instruments, they can be displayed either as single figure
move the UCI probe with slow and steady speed. The probe showing the actual reading, or as average figure showing the
should be perpendicular with respect to the surface. The average of the hardness readings taken so far. Equivalent
maximum angular deviation from the perpendicular position hardness numbers on other scales can be obtained by using a
should be less than 5 degrees. Avoid twisting of the probe hardness conversion table (see also Section 12) or by calibra-
housing. There should be no lateral forces on the indenter. tion according to Section 6.
Therefore, avoid slip. 10.6 Number of MeasurementsFive measurements taken
in an area of approximately 650 mm2 shall constitute one test.
10.3 Test DirectionHardness testing according to the UCI
If the material being tested is considered to be inhomogeneous,
method generally can be carried out in any direction, without
ten measurements or more shall be made to constitute one test.
the necessity of corrections depending on the loading. There
may be an effect of the measurement direction on the hardness NOTE 1650 mm2 is an area approximately equal to 1 in.2.
measurement depending on the manufacturer and the test load 10.7 ReportingThe numerical hardness value shall be
of an UCI probe. This is due to the mass of the vibrating rod, followed by the symbol for the UCI test, HV(UCI) in the case
which may influence the test load in dependence on the of a Vickers reading with a suffix number denoting the test
direction of measurement; that is, the mass of the rod will force in kgf. Example: 446 HV(UCI) 10 = UCI hardness
increase the load when measuring top to bottom and vice versa. number of 466 under a force of 10 kgf. If numerical hardness
This should be considered especially for test loads below 10 N. values are presented in other scales by calibration according to
In this case the user has to verify the influence of test Section 6, they should analogously be reported as 45 HR-
orientation on the hardness reading depending on test load and C(UCI) or 220 HBW(UCI) etc. Reporting of converted values,
hardness of material. see Section 12.
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 A1038 13
11. Precision and Bias3,4 Certified Brinell Diameter
Certified Brinell
(3000 kg load - 10 mm
11.1 The precision of this test method is based on an Hardness
indenter)
interlaboratory study conducted in 2009. Each of 13 laborato- Test Block 1: 143 4.985 mm
0300142
ries tested five different materials. Every test result repre- Test Block 2: 194 4.325 mm
sents the average of five individual measurements per Para- 0729385
graph 10.6 of A1038. Laboratories reported two replicate test Test Block 3: 242 3.897 mm
0800213
results (from a single operator) for each of two different Test Block 4: 312 3.446 mm
analysis configurations (hand held and test stand). Practice 0722420
E691 was followed for the design and analysis of the data. Test Block 5: 377 3.144 mm
0723157
11.1.1 Repeatability limit (r)Two test results obtained
within one laboratory shall be judged not equivalent if they 11.4 To judge the equivalency of two test results, it is
differ by more than the r value for that material; r is the recommended to choose the test block closest in characteristics
interval representing the critical difference between two test to the test material.
results for the same material, obtained by the same operator 12. Hardness Scale Conversions
using the same equipment on the same day in the same
laboratory. 12.1 Conversion of Hardness NumbersSome instruments
allow also an automatic conversion of measured hardness
11.1.1.1 Repeatability limits are listed in Table 2 and Table
numbers into other hardness scales. Such conversion into other
3.
hardness values or also into tensile strength, measured in
11.1.2 Reproducibility limit (R)Two test results shall be
N/mm2, is made according to Hardness Conversion Tables
judged not equivalent if they differ by more than the R value
E140. Therefore, reporting of converted values and all limita-
for that material; R is the interval representing the critical
tions specified in Hardness Conversion Tables E140 do apply.
difference between two test results for the same material,
12.1.1 Conversion between hardness numbers is only pos-
obtained by different operators using different equipment in
sible with certain limitations. Hardness values, measured by
different laboratories.
different methods cannot be correlated by established math-
11.1.2.1 Reproducibility limits are listed in Table 2 and ematical relationships. The form and material of the indenter,
Table 3. the size of the indent and the measured number depend on the
11.1.3 The above terms (repeatability limit and reproduc- type of hardness test that is used.
ibility limit) are used as specified in Practice E177. 12.1.2 Conversion of one hardness number either into
11.1.4 Any judgment in accordance with statements 11.1.1 another hardness number or a unit of tensile strength may be
and 11.1.2 would have an approximate 95 % probability of inaccurate or inadmissible, depending on the material, its
being correct. preparation and its surface finish.
11.2 BiasSee Table 4. 12.2 Conversion to Tensile StrengthThe conversion into
11.3 The precision statement was determined through sta- the stress unit N/mm2 is limited to loads equal to or greater
tistical examination of 258 results, from 13 laboratories, on five than 98 N.
materials. These five materials were identified as follows: B. VERIFICATION OF UCI HARDNESS TESTING
INSTRUMENTS
13. Scope
13.1 Part B covers the verification procedure for UCI
3
Supporting data have been filed at ASTM International Headquarters and may hardness testing instruments by using suitable hardness refer-
be obtained by requesting Research Report RR:A01-1002. Contact ASTM Customer ence blocks. Direct verification has to be done by the manu-
Service at [email protected]. facturer.
4
Supporting data have been filed at ASTM International Headquarters and may
be obtained by requesting Research Report RR:A01-1003. Contact ASTM Customer
Service at [email protected].

TABLE 2 Test Stand: HV (UCI)

Repeatability Reproducibility
Test Repeatability Reproducibility
AverageA Standard Standard
Block Limit Limit
Deviation Deviation
x Sx Sr SR r R
0300142B 745.13
0729385 192.39 5.45 1.68 5.57 4.71 15.61
0800213 220.61 7.14 1.91 7.27 5.33 20.35
0722420 306.91 9.67 1.26 9.71 3.54 27.18
0723157 377.20 6.55 4.03 7.15 11.29 20.01
A
The average of the laboratories calculated averages.
B
Test Block 1 data was deleted from consideration when it was realized that it was fabricated from aluminum while blocks 2, 3, 4, and 5 were fabricated from steel. The
differing materials require individual calibration.
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TABLE 3 Test Stand: HV (UCI)
Repeatability Reproducibility
Test Repeatability Reproducibility
AverageA Standard Standard
Block Limit Limit
Deviation Deviation
x Sx Sr SR r R
0300142B 723.608
0729385 189.915 6.398 1.868 6.532 5.229 18.291
0800213 219.277 8.135 2.105 8.270 5.894 23.156
0722420 305.654 10.357 8.093 11.833 22.660 33.132
0723157 370.285 10.469 7.632 11.778 21.370 32.978
A
The average of the laboratories calculated averages.
B
Test Block 1 data was deleted from consideration when it was realized that it was fabricated from aluminum while blocks 2, 3, 4, and 5 were fabricated from steel. The
differing materials require individual calibration.

TABLE 4 Comparative Vickers Hardness

ILS #358 ILS #358
Test Calculated True Determined Determined Bias Bias
Block Hardness ValueA Hardness ValueB Hardness ValueC (Test Stand) (Hand Held)
(Test Stand) (Hand Held)
0300142 143.06 NR NR NR NR
0729385 189.70 197.40 196.14 +4.06 +3.39
0800213 240.32 228.44 227.98 -4.94 -5.13
0722420 321.75 311.20 314.22 -3.28 -2.34
0723157 388.78 382.46 372.28 -1.63 -4.24
A
The average of the three testing laboratories calculated averages (obtained using an actual Vickers hardness tester 5 kg test force) from ILS #619. Testing performed
in accordance with Test Method E384.
B
The average of five testing laboratories calculated averages (obtained using UCI (ultrasonic contact impedance) hardness testing equipment with the data expressed
in Vickers hardness numbers) from ILS #358. All included labs utilized 5 kg test force.
C
The average of five testing laboratories calculated averages (obtained using UCI (ultrasonic contact impedance) hardness testing equipment with the data expressed
in Vickers hardness numbers) from ILS #358. All included labs utilized 5 kg test force.
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14. General Requirements 15.5 The hardness reference block shall be calibrated using
14.1 InstrumentBefore a UCI instrument is verified, the a standard and certified hardness testing device per Test
instrument shall be examined to ensure that: (1) the batteries in Method E10, Test Methods E18, or Test Method E384. Make at
the indicating unit are not discharged, and (2) the indenter is least five randomly distributed hardness measurements on the
clean, that is, free from foreign matter like dust, grit, grease or test surface of the reference block and take the arithmetic mean
oil. of all of the readings as the mean hardness of the block.
15.6 Each block shall be marked with (1) the arithmetic
15. Hardness Reference Block mean of the hardness values found in the standardization test
15.1 In order to avoid perturbing vibrations in the reference suffixed by the scale designation letter (for example HV, HRC,
blocks caused by the ultrasonic sensor, they should be suffi- HRB, HBW, HBS, etc.), and (2) with the name or mark of the
ciently large. Recommended is to use steel blocks with supplier. If edge of block is marked, the lettering shall be
dimensions not less than 80 mm in diameter and 16 mm in upright when the test surface is upward.
thickness.
16. Verification
15.2 Each block shall be specifically prepared and heat-
16.1 Check the UCI hardness-testing instrument by making
treated to give a specific hardness and the necessary
at least two measurements on a standard reference block of the
homogeneity, such as in Test Methods E18, and stability of the
selected hardness scale.
surface hardness distribution.
16.2 The instrument shall be considered verified if each
15.3 The test surface shall be polished or fine ground and
hardness reading falls within 63 % of the reference block
free of scratches and other discontinuities, which would
hardness value. Unverified instruments must not be used for
influence the UCI measurement. The surface finish of the test
testing. They should be repaired, if necessary, and be verified
surface shall not exceed 0.4 m maximum.
subsequently.
15.4 To ensure that no material is subsequently removed
from the test surface of the reference block, an official mark or 17. Keywords
the thickness to an accuracy of 60.025 mm at the time of 17.1 portable hardness testing; superficial hardness; ultra-
calibration shall be marked on the test surface. sonic contact impedance (UCI); vickers diamond indenter

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APPENDIX

(Nonmandatory Information)

X1. GUIDELINES FOR SELECTION AND USE OF UCI INSTRUMENTS

TABLE X1.1
Load Model Features Typical Applications

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98 N standard length (manual) relatively large indentation; requires minimal surface small forgings, cast material, weld inspection, HAZ
preparation

49 N standard length (manual) for general use induction hardened or carburized machine parts, for
example, camshafts, turbine weld inspection, HAZ

extended length (manual) 30 mm extended length measurement in grooves, on gear tooth flanks and roots

short probe (manual) reduced length (90 mm); electronics in separate housing turbine blades, inside wall of pipes with >90 mm

9.8 N standard length (manual) load is easy to apply and provides control to test on ion-nitrided stamping dies and molds, forms, presses,
sharp radii thin walled parts

extended length (manual) 30 mm extended length bearings, tooth flanks

short probe (manual) reduced length (90 mm); electronics in separate housing turbine blades, inside wall of pipes with >90 mm

7.8 N motor probe style load is applied by servomotor finished precision parts, gears, bearing raceways

3N motor probe style load is applied by servomotor; rather small indentations thin layers, for example, copper or chromium on steel
cylinders;
copper rotogravure cylinders;
coatings, case hardened parts

1N motor probe style load is applied by servomotor; rather small indentations thin layers and coatings

SUMMARY OF CHANGES

Committee A01 has identified the location of selected changes to this standard since the last issue
(A1038 10a) that may impact the use of this standard. (Approved Nov. 1, 2013.)

(1) Added new bias information in 11.2.

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