Plant Engineering: Electrical Cable Test Applicability Matrix For Nuclear Power Plants
Plant Engineering: Electrical Cable Test Applicability Matrix For Nuclear Power Plants
Plant Engineering: Electrical Cable Test Applicability Matrix For Nuclear Power Plants
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www.epri.com Final Report, December 2011
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Acknowledgments The following organization prepared this report:
Principal Investigator
G. Toman
Objective
To link cable aging mechanisms with tests that can identify their
presence and assess the severity of the condition. The report also
discusses the tests and their applicability to specific cable
conditions and problems.
Approach
Many tests have been developed for various types and designs of
cables. Although most of these tests have applicability under a given
set of conditions, most tests apply to a very specific set of cable
designs and applications. Some are limited to the aging of specific
insulation materials; others are applicable to certain cable designs,
such as shielded cables. Some may or may not be useful if the shield
in a cable has tarnished or otherwise deteriorated.
v
The methods are also discussed in terms of the effects of
environments on cables, such as elevated temperature and
submergence that may cause degradation of cable components.
Results
The report describes the common cable types and designs as a basis
for discussion of test applicability. It then describes the tests in terms
of applicability to cable component aging assessment under various
common environmental conditions.
The last section of the main body of the report describes tests in
terms of cable concerns such as post-installation testing, condition
monitoring and aging management, and troubleshooting. The
forensics process and applicable tests are also described.
Keywords
Applicability of cable test methodology
Cable aging
Cable aging management
Cable testing
Table of Contents
Section 1: Introduction.............................................1-1
Background.....................................................................1-1
Cable Design, Application, and Degradation
Mechanisms ....................................................................1-2
Instrumentation ...........................................................1-2
Medium-Voltage Cable Aging Concerns........................1-7
Section 4: References...............................................4-1
vii
C-03 Gel Content (Solubility) and Swelling Ratio
Measurements ................................................................ A-8
C-04 Plasticizer Content Measurement............................. A-11
C-05 Fourier Transform Infrared Spectroscopy .................. A-13
C-06 NIR Spectroscopy ................................................. A-16
C-07 Thermogravimetric Analysis.................................... A-19
E-01 Insulation Resistance dc Test.................................... A-22
E-02 Polarization Index Test ........................................... A-26
E-03 Time Domain Reflectometry Test............................... A-29
E-04 Line Impedance Resonance Analysis ........................ A-31
E-05 Dielectric Spectroscopy .......................................... A-35
E-06 Dissipation Factor (Tan ) ....................................... A-38
E-07 Partial Discharge (Off-line) ...................................... A-43
E-08 Continuity (Loop) Resistance Test ............................. A-47
E-09 Differential Insulation Resistance .............................. A-49
M-01 Hardness Test ...................................................... A-51
M-02 Tensile Strength and Elongation-at-Break Test ........... A-54
M-03 Indenter Modulus Testing....................................... A-58
M-04 Density Testing ..................................................... A-62
M0-5 Acoustic Velocity Testing ....................................... A-65
M-06 Thermal Fingerprinting .......................................... A-67
M-07 Nuclear Magnetic Resonance in Solution ................ A-70
M-08 Micro Modulus..................................................... A-72
V-01 Visual Examination ................................................ A-74
V-02 Microscopic Examination ....................................... A-77
List of Figures
ix
Figure A-4 LIRA system block diagram .................................. A-31
Figure A-5 LIRA plot for a 98.43-ft (30-m) cable showing a
thermal damage signal at 73.82 ft (22.5 m) .................... A-32
Figure A-6 Loss angle, ...................................................... A-38
List of Tables
xi
Section 1: Introduction
Background
Many test methods exist for assessing the condition of electrical cable insulations,
conductors, and shields. Very few test methods have broad applicability, and the
user must use the tests wisely for the particular cable type, application, and
concern. With respect to cable type, instrumentation, control, and power cables
have different designs, materials, and applications that change the way in which
they function and age. Power cables are further divided by voltage class with low-
voltage cable (rated <2000 V, and operating at <1000 V) having simple designs
and medium-voltage cable (rated 5 to 46 kV) having much more sophisticated
designs and aging considerations. The tests many be divided into groups such as
manufacturing tests, postinstallation tests, maintenance tests (condition
monitoring), and troubleshooting. Some of the most common tests, such as
insulation resistance and time domain reflectometry (TDR), are excellent
troubleshooting tools, but in most cases are insensitive to the aging of cable
components so that little or no advanced warning is given with respect to the
onset of severe aging.
The following section describes the types of cables used in nuclear plants, their
design, their applications, and the resulting degradation mechanisms that are of
concern so that appropriate test methods can be identified. A separate section
follows on troubleshooting methods. This report focuses on the types of cables
used in nuclear power plants and not on cables used in utility distribution systems
and other industrial applications. Accordingly, the recommendations listed here
may differ significantly from those that apply to utility distribution systems
because the designs of the nuclear plant cables differ from the designs used in
distribution systems.
1-1
Cable Design, Application, and Degradation Mechanisms
Instrumentation
The two basic types of instrumentation cable designs used in nuclear plants are
twisted shielded pairs, triples, etc., and coaxial types. While other specialty
designs exist, they are beyond the scope of this document.
A number of different shield designs have been used. One of the more common
designs uses aluminized polyester (often Mylar1) tape that is wrapped around a
twisted pair or triplet of insulated conductors. A drain wire is placed along the
aluminized side of the tape to provide a connection between the tape and the
ground and to provide a convenient means of connecting the ground. Alternate
means of shielding use a metallic shield, which can be in the form of a helically
wrapped tape, a braid woven from fine wires, or fine parallel wires surrounding
the pairs or triplets.
The insulations used in instrument and control cables are the same as those used
in control and low-voltage power cables. These are cross-linked polyethylene
(XLPE), fire-retardant ethylene propylene rubber (FR-EPR), bonded jacket
EPR (chlorosulfonated polyethylene/EPR [CSPE/EPR]) and neoprene/EPR
[NEO/EPR]), and silicone rubber. Polyvinyl chloride (PVC), although rarely
used as an insulation in the United States, is commonly used as an insulation
elsewhere in the world. In bonded jacket EPR, the EPR layer is not fire
retardant. A NEO or CSPE jacket is bonded to the insulation layer to provide
fire retardancy. Less common, but occasionally found, insulations are butyl
rubber, CSPE (Hypalon2), Kapton2 (polyimide tape), and Tefzel.2 Jackets are
typically NEO, CSPE, or PVC (limited U.S. usage). Instrument cables are often
rated for 300 V or less and are not subject to significant operating currents.
Therefore, the insulation thicknesses on twisted shielded cables may be two-
thirds of that used on control and power cable with similar conductor sizes,
causing the insulation system to be more sensitive to thermal and radiation aging
than control and power cables using the same insulation.
1
Mylar is a registered trademark of DuPont.
2
Hypalon, Kapton, and Tefzel are registered trademarks of DuPont.
1-2
Inside the power plant, thermal aging is the key aging concern. Most of the
polymers will harden, eventually lose tensile properties, and then finally powder
and fail if the aging is not controlled. Thermal aging will likely overshadow all
radiation effects, given the generally low dose rates around most cables.
The polymers used as insulation in coaxial and triaxial designs are designed to
have specific impedance characteristics. They are not designed for high-
temperature conditions and have lower temperature ratings than power and
control cables. Various insulations have been used including polyethylene (PE),
XLPE, and EPR.
Mineral-insulated cables are available with stainless steel jackets. These cables are
impervious to radiation and elevated temperatures. However, the connectors
generally contain polymeric seals or seal systems that can age from elevated
temperature or radiation.
Control Cables
1-3
applied to add flame retardancy. Common insulations used in control cables are
XLPE, FR-EPR, EPR with a bonded layer of NEO or CSPE, EPR with a
nonbonded layer of NEO or CSPE, CSPE alone, silicone rubber, PVC, and
butyl rubber. PVC is not used as insulation in the United States, but has been
used in Canada, Japan, Korea, Eastern Europe, and the former Soviet Union.
Butyl insulation was used in very few early plants. The most common insulations
are XLPE, FR-EPR, EPR/NEO, and EPR/CSPE. EPR/NEO was phased out
of manufacture by the early 1980s.
Although the insulation systems for most control cables are rated at 90C at the
conductor, the overall cables are not suitable for 90C environments on a
continuous basis. The jackets are rated at 75C or less. In EPR with bonded
CSPE, the CSPE layer ages faster than the EPR layer and becomes the
controlling layer with respect to failure under manipulation of the cable during
maintenance and under high-pressure steam accident environments such as those
in containment.
Low-voltage power cables are essentially the same as those of control cables, but
have thicker insulations depending on the conductor size. The insulation
thicknesses range between 0.045 in. (1.1 mm) and 0.08 in. (2 mm). The
insulations are generally XLPE, FR-EPR, EPR/NEO, EPR/CSPE, butyl
rubber, and silicone rubber. PVC was used in many non-U.S. plants. The cables
are generally rated for 90C) conductor temperatures in a 40C ambient with the
exception of butyl rubber and PVC, which have lower thermal ratings, and
silicone rubber, which has a conductor rating of 120C and higher.
The aging concerns for low-voltage power cables are the same as those for
control cables.
1-4
Medium-Voltage Power Cables
Medium-voltage power cables are more complex than low-voltage power cables
because the voltage stresses in the insulation are higher, and voltage stressrelated
degradation mechanisms become a concern. The thickness of insulation in a low-
voltage power cable is dictated by mechanical concerns related to handling,
installation, and in-service physical stresses. The insulation is much thicker than
necessary for voltage withstanding purposes. However, at operating voltages
above 4 kV phase to phase, the thickness is of the insulation is dictated by the
applied voltage and not handling/installation concerns. The voltage is high
enough that small air gaps between the insulation and the conductor can break
down due to operating voltage or voltage surges. If an air gap existed between the
conductor and interior surface of the insulation, the discharge across the air gap
would cause small increments of damage to the insulation that would eventually
cause it to fail. To eliminate such air gaps, a conductor shield is applied to the
conductor before the insulation is applied. The earliest designs used impregnated
cotton tapes. These were phased out in the very early 1970s. The next design
used semiconducting polymer tapes. These were phased out in the mid-1970s.
The current designs use extruded polymer shields. Nearly all manufacturers use
semiconducting shields with a low resistance, but not low enough to be classified
as a conducting material. The exception is a Kerite design in which a high
permittivity layer is used instead of the semiconducting layer. The design is called
Permashield.
The conductor shield is used in all medium-voltage designs, whether the cable is
a nonshielded or shielded design, which refers to the insulation shield system. In
5-kVrated cables used in power plants, use of an insulation shield is optional. In
a cable having an insulation shield, called a shielded cable, a shield is applied to the
outer surface of the insulation, and a metal tape or wire is used to drain or ground
the shield. Like the conductor shield, the insulation shield could be cotton tape
(late 1960s), polymer tape (early 1970s), or extruded polymer (mid-1970s to
date). When extruded polymer shields came into being, the manufacturers
removed the carbon black from the insulations so that the black polymer
insulation shield, which must be removed during splicing and termination, could
be easily distinguished from the pink or brown color of the insulation.
For nuclear plants, the most common metallic component of the insulation shield
is a helically wrapped copper tape with a 10% overlap (Figure 1-1). In earlier
cable designs, the tapes were tinned to prevent the copper from deteriorating
from excess chlorine and sulfur in the jacket materials. Modern cables do not
need tinned shields because the jackets do not have free sulfur and chlorine.
Some cables used zinc tape. The tapes were used because the cables were more
flexible than distribution cables. The metallic component in a distribution cable
shield generally is made up of round or flat copper wires of sufficient size to
carry full-phase current when used in single-phase systems (Figure 1-2). The
only distribution cables expected in a nuclear plant are those associated with
off-site feeds.
1-5
Figure 1-1
Helical metal tape shield
Figure 1-2
Concentric neutral (flat strap design)
One alternate design that does not use flat tapes is the UniShield design. The
UniShield cable is a compact-design EPR insulated cable with a diameter that is
as small as that of an XLPE cable (Figure 1-3). This is achieved by having a
compacted conductor, a thinner layer of insulation, and a jacket that doubles as
the semiconducting layer. Six corrugated wires are located in the jacket and run
longitudinally to drain the jacket.
1-6
Figure 1-3
UniShield design: drain wire in a semiconducting jacket
A new shield design uses linear corrugated copper that is wrapped around the
semiconducting layer and is either glued shut or welded. This design allows a
flexible cable, with a water-impervious layer that is similar in thickness to a tape
shield system. In addition to keeping water out of the core of the cable, this
shield design improves testability of the cable using partial discharge (PD)
methods. Tape shields act as inductors once a slight tarnish occurs on their
surface, which causes attenuation of high-frequency signals and often eliminates
PD testing.
Thermal Aging
1-7
Partial Discharge
Wet Aging
For underground wet and submerged cable, the types of degradation and failure
mechanisms change with the vintage of the cable and in some cases the design.
Before the mid-1970s, EPR cables were manufactured with clean, calcined clay
that was untreated. This led to cable insulations that would absorb up to 3%
moisture by weight and had clays that were more weakly bound to the EPR than
in modern cable. In approximately 1975, the industry switched to clay that was
treated with silane that sealed the clay and made it chemically bind to the EPR,
resulting in EPR insulations that absorb no more than 0.3% moisture and that
are much stronger mechanically than earlier versions. The old-style EPRs
experience water-related degradation that results in low insulation resistance
tunnels in the insulation. The first occurrence of this type of degradation has
been observed at 30 to 33 years. No failures of modern silane-treated clay EPR
have occurred to date in standard design cables.
The UniShield design has experienced failures under wet conditions that are
attributed to other failure mechanisms. Failures have occurred when gaps
occurred between the jacket and insulation that could have occurred from pulling
damage. Other failures have occurred from corrosion of the shield drain wires
that resulted in partial discharging within the shield that led to failure.
Cable aging must be understood in terms of a cable system rather than just an
insulation on a conductor. The splices and terminations complete the cable, and
their failure has the same effect on the plant as an insulation failure. In control
and low-voltage power cables, the conductor and insulation are continued
through a splice, and a jacket may or may not be used. In twisted shielded pairs
and triples, the conductors and their insulations are continued as well as the
shield and drain wire. A jacket covering is necessary to protect the shield and
drain at the splice. For coaxial and triaxial cables, special connectors specifically
designed for the application must be used at splices and terminations. For low-
voltage power and control, terminations generally consist of terminal lugs that
1-8
land on terminal strips with the insulation stopping at the lug. Terminations at
motors generally consist of bolted connections that are insulated with tape, heat
shrink, cold shrink, or gel systems.
The splices and terminations for shielded medium-voltage cable are much more
complex. In a termination, the conductor shield and insulation are removed to
allow a lug to be applied. The insulation shield is removed for a significant length
along the insulation, and a voltage stress-control layer (additional insulation, a
capacitive stress-control layer, or a high-permittivity layer) must be applied, and
the metallic layer either grounded or terminated. Care must be taken to have no
air gaps or insulation cuts in the stress-control area.
For splices, all of the layers in the cable must be replicated in the splice, and the
voltage gradients at the cut backs of the insulation shield must be controlled.
Voids or contaminants in the splice will likely cause failure. For more modern
(post-1975) medium-voltage cable, splice and termination workmanship are
more likely to cause failure than water-induced degradation of the insulation.
1-9
Section 2: Cable Component Aging and
Aging Assessment
Insulation and Jacket Aging and Assessment
The main aging stressors for all types of cables located in dry environments are
temperature, radiant heating, radiation, and chemical conditions. For instrument
and control cables, external temperature and radiant heating are dominant causes
of insulation and jacket aging. Although radiation can cause insulation and jacket
aging, doses that are high enough to have an effect coexist with elevated
temperature, and the thermal effects most often outweigh the radiation effects.
For power cables, external temperature and radiant heating are also dominant
causes of insulation and jacket aging. In addition, ohmic heating from conductor
current can increase thermal aging significantly. However, derating factors that
are commonly used in plant applications most often limit the degradation caused
by ohmic heating. As with instrument and control cables, in areas with
significant radiation doses, thermal effects generally dominate the aging. Table
2-1 lists the aging effects of elevated temperature, radiant heating, and radiation
on the types of insulation used in nuclear plant cables.
2-1
Chemical, Oil, and Hydraulic Fluid Exposure
Exposure of cable jackets and insulations to hydraulic fluid and oil can cause
severe degradation. Softening and swelling of rubber jackets and insulations are
likely. XLPE is less likely to be affected by hydraulic fluids and oils at lower
temperatures, but if an exposure occurs, cleaning of the surface is required to
prevent long-term effects.
2-2
Table 2-1
Insulation degradation and condition assessment correlation
Insulation Material Elevated Temperature and Radiant Elevated Radiation Condition Assessment Tests
Heat
XLPE 122F (50C): little effect <5 Mrd (<50 kGy): little Due to crystallinity, in situ tests are
122158F (5070C): long-term loss of observable effect ineffective. If jacket is in good
tensile strength >5 Mrd (>50 kGy): some condition, XLPE will be in good
>158F (>70C): significantly shortened life observable effect, likely condition. Multiple laboratory tests are
overshadowed by thermal effects available.
FR-EPR 122F (50C): little effect <5 Mrd (<50 kGy): little Indenter modulus and acoustic velocity
122140F (5060C): long-term hardening observable effect testing to assess hardening in-plant.
and loss of tensile strength >5 Mrd (>50 kGy): some Inaccessible (in conduit) cables may be
>140F (>60C): significantly shortened life observable effect, likely assessed electrically via line
overshadowed by thermal effects impedance resonance analysis (LIRA).
Numerous laboratory tests are
available.
Bonded jacket EPR, 104F (40C): little effect <5 Mrd (<50 kGy): little NEO layer may be tested in-plant with
NEO/EPR 104122F (4050C): NEO layer hardens observable effect Indenter modulus to assess hardening.
with time >5 Mrd (>50 kGy): some Inaccessible (in conduit) cables may be
>122F (>50C): NEO layer hardens and observable effect, likely assessed electrically via LIRA.
cracks in a relatively short period; EPR layer overshadowed by thermal effects Numerous laboratory tests are
behaves similarly to FR-EPR above available.
Note: With severe thermal aging, the NEO
layer gives off chlorine that will corrode
surrounding metals including terminations
and exposed relay contacts.
2-3
Table 2-1 (continued)
Insulation degradation and condition assessment correlation
Insulation Material Elevated Temperature and Radiant Elevated Radiation Condition Assessment Tests
Heat
Bonded jacket EPR, 122F (50C): little effect <5 Mrd (<5 kGy): little CSPE layer may be tested in-plant with
CSPE/EPR 122149F (5065C): CSPE layer hardens observable effect Indenter modulus or acoustic velocity to
with time >5 Mrd (>5 kGy): some assess hardening. Inaccessible (in
>149F (>65C): CSPE layer hardens in a observable effect, likely conduit) cables may be assessed
relatively short period; EPR layer behaves overshadowed by thermal effects electrically via LIRA. Numerous
similarly to FR-EPR above laboratory tests are available.
Note: Aging of the insulation system is
controlled by the CSPE layer. Once
hardened, the CSPE layer will crack when
manipulated or when exposed to a loss of
coolant accident environment. The crack will
propagate through the EPR layer as well.
Silicone rubber No thermal damage to temperatures in <5 Mrd (<5 kGy): little Silicone rubber has limited mechanical
excess of 212F (100C) observable effect properties. Physical damage is
>5 Mrd (>5 kGy): some possible. Standard troubleshooting
observable effect techniques may be used to assess
physical damage.
CSPE (Hypalon) 122F (50C): little effect <5 Mrd (<5 kGy): little CSPE may be tested in-plant with
122149F (5065C): CSPE layer hardens observable effect Indenter modulus to assess hardening.
with time >5 Mrd (>5 kGy): some Inaccessible (in conduit) cables may be
>149F (>65C): CSPE layer hardens in a observable effect, likely assessed electrically via LIRA.
relatively short period overshadowed by thermal effects Numerous laboratory tests are
available.
Note: Severely aged Hypalon will crack
when bent and will likely split in a loss of
coolant accident environment.
2-4
Table 2-1 (continued)
Insulation degradation and condition assessment correlation
Insulation Material Elevated Temperature and Radiant Elevated Radiation Condition Assessment Tests
Heat
Butyl rubber (sulfur 122F (50C): little effect; elevated May soften when exposed to May be tested with Indenter modulus.
cure) temperatures may soften with aging significant doses
Tefzel No thermal damage to temperatures 158 Significant loss of properties at Hard plastic and laboratory tests are
176F (7080C) 20 Mrd (200 kGy) needed to assess condition.
Kapton No significant thermal aging effects Kapton is a tape that is held in Application of a grounded wet cloth
place by thin layers of Teflon. with insulation resistance testing may
Kapton is unaffected by be useful. Otherwise, physical
irradiation, but the Teflon layer assessment and testing in the
deteriorates by a few megarads laboratory are necessary.
of exposure. Thereafter, wetting
will likely cause shorting.
2-5
Kapton Insulation Concerns
Nearly all of the insulations in use in nuclear power plants are extruded onto the
conductor by forcing the molten polymer as the conductor passes through a die.
The result is a uniform layer of insulation. Kapton is the exception. Kapton is a
0.001-in. (0.025-mm) polyimide tape having a 0.0001-in. (0.0025-mm) layer of
Teflon on each face. The Kapton tape is helically wrapped on the conductor. A
second layer is applied in the opposite direction. The Teflon layers are then
sintered to each other by passing the insulated wire through a beta beam. Kapton
can withstand 3000 Mrd (30 MGy) and retain 75% of its original tensile
properties [1]. However, the Teflon layers will degrade after a few megarads (a
few 10s of kilograys), leaving only the mechanical wrap of the Kapton as the seal,
making the insulation susceptible to shorting upon wetting. Kapton can lose
tensile strength and crack in warm, wet environments if bent tightly. A detailed
discussion of the aging and issues of Kapton insulation is provided in Review of
Polyimide Insulated Wire in Nuclear Power Plants, NP-7189 [1].
The shield in an instrument circuit is grounded at one end of the circuit, and the
far end is not grounded. If both ends of the shield are grounded, a transformer
action can occur. and noise will be induced into the circuit. If the jacket fails and
the shield is grounded at multiple points, noise will be induced in the circuit. If
noise occurs, lifting of the ground and measuring insulation resistance between
shield and ground are recommended. Jacket damage from thermal stress or
chemical exposure is possible for instrument cable with twisted shielded
construction. For the function of the shield to be affected in dry applications, the
jacket would have to fail such that an extraneous conductive path would occur
between the shield and the ground. For NEO-jacketed cables, such paths are
possible because NEO shrinks circumferentially and axially when highly
thermally aged, causing wide cracks to form. Hypalon (CSPE) and chlorinated
polyethylene (CPE) jackets will harden from thermal stress, but generally do not
crack spontaneously.
Deterioration of the shield without failure of the jacket is not expected. Jacket
failure or saturation with water is a possible means of adversely affecting shield
function in underground applications. Physical damage to jackets during
installation in underground systems may result in multiple shield grounds if the
system becomes wet. Color jackets (pigmented through the depth) may also
allow enough moisture through to cause grounds. The curing of jackets that will
be dyed is different from those that are black due to carbon content. To make the
colors stable over long periods, alternate curing processes are used that allow the
material to absorb more water.
2-6
For instrument cable, the presence or absence of noise on the circuit is a direct
indication of the condition of the shield. If the shield is suspected of having
multiple grounds, a time domain reflectometer may be used to locate the
additional grounds such that targeted corrective actions can be made. In cases in
which submergence was the cause of the additional grounds, draining of the duct
system worked for at least one plant.
2-7
Section 3: Cable Test Versus Cable Concern
Introduction
This section relates cable tests to the concerns that arise for plant cables. The
concerns are as follows:
Postinstallation testing: tests that prove the cable circuit is ready for service
Condition monitoring/aging management: test and assessments that
determine the current condition of the cable and whether it is acceptable for
use for a period of time (one or more operating cycles)
Troubleshooting: tests to determine the nature of degradation and
determine whether repair is possible or replacement is necessary
Failure and forensics assessments: tests to identify the reason for failure or
degradation and the need for corrective action on similar applications and
circuits
Post-Installation Testing
3-1
Table 3-1
Postinstallation test applicability
3-2
Condition Monitoring and Aging Management
The tests and assessments that should be used depend on the stressor of concern
that could cause aging of a cable subcomponent, the type of cable, and the nature
of the application.
Wetting and submergence are of highest concern for medium-voltage cables and
splices, but can affect improperly made low-voltage splices. There is no literature
indicating a generic concern for low-voltage applications; however, jacket
deterioration on shielded instrument cable may lead to multiple shield grounds
and increase noise in the instrument circuit.
3-3
Oil, chemical, and hydraulic contamination of cables is generally localized and
affects a limit number of circuits and requires case-specific analysis and action.
Similarly, vibration fatigue of conductors and insulation is limited to a particular
piece of equipment and is likely to be unique to the application when observed.
Table 3-2 provides a linkage of stressors coupled with cable, splice, and
termination component that could be affected and the linkage to appropriate
tests. Table 3-3 provides a linkage between the possible tests and the cable types
and configurations to which they apply.
3-4
Table 3-2
Condition monitoring and aging management tests
3-5
Table 3-2 (continued)
Condition monitoring and aging management tests
3-6
Table 3-2 (continued)
Condition monitoring and aging management tests
3-7
Table 3-3
Applicability of electrical tests to medium-voltage cable designs and insulations
Cable Type
3-8
Table 3-3 (continued)
Applicability of electrical tests to medium-voltage cable designs and insulations
Cable Type
(VLF DF (tan ) May be used. Not recommended; May be used. May be used. May be used. May be used. May be used. May be used.
no shield to form
ground plane for
test.
VLF PD May be used. Not recommended; May be used. Corrosion of May be used. May be used. May be used. May be used.
few useful data tape shield EPR may EPR and EPR may
expected. may attenuate attenuate high corrosion of attenuate high
high frequencies. shield likely to frequencies.
frequencies. Verify attenuate high Verify
Verify acceptable frequencies. acceptable
acceptable attenuation Verify attenuation with
attenuation with calibration acceptable calibration
with calibration pulse. attenuation pulse.
pulse. with
calibration
pulse.
3-9
Table 3-3 (continued)
Applicability of electrical tests to medium-voltage cable designs and insulations
Cable Type
3-10
Table 3-3 (continued)
Applicability of electrical tests to medium-voltage cable designs and insulations
Cable Type
Note 1. The tests listed for EPR with helical metal tape shields apply to butyl rubber as well.
3-11
Troubleshooting
In many cases, nuclear cable circuits are simple and relatively short, making
accurate location of the fault unnecessary. All three phases of the faulted cable
will be removed and replaced. However, some circuits are long and contain
multiple splices, and replacement of the entire circuit is neither cost-effective nor
necessary. A detailed discussion of fault location techniques with advantages and
disadvantages is provided in Underground Cable Fault Location Manual, EPRI
TR-105502 [2]. The most common methods are summarized here.
3-12
Figure 3-1
Faulted cable termination in a metal-clad switchgear compartment. Note: Slightly
burned condition of B-phase stress-relief adaptor.
Figure 3-2
Burn through of stress-relief adaptor
3-13
Identification of Faulted Phase(s)
Insulation Resistance
The simplest and most common starting point is insulation resistance testing.
Once the cables have been determined from the source and load, insulation
resistance tests can be used to identify those phases that are faulted. A nonfaulted
phase should have an insulation resistance of at least a gigohm-1000 ft (305
Mohm-km). Unless the fault is solidly grounded, which is rare, the insulation
resistance can be quite high because the metal shield often burns out in the
vicinity of the fault. Figure 3-3 shows a faulted cable that blew out the helically
wrapped copper tape shield. Although this fault had multiple restrikes, loss of the
shield around the fault is common and can result in an insulation resistance
greater than 10 Mohms. Figure 3-4 shows another cable, with the jacket
removed, having shield loss from the fault. The damage to the insulation and
conductor in Figure 3-4 is much less severe than that shown in Figure 3-3, and
yet there is still substantial shield loss.
Figure 3-3
Cable fault in which the shield burned out. Note: The shield has vaporized and is
not visible at the edges of the hole in the jacket.
3-14
Figure 3-4
Cable with shield loss from fault
Once the faulted phase is identified, insulation resistance testing can be used to
locate the fault by sectionalizing. In this method, the cable is cut in two. For
cables with an underground section, the cut is generally made at the point where
the cable enters the duct system, given that the fault is expected to be in the
underground section. If it is, then the underground section is replaced after
confirming the adequacy of the dry section through appropriate condition
assessment tests. If the underground segment is long and contains splices, further
sectioning can be performed to identify the faulted section.
Low-Voltage TDR
3-15
detected if it has a high impedance, which could be the case if the shield has been
disrupted by the fault current. A zero resistance fault would absorb all of the
pulse energy such that the pulse would not reach the far end of the cable and no
signal would be reflected. If the conductor is grounded, the return pulse from the
fault is reflected and seen as a negative pulse. The pulse from the open
termination that is reflected is a positive pulse. If an open circuit occurs, the pulse
will reflect from the open point, and there will be no reflection from the far open
circuited termination. Greater accuracy can be obtained from testing the faulted
phase from both directions. Attenuation of the TDR signal from EPR and butyl
rubber may adversely affect the results as will slight tarnishing of a tape shield,
which will cause it to act as an inductive high-frequency filter. EPRI report
TR-105502 [2] provides more detail on use of TDR.
However, the thumper may be used in conjunction with a TDR system that
registers the pulse at the fault as well as the reflection of the pulse from the far
termination. This TDR allows location of the fault after just a few discharges.
The thumper has sufficient voltage to break down the fault if it has too high of
an impedance for a low-voltage TDR to work properly. Figure 3-5 shows a
schematic of a thumper with a TDR attachment.
3-16
Figure 3-5
Thumper with TDR [2]
Electrical balance bridges may be used in fault location. The Murray Loop,
which is an adaptation of the Wheatstone Bridge, is a commonly used bridge for
phase to ground faults. Figure 3-6 shows a diagram of a Murray Loop. The ratio
of D1 to D2 when the bridge is balanced is the same as the ratio of d1, the
distance through a good conductor to the fault through the connected far ends,
to d2, the distance from the test end to the fault on the faulted conductor.
Figure 3-6
Murray Loop adaptation of a Wheatstone Bridge [2]
3-17
Forensics and Failure Assessment
When repairs and replacement are being planned, careful removal and protection
of the failed cable, splice, or termination should be performed to allow failure
assessment and forensic activities to be performed. If a cable, splice or
termination has failed, a few feet (1 m) or more on each side of the splice or cable
failure point or leading away from the termination should be removed with the
failure site. The extra material will allow the forensics team to more easily
understand the context of the failure. If possible, long sections of cable (3060 ft
[9.118.3 m]) should be sent to the laboratory to allow electrical testing of the
cable after the fault has been removed. Although short sections of cable can be
tested, short sections require special terminations and make some tests, such as
low-frequency DF testing, impractical. Upon removal, the ends of the specimen
should be capped and the cable, splice, or termination wrapped in PE to keep
moisture in the cable and dirt out. The specimen should be handled with care.
Any damage done during removal should be carefully documented and forwarded
to the laboratory. The laboratory in which the forensic work will be performed
should be selected carefully. It should have experience with assessment and
testing of the type of cable and insulation system being evaluated. Not all
laboratories can perform assessments of butyl rubber and EPR. Some laboratories
have good experience with XLPE distribution cables, but may have little or no
experience with the designs used in nuclear plants. Sending a plant staff member
to witness the forensics activity is highly recommended to provide a
communications path to plant information for the forensics team and as an
opportunity to learn more about cable design and the associated failure
mechanisms.
The order of testing and assessment should proceed from the least invasive and
likely to cause more damage toward breakdown testing and complete disassembly
and dissection. Visual inspections and photographing of the as-received
condition are important. Comparison of the cable and splice construction with
that of the original plant receipt inspection or manufacturers literature is useful
for confirming that the design and configuration of the cable, splice, or
termination are as they were expected to be. Small differences could be
significant with respect to failure.
Generally, once removed from the duct, the fault location is obvious and the
faulted section can be removed from the remaining cable for detailed assessment,
and the remaining sections can be subjected to electrical condition assessment
tests and breakdown tests to understand the general condition of the cable
around the faulted section. This electrical testing will indicate whether there is
general degradation in the cable or just a localized degradation.
3-18
causing the breakdown of the insulation remain, making a positive identification of
the cause of the failure possible. Taking transverse wafers of sections surrounding
the fault and through the fault is a common means for assessing the material in the
cable. XLPE is translucent, and flaws can often be seen in the material. Heating
the XLPE wafers in oil will cause the XLPE crystals to melt and cause the material
to become transparent. Figure 3-7 shows an XLPE-insulated conductor while in
hot oil. Figure 3-8 shows a wafer through the tree after the wafer was stained, and
Figure 3-9 shows a flaw at the base of the tree where it started.
Figure 3-7
Large water tree viewed through a hot oil bath
Figure 3-8
Cross section of water tree shown in Figure 3-7
3-19
Figure 3-9
Flaw in the conductor semiconducting layer at the base of the water tree in
Figure 3-8
Finding flaws and defects in black butyl rubber and black EPR is often difficult
because of the opacity of the materials. Finding flaws in pink EPR is somewhat
easier, but it is possible to identify only conditions observable from the surface of
the wafer. For water-related degradation, boiling the wafers in water for a
significant period will sometimes cause local swell or voids to appear, indicating
areas of water-related degradation. Figure 3-10 shows the opacity of a black butyl
rubber wafer. Boiling of the specimen revealed fissures and swelling in a low-
resistance channel in the insulation.
Figure 3-10
Micrograph of insulation wall at a low-resistance channel showing swelling and
fissures in butyl rubber
3-20
Figures 3-11 and 3-12 show wafers cut through breakdown channels. Again,
boiling of this pink EPR from a UniShield cable showed bow-tie and vented
treelike formations.
Figure 3-11
Micrograph of a breakdown channel through bow-tie water tree
3-21
The causes of failures may be due to flaws or damage to jackets, the shield
system, conductor, or insulation. Frequently, degradation is related to a voltage
stress riser caused by a defect from manufacture or damage during installation
and handling that takes a number of decades to cause failure. A wet or
submerged environment enhances the failure mechanism.
Moisture content of the insulation, insulation shield polymer, and jacket can
provide insights with respect to the role played by water. Water content at the
outer and inner surface of the insulation provides further insight. Water-related
corrosion of the metallic shield and conductor also provide information regarding
the importance of water in the failure.
Once the polymer or tape shield has been removed from the cable, the local
differential resistance between the surface of the insulation and the conductor can
be assessed. Insulation resistance between the conductor and a small surface
probe (0.2- to 0.3-in. [5- to 8-mm] diameter) can be evaluated by passing the
probe along the surface of the insulation (see Appendix A, section E-09). In
butyl and blank EPR insulations 30+ years old that were subjected to wet-
energized aging, tunnels of low insulation resistance that were approximately
1/1000th of the resistance of the surrounding insulation have been found. When
the shield was restored and electrical breakdown tests were performed, the
insulation consistently broke down in one of these tunnels. The micrograph in
Figure 3-10 shows the degradation found in one such tunnel in butyl rubber
insulation.
Assuming a significant length of cable has been sent to the forensics lab, the
segments of cable surrounding the fault can be subjected to electrical testing once
the failed section has been removed. The electrical tests will provide information
that indicates whether the degradation was localized at the fault or throughout
the cable. Depending on the type of insulation and shield, PD, DF, dielectric
spectroscopy, or other tests may be performed to determine the overall condition
of the cable. Then, a breakdown test can be performed to determine whether the
cable is significantly degraded. If a dry section with little aging or a warehouse
sample has been provided, the unaged condition may be identified for
comparison. If the cable segments surrounding the faulted section test like new,
the failure can be assumed to be localized and likely related to a manufacturing or
installation issue. If the cable tests indicate a degraded state, dissection of the
cable surrounding the breakdown will indicate whether the condition is similar to
that in the area of the in-service fault. A determination can be made as to
whether the degradation is distributed. Distributed degradation indicates that
the cable and cables of the same type and subject to similar conditions are aging
and that testing to determine the actual condition of similar cable applications
is necessary.
3-22
Section 4: References
1. Review of Polyimide Insulated Wire in Nuclear Power Plants. EPRI. Palo Alto,
CA: 1991. NP-7189.
2. Underground Cable Fault Location Manual. EPRI, Palo Alto, CA: 1995.
TR-105502.
4-1
Section 5: Acronyms
cm1 inverse of centimeters
CPE chlorinated polyethylene
CSPE chlorosulfonated polyethylene (Hypalon)
CSPE/EPR ethylene propylene rubber insulation with a bonded jacket of
chlorosulfonated polyethylene
DF dissipation factor
DSC differential scanning calorimeter
EPR ethylene propylene rubber
FR-EPR fire-retardant ethylene propylene rubber
FTIR Fourier transform infrared
HDPE high-density polyethylene
LIRA line impedance resonance analysis
Mrd megarad
NEO neoprene (chloroprene)
NEO/EPR EPR insulation with a bonded jacket of neoprene
NIR near-infrared
NMR nuclear magnetic resonance
OIT oxidation induction time
PD partial discharge
PE polyethylene
PI polarization index
PVC polyvinyl chloride
SBR styrene butadiene rubber
TDR time domain reflectometry
TGA thermogravimetric analysis
VLF very low frequency
XLPE cross-linked polyethylene
5-1
Appendix A: Test Method Descriptions
C-01 Oxidation Induction Time Test A-2
C-02 Oxidation Induction/Onset Temperature Test A-6
C-03 Gel Content (Solubility) and Swelling Ratio Measurements A-8
C-04 Plasticizer Content Measurement A-11
C-05 Fourier Transform Infrared Spectroscopy A-13
C-06 NIR Spectroscopy A-16
C-07 Thermogravimetric Analysis A-19
E-01 Insulation Resistance dc Test A-22
E-02 Polarization Index Test A-26
E-03 Time Domain Reflectometry Test A-29
E-04 Line Impedance Resonance Analysis A-31
E-05 Dielectric Spectroscopy A-35
E-06 Dissipation Factor (Tan ) A-38
E-07 Partial Discharge (Off-line) A-43
E-08 Continuity (Loop) Resistance Test A-47
E-09 Differential Insulation Resistance A-49
M-01 Hardness Test A-51
M-02 Tensile Strength and Elongation-at-Break Test A-54
M-03 Indenter Modulus Testing A-58
M-04 Density Testing A-62
M-05 Acoustic Velocity Testing A-65
M-06 Thermal Fingerprinting A-67
M-07 Nuclear Magnetic Resonance in Solution A-70
M-08 Micro Modulus A-72
V-01 Visual Examination A-74
V-02 Microscopic Examination A-77
A-1
C-01 Oxidation Induction Time Test
Uses
Test Description
The time between the start of the test and the start of the exothermic reaction is
the OIT. A test temperature is chosen that results in a test duration of
approximately 1 hour for a new specimen. The OIT for a material that has aged
significantly will be on the order of 5 minutes or less. For some materials, the
OIT value decreases progressively with time at stress.
Acceptance Criteria
The acceptance criteria are based on experimentation and are expressed as time in
minutes. For PEs or EPR, it has been found that an OIT of less than 1 minute
(at the standard temperature) indicates the insulation has reached the
embrittlement stage and the elongation has decreased significantly. The OIT
decreases progressively with age and rapidly with increased total radiation dose.
3
The references cited in this Appendix are separate from the references for the main body of
the report.
A-2
An OIT of less than 4 minutes for a thermally aged, filled XLPE material having
a 52-minute unaged OIT has a corresponding elongation-at-break of less than
50% [2]. The OIT for this material when aged at 130C showed a decrease to 10
minutes after 30 days of aging. The OIT then stabilized until approximately 120
days and then began a sudden change. For this filled XLPE, use of OIT might
be difficult because of the long period of stability followed by the sudden change.
Reference 2 also provides data for unfilled XLPE that has a gradual, continually
dropping characteristic. For this unfilled XLPE, the OIT started at 36 minutes,
and when it decreased to 1 minute after approximately 300 days of thermal aging
at 130C, the elongation-at-break had decreased to approximately 50%. Use of
OIT would be more practical with this XLPE due to the steady decrease in value
with continued aging.
Figure A-1 shows a thermogram from an OIT test. A tangent is drawn with
respect to the horizontal portion of the curve. Then a tangent is drawn to the
lower portion of the curve when heat absorption stops. The intersection is the
end of the OIT period. The point at which the material reaches the test
temperature is deducted from the end to determine the OIT. Although the DSC
can automatically determine the OIT, manual interpretation is often needed if
there is a small reaction followed by a larger reaction later in the curve. The
automatic determination will use the first reaction in the OIT, which gives the
wrong interpretation.
Figure A-1
Thermogram showing multiple plots from unaged to highly aged insulation
A-3
Material Applicability
XLPE, PE, and EPR have been characterized using the test. It has been found to
be less useful for butyl rubber, SBR, and PVC.
Test Nature
A DSC is needed.
Relative Cost
Test Considerations
1. The test is indicative of the condition of the cable material at the site of the
sample. Condition of the remainder of the cable must be determined by
additional testing along the length or by inference from knowledge of
conditions affecting the cables run.
2. Test results might be affected by manufacturing variations in the cable
materials (that is, amount and uniformity of antioxidants in the material).
Although initial OIT values might be 1 hour or more, OITs between 1 hour
and 10 minutes might provide very limited useful information. Physical cable
properties often change only near the point at which the antioxidant has been
consumed. Therefore, OITs of 10 minutes or less are more important with
respect to correlation of OIT with actual physical condition.
Training is required for personnel removing samples and operating the DSC. A
standard procedure is available [4]. References 1 and 4 provide a description of
sample preparation techniques. Skill is required to interpret the results.
A-4
Maturity of Technique
References
1. Reduction of Oxidation Induction Time Testing to Practice as a Life Assessment
Technique for Cable Insulation. EPRI, Palo Alto, CA: 1996. TR-106370.
2. Improved Conventional Testing of Power Plant Cables. EPRI, Palo Alto, CA:
1996. TR-105581.
3. A. B. Reynolds, T. E. Doyle, and L. R. Mason, Oxidation Induction Time
(OIT) Technology for Electric Cable Condition Monitoring and Life
Assessment, Pacific-Sierra Research Corporation. U.S. Department of
Energy Report DOE/ER/82249-2. 1999.
4. Test Method for Oxidative Induction Time of Polyolefins by Differential Scanning
Calorimetry. ASTM-D3895. 2007.
A-5
C-02 Oxidation Induction/Onset Temperature Testing
Uses
Test Description
This test is similar in concept to OIT (see section C-01) in that it evaluates the
antioxidants remaining in the cable polymer.
In this test, the specimens are heated at a constant rate of 10C/min under a
pressurized oxygen atmosphere. The oxidation induction temperature is the
temperature at which exothermic reaction begins.
Acceptance Criteria
Reference 1 provides samples of such curves for styrene butadiene rubber (SBR)
and butyl rubber.
Material Applicability
SBR and butyl rubber have been characterized with respect to pressurized
(2 MPa) oxidation induction temperature in Reference 1. The test appears to be
useful for primarily these rubber materials for which standard techniques using
atmospheric pressure provided no distinct exotherm.
A-6
Cable Application Limitations
Test Nature
A DSC is needed. If SBR or butyl rubber is to be tested, the DSC will require a
pressurized DSC cell test.
Relative Cost
Test Considerations
1. The test is indicative of the condition of the cable material at the site of the
sample. The condition of the remainder of the cable must be determined by
additional testing along the length or by inference from knowledge of
conditions affecting the cable run.
2. Test results might be affected by manufacturing variations (that is, amount
and uniformity of antioxidants in material).
Maturity of Technique
Reference
1. Improved Conventional Testing of Power Plant Cables. EPRI, Palo Alto, CA:
1996. TR-105581.
A-7
C-03 Gel Content (Solubility) and Swelling Ratio
Measurements
Uses
Test Description
The gel content (solubility) test measures the relative amount of material that can
be dissolved in a test solvent. The swollen weight of the sample after immersion
in a test solvent divided by the final sample weight after driving off the solvent
gives solvent uptake factor. For certain polymers, trends in gel content and
solvent uptake factor correspond to mechanical property changes with aging (for
example, elongation-at-break properties).
Use of these tests requires an understanding of the nature of the material and the
chemical process involved with aging degradation. For a highly cross-linked
polymer, the gel content will be very high. For butyl rubber that is initially highly
cross-linked, there is a long induction period followed by a relatively rapid
decrease in gel content. For PVC insulation that is uncross-linked, the gel
content is initially low. After a long aging induction period, the gel content
increases relatively rapidly. For NEO and CSPE jackets, the degree of cross-
linking further increases with aging and reflects in the solvent uptake factors.
Initially, uptake factors corresponded to two to three times and with aging
reduced to approximately a factor of 1. This change can be correlated with the
elongation properties.
Figure A-2 shows a series of swell/gel tests being performed in parallel. The
solvent is condensed in the coils above the heated solvent and returned to the vial
to preclude loss of solvent and the material under test.
A-8
Figure A-2
Swell/gel tests with condensing coils
An acceptable solvent for PVC is tetrahydrofuran. For XLPE, PE, CSPE, and
NEO, it is xylene, and for EPR, butyl rubber, and SBR, it is toluene.
Acceptance Criteria
There are no absolute acceptance criteria for these tests. Characterizations with
respect to thermal aging of PVC, butyl rubber, XLPE, EPR, and SBR are
provided in Reference 1. These characterizations include correlations with
change in elongation characteristics for the materials. Care must be used in
interpreting these results because the responses of various materials differ with
respect to aging. First, the existence of gel content (insolubility) for PVC or a gel
content less than 80% for butyl rubber is an indication that additional
confirmatory tests are required. Second, for common CSPE and NEO jackets,
the uptake factor reduces from 2 to 3 to about 1.6 as the elongation values
reaches 50% absolute.
Material Applicability
These tests might be useful in evaluating PVC and butyl rubber, CSPE and
NEO [1,3]. For PE, EPR, SBR, and XLPE, detectable differences only occur at
the point near embrittlement.
A-9
Cable Application Limitations
There are no cable application limitations beyond those listed for material
applicability.
Test Nature
Relative Cost
Test Considerations
The test is indicative of the condition of the cable material at the site of the
sample. The condition of the remainder of the cable must be determined by
additional testing along the length or by inference from knowledge of conditions
affecting the cable run.
Maturity of Technique
References
1. Improved Conventional Testing of Power Plant Cables. EPRI, Palo Alto, CA:
1996. TR-105581.
2. Determination of Gel Content and Swell Ratio of Cross-Linked Ethylene Plastics.
ASTM D2765-84. 1984.
3. Initial Acceptance Criteria Concepts and Data for Assessing Longevity of Low-
Voltage Cable Insulations and Jackets. EPRI, Palo Alto, CA: 2005.
TR-100211.
A-10
C-04 Plasticizer Content Measurement
Uses
Test Description
For PVC, the plasticizer content can be correlated with retention of elongation
properties when the material is subjected to thermal aging.
The test is performed by heating the material in a solvent and determining the
loss in weight caused by extraction of the remaining plasticizers. For unaged
materials, plasticizer contents of 20 to 30% by weight are typical, and a weight
of less than approximately 15% is indicative of thermal degradation.
Acceptance Criteria
Material Applicability
Test Nature
A-11
Relative Cost
Test Considerations
1. The test is indicative of the condition of the cable material at the site of the
sample. The condition of the remainder of the cable must be determined by
additional testing along the length or by inference from knowledge of
conditions affecting the cable run.
2. Testing of unaged or mildly aged specimens is desirable to provide a basis for
evaluating the degree of aging, due to loss of plasticizer, in more severely
aged specimens.
Maturity of Technique
Reference
1. Improved Conventional Testing of Power Plant Cables. EPRI, Palo Alto, CA:
1996. TR-105581.
A-12
C-05 Fourier Transform Infrared Spectroscopy
Uses
Test Description
Applicability
Acceptance Criteria
There are no absolute acceptance criteria for this test technique. This test
requires the establishment of baseline values. Some work in relating those values
to actual elongation or embrittlement results has been completed.
Experimental data indicate that aged and oxidized polyolefins exhibit a carbonyl
peak at 1730 cm1 or an increase in the peak intensity. The presence of elevated
absorbance in the carbonyl region corresponds to a significant loss of antioxidant
in the material. For many polyolefin insulating materials, the change in the
carbonyl peak might be detected in advance of embrittlement. Reference 1
provides data showing the increase in the carbonyl peak with increased aging for
a filled XLPE and SBR, an unfilled XLPE, an EPR, and PE insulation.
A-13
Material Applicability
1. The technique detects the carbonyl formation in XLPE and HDPE before a
sharp decrease in elongation. This technique is less successful for EPR, SBR,
and PVC in which carbonyl formation is coincident with the decrease in
elongation.
2. Infrared spectroscopy can be used to identify the type of polymer used in
organic cable insulation.
There are no cable type limitations beyond those listed for materials.
Test Nature
Relative Cost
Test Considerations
1. When a sample is removed from the cable, the results will characterize the
cable at the sample location only. Multiple samples from one cable or an
initial evaluation to determine the worst-case location of the cable run might
be required.
2. The test detects chemical variations in the polymer regardless of the cause
(that is, formulation, contamination, and manufacturing variations).
3. The spectrometer is suited for laboratory tests only.
A-14
Maturity of Technique
Reference
1. Improved Conventional Testing of Power Plant Cables. EPRI, Palo Alto, CA:
1996. TR-105581.
A-15
C-06 NIR Spectroscopy
Uses
NIR spectroscopy is a nondestructive test that may be used in situ to identify the
cable material and the degree of aging. It is only applicable to insulations that do
not contain carbon black. The test analyzes broad-band light absorbed from the
surface of cable insulation to determine its absorption characteristics in the NIR
range. By comparing NIR scans of the material in question with the library of
characterized insulations, the material type and degree of degradation can be
determined.
Test Description
A broad spectrum light from an NIR source is directed to the surface of the cable
jacket or insulation onto a spectrophotometer via a fiber-optic cable. The
spectrophotometer creates a plot of wavelength and intensity of the light. As with
FTIR spectroscopy, strong NIR absorbers include species such as C-H, O-H, N-
H, C-O, C-H, COOH, and aromatic C-H groups. Some of these functional
groups (namely, C-O, O-H, and COOH) are formed as cable polymer
components age. The concentration of these functional groups increases with
aging. In the case of PVC, the evaporative loss of plasticizers by volatilization will
result in a decrease in some of these functional groups. Each material produces
different absorption spectra as it degrades. For PVC, FR-XLPE, and FR-EPR
insulation, chemical changes as a result of oxidation due to thermal, radiation,
and combined thermal and radiation aging can be spectroscopically quantified
and correlated with changes in mechanical elongation-at-break. Laboratory-aged
specimens are used to create a spectra library of different manufacturers
polymers with varying degradation, and these are used for comparison with in-
plant results.
A-16
Figure A-3
The NIR spectroscopic equipment as used in the field
Acceptance Criteria
There are no absolute acceptance criteria. The comparison of a test result with
the library of existing aged specimens can be used to identify both the material
compound and the mechanical property changes of the material. Being able to
identify the cable compound and hence the manufacturer is particularly useful for
early vintage PVC cables because these were frequently unmarked.
Material Applicability
The test may only be applied to cable insulation and jacket surfaces that will
transmit NIR light. Cable compounds containing carbon black cannot be
assessed because they absorb light in the NIR range.
Test Nature
A-17
Relative Cost
Test Considerations
The test may be performed in situ, but only on cables that are not dark colored.
The best colors for aging assessment are white, red, and orange, whereas
brownish-, blue-, or gray-colored wires limit the analysis of the data. The test is
indicative of the condition of the cable material at the site of the sample. The
condition of the remainder of the cable must be determined by additional testing
along the cable length or by inference from knowledge of conditions affecting the
cable run.
Maturity of Technique
The technique is mature and has been used extensively in situ for cable material
identification.
References
1. K. Anandakumaran, Condition Monitoring of Low Voltage Cables. Paper
presented at the EPRI EQ Technical Meeting, Tucson, AZ (November
2008).
2. K. Anandakumaran, Condition Assessment of Installed Nuclear Power
Plant (I&C) Cables. Annual Conference Proceedings of the Canadian
Nuclear Society (CNS), Montreal, Quebec, Canada (May 24, 2010).
A-18
C-07 Thermogravimetric Analysis
Uses
The test heats a small specimen of polymer at a constant temperature ramp rate
while monitoring weight under controlled environmental conditions. As organic
materials evolve and oxidize, a characteristic plot of weight change curve is
obtained. The residual from the test is an indication of inorganic filler in the
material. For cable insulations and jackets, the residual material after heating
includes clay fillers, metallic fire retardants, and lead (lead oxide is a stabilizer in
medium-voltage EPR insulation). Comparison of the test sample
thermogravimetric analysis (TGA) data with the known cable insulation and
jacket may allow the determination of the polymer type or show similarity
between formulations.
This test is useful for evaluating PVC insulation or jacket subjected to radiation
or combined radiation and thermal environment. The temperature at which 5%
weight (TGA 5% temperature) loss occurs has been correlated with loss of
elongation. Under radiation or combined radiation and thermal environment,
breakdown of polymer chains occurs, and the TGA 5% temperature decreases
with aging. With only thermal aging, plasticizer loss is the predominant aging
mechanism and plasticizer content (see section C-04) measurement is a more
suitable technique to assess aging.
Test Description
The test consists of heating a small sample (~10 mg) of polymeric material at a
constant rate of 10C/min under a nitrogen atmosphere while monitoring the
change in weight. This produces a TGA plot of the temperature at which 5%
weight loss occurs. As the polymer chain is broken due to aging, the 5% weight
loss temperature decreases.
A-19
Acceptance Criteria
Material Applicability
The test is most useful for PVC insulation or jacket that has been subjected to
radiation or combined radiation and thermal aging.
Test Nature
Relative Cost
Test Considerations
The test is indicative of the condition of the cable material at the site of the
sample. The condition of the remainder of the cable must be determined by
additional testing along the length or by inference from knowledge of conditions
affecting the cable run.
A-20
Maturity of Technique
A-21
E-01 Insulation Resistance dc Test
Uses
Test Description
For low-voltage cable in dry applications, high insulation resistances are not a
direct indication that no problems exist. Cracked insulation may have high
insulation resistance because dry air is a good insulator. Accordingly, insulation
resistance does not always provide an indication of damage and will not
necessarily provide a useful trend related to gradual deterioration. However, the
technique is useful for detecting and eliminating damage that results in leakage
paths across the insulation from conditions such as cuts coupled with high
humidity or chemical contaminations. The test evaluates the bulk resistance of
the insulation and includes all materials between the two terminals of the test
device, including jackets, insulation, and air gaps. If a section of the conductor is
exposed, the success in detecting the problem will be a function of the orientation
of the exposed conductor and the length of the tracking/insulation path to the
measurements ground plane.
The bulk resistance of the insulation system might be measured from conductor
to conductor, from conductor to all other conductors, from conductor to ground
or shield, or from conductor to all other conductors grounded. The test may be
performed at any voltage from 50 to 2500 Vdc, with 50 and 500 Vdc being
common values. Most tests of control cable are performed at 500 V, which is
considered to provide sufficient electrical stress to identify significant flaws
but which is not overly stressful. The leakage current from the test is converted
to ohms.
A-22
The test is useful for detecting gross imperfections, deterioration, and damage
that result in significantly lower insulation resistance values (multiple decades
of change).
Insulation resistances for good cable are often greater than many thousands of
megohms-1000 ft. Depending on the nature of a cable damage site and its
cleanliness, the insulation resistance might remain high or might decrease to a
megohm-1000 ft or less. If the conductors are separated by dry air, the insulation
resistance will be high and a problem might not be detectable. If the conductors
are joined by moisture or a conducting film or are shorted together, the insulation
resistance will be low and the problem detectable.
Acceptance Criteria
A-23
Evaluating the trend in measurements taken over a period of time may provide
insights regarding the condition of the cable and the environment of the cable.
However, insulation resistance testing alone will not necessarily provide a direct
indication of the state of the cable insulation. Testing of severely degraded
insulation located in dry air might produce very high insulation resistance values.
Material Applicability
Insulation resistance testing should be applied to coaxial and triaxial cables with
caution because significant capacitive charges can be accumulated during the test.
These charges might adversely affect the instruments used on these circuits if the
charge is not fully drained before the circuit is returned to service.
For other cable types, the voltages used in insulation tests do not impose a
significant stress on the insulation system. Therefore, the test might not detect
even gross damage unless the damage site is in contact with the return path for
the test or has a conducting contaminant such as moisture available to complete
the return path for the leakage current.
Test Nature
A megohmmeter is needed.
Relative Cost
Test Considerations
1. The cable generally must be disconnected.
2. Trending of results will be affected by the bulk temperature of the cable.
Measurements performed on the same cable at 32 and 86F (0 and 30C)
might vary by an order of magnitude or more. Making measurements under
similar ambient environment conditions will reduce variability of trending.
A-24
3. Differences in physical arrangement of cables within trays and conduits
might cause even similar circuits to have different insulation resistance values.
However, if the purpose of the test is to identify gross changes in insulation
resistance values, these differences in initial values might not matter.
4. Insulation resistance tests will not detect gradual radiation and thermally
induced aging. However, gross physical damage or deterioration under wet
conditions should be detectable.
Evaluation of the results requires an understanding of the cable type and its
application and physical layout for the results to be most useful. As a go/no-go
measurement, less experience is necessary.
Maturity of Technique
Reference
1. Plant Support Engineering: Aging Management Program Development Guidance
for AC and DC Low-Voltage Power Cable Systems for Nuclear Power Plants.
EPRI, Palo Alto, CA: 2010. 1020804.
IEEE Guide for Field Testing Power Apparatus Insulation. IEEE Standard 62-
1978. New York, NY: Institute of Electrical and Electronic Engineers.
A-25
E-02 Polarization Index Test
Uses
Test Description
PI testing measures the insulation resistance at one minute and 10 minutes after
the dc potential is applied to the cable. The ratio of the 10-minute resistance to
the one-minute resistance is the PI. The insulation resistance between the cable
conductor and the shield or exterior of the insulation is measured with a
megohmmeter, which applies a dc voltage (typically 500 Vdc) and translates the
leakage current into ohms. This test detects gross insulation imperfections,
damage, and/or deterioration in cables. This test is frequently used on large
motors, but can be used on cables as well.
A similar test is the polarization ratio test. It measures the insulation resistance at
two points in time as specified by the test method after the dc potential is applied
to the cable. The ratio of the second resistance to the first resistance is the
polarization ratio.
For most low-voltage cables, the PI will be 1 because the absorption and
charging currents decay well within one minute. Long cables and cables with
shields might have ratios >1. Values <1 indicate leakage current is increasing
during the duration of the test, which is unacceptable.
A-26
Modem test equipment is available that records the insulation resistance from
initial application of the test voltage through completion, allowing absorption
and charging currents to be observed and allowing the most appropriate
insulation resistance values to be used in the polarization ratio calculation.
Acceptance Criteria
PIs and polarization ratios must have values of at least 1 for low-voltage cables.
Polarization ratios <1 are indicative of leakage currents that are increasing with
the duration of the test, which is unacceptable. Long, well-shielded circuits
might result in indices and ratios >1. For circuits with PIs that are initially >1,
reductions in value in subsequent measurements might indicate advanced
degradation, even if the subsequent PIs are >1.
Material Applicability
For other cable types, the voltages used in insulation tests do not impose a
significant stress on the insulation system. Therefore, the test might not detect
even gross damage unless the damage site is in contact with the return path for
the test or has a conducting contaminant such as moisture available to complete
the return path for the leakage current.
Test Nature
A megohmmeter is needed.
Relative Cost
Test Considerations
1. The cable will have to be disconnected to allow tests to be performed.
2. Polarization tests will not detect gradual radiation and thermally induced
aging. However, gross physical damage or wetting of a significant length of
cable should be detectable.
A-27
Training and Experience Requirements
Maturity of Technique
A-28
E-03 Time Domain Reflectometry Test
Uses
Test Description
Acceptance Criteria
TDR results are evaluated on the basis of comparison with a baseline result or
through detection of impedance changes that are not expected in the circuit
being evaluated. The test is most effective in detecting relatively gross conductor
damage or near short circuits. The test can also detect wet sections of cables.
Material Applicability
The test can be applied to most cable geometries. The cable must be shielded or
have multiple conductors for the test to be effective. Higher quality results can be
expected from shielded and coaxial/triaxial constructions.
Test Nature
A-29
Test Equipment Necessary
Relative Cost
Test Considerations
1. The test might require isolation of connected equipment from the tested
cable to eliminate interference of the signal from the equipment and to allow
connection of the test equipment.
2. Splice points between segments and segments having different insulation
systems will be detected (for example, if a circuit has two segments, one with
an EPR insulation, and one with XLPE insulation, the differences in
insulation characteristics might be detected). Therefore, a knowledge of the
cable circuit is required to allow interpretation of results.
3. The test might not detect small defects up to and including through-
insulation cuts and cracks if the damage site does not affect impedance
significantly (for example, clean, dry through cuts and cracks might not be
detected).
Maturity of Technique
A-30
E-04 Line Impedance Resonance Analysis
Uses
LIRA is useful for detecting damage to and aging of cable insulation. The test
uses conductors in a cable to modulate a white noise signal or frequency sweep
that is analyzed for impedance resonances that are related to the distance to the
far termination, geometric differences along the length that affect capacitance,
and aging of the insulation either along the entire length or at specific locations.
LIRA provides a relative degree of damage and the location along the length of
the cable.
Test Description
Figure A-4
LIRA system block diagram [2]
A-31
Figure A-5
LIRA plot for a 98.43-ft (30-m) cable showing a thermal damage signal at 73.82 ft
(22.5 m) [3]
Acceptance Criteria
No generic acceptance criteria exist. Some data are being generated by specific
users that relate DNORM to specific degrees of aging on specific manufacturers
insulation systems. DNORM is a value generated by the LIRA software that is
derived from the degradation signal in comparison with a stable termination
signal. Use of DNORM instead of the amplitude of the degradation signal alone
allows comparison of different tests of the same or related cables.
Material Applicability
The test is applicable to any insulation material between two adjacent conductors
with continuous spacing or between a conductor and a concentric shield.
A-32
Test Nature
The test is nondestructive. Most tests are performed with the cable de-energized
and at least one lead lifted at one termination. The opposite end of the cable may
be open or shorted without adversely affecting the test. The only problem would
be if the impedance of the load at the opposite end closely matched that of the
cable, which should be rare. The test places a low-energy, high-frequency white
noise on the cable at approximately 3 V, which would not adversely affect any
power plant cable.
Relative Cost
A LIRA test set is expensive. Individual tests are inexpensive and take a few
minutes at most to administer.
Test Considerations
Maturity of Technique
The technology is a relatively young and in-plant use has been limited to
European plants for the most part.
A-33
References
1. Plant Support Engineering: Line Impedance Resonance Analysis for Detection of
Cable Damage and Degradation. EPRI, Palo Alto, CA: 2007. 1015209.
2. P. Fantoni and J. I. Juvik, Condition Monitoring of Electrical Cables Using
Line Resonance Analysis (LIRA). Paper B.7.3 presented at the JiCable11
8th International Conference on Insulated Power Cables, Versailles, France
(June 1923, 2011).
3. G. Toman and P. Fantoni, Cable Aging Assessment and Condition
Monitoring Using Line Resonance Analysis (LIRA), ICONE16-48523.
Proceedings of the 16th International Conference on Nuclear Engineering.
ICONE16, Orlando, FL (May 11-15, 2008).
A-34
E-05 Dielectric Spectroscopy
Uses
In this test, the current passing through the insulation in response to a step
change in voltage is analyzed by transforming the acquired current data into a
function of frequency to arrive at dielectric impedance as a function of frequency.
The variation in dielectric impedance is primarily due to bulk cable capacitance
and conductance.
The real and imaginary parts of the permittivity, the change in the real
permittivity, and the tan are evaluated with respect to voltage and frequency
change. At each applied voltage, a frequency sweep is performed, and the
permittivity and tan parameters are evaluated.
Naturally, the desired response from a cable is low-loss, linear permittivity. For
XLPE, the test should provide an early indication of the onset of water treeing by
comparison with VLF and line frequency tan through the voltage-dependent
permittivity assessment.
A-35
Acceptance Criteria
Material Applicability
The test is most useful for medium-voltage cable that has been subjected to long-
term wetting and applies to EPR as well as XLPE insulation
The test may be applied to all EPR and XLPE cables having an insulation shield,
whether helical metal tape, concentric neutral, or UniShield type.
Test Nature
Relative Cost
Test Considerations
1. Cables must be de-energized and disconnected from the associated load.
2. Up to twice line-to-ground voltage is applied during the test.
Maturity of Technique
A-36
Reference
1. P. Werelius, P. Tharning, R. Eriksson, B. Homgren, and U. Gafvert,
Dielectric Spectroscopy for Diagnosis of Water Tree Deterioration in
XLPE Cables, IEEE Transactions on Dielectrics and Electrical Insulation. Vol.
8, No. 1 (2001).
A-37
E-06 Dissipation Factor (Tan )
Uses
Test Description
A prescribed high voltage is applied to the cable system being tested, and the
current through the sample is measured. The principle of operation is based on
the fact that when a steady-state ac test voltage is applied across a cables
insulation (i.e., conductor to shield); the resulting apparent total current that
flows consists of a charging current due to the capacitance of the cable insulation
and a leakage current. For the ideal lossless dielectric, the phase angle between
current and voltage is 90. However, the contribution of the leakage current due
to either inherent losses in the dielectric or defects, results in a loss angle,
(Figure A-6). Measurement of the loss angle through either a bridge technique
or digital methods enables the DF to be recorded. Tan is IC/IR.
Figure A-6
Loss angle,
A-38
Typically, DF testing is conducted at two or more voltages so that the tip-up or
tan may be derived. The tip-up or tan is the difference in tan between
one measured at higher voltage and one measured at a lower voltage. Historically,
DF measurements, recorded at multiple incremental voltages, were used on fluid-
filled cables to identify the ionization potential, or PD inception voltage, of the
cable being tested. The usefulness of the DF data increases significantly if tests
are performed at two or more voltages.
Acceptance Criteria
Acceptance levels exist for 60-Hz DF measurements for factory testing of new
cable insulation [1]. At present, there are no industry-recognized acceptance
criteria for testing of installed cable systems using power frequency voltage
sources.
Material Applicability
A-39
Cable Application Limitations
This test method may be used on all cables that have a contiguous metallic shield.
DF testing cannot be used on unshielded cables.
Test Nature
The test can be performed in the plant. Essentially, the test is nondestructive;
however, this statement needs to be qualified because it is dependent on the
applied voltage. The IEEE and EPRI documents require that the cable is tested
above nominal line-to-ground operating voltage, and thus there is a finite risk of
failure during the test if the cable is in a highly degraded condition.
Relative Cost
Test Considerations
A-40
5. If possible, the presence of splices or joints in the circuit should be noted
because the condition of these accessories and the possibility of interruption
of the cable shield at the splice or joint may significantly affect the test
results.
6. Cable terminations should be inspected and cleaned if surface contamination
is evident. Cleaning of the termination surfaces may be performed regardless
of the presence of contamination. Further, the type of terminations should
also be considered because the presence of nonlinear stress grading materials
in a termination may significantly affect the test results.
Although guidelines exist [3] for the interpretation of VLF DF data, caution
should be exercised, especially in the event of an anomalous result, given the factors
described. If anomalous results occur in circuits containing underground splices,
the splices should be inspected for signs of installation errors, degradation, or
damage. For circuits having butyl or black EPR rubber insulation, high tan
values, high tan , and/or increased standard deviations may be indicative of
distributed water-related degradation if the cable is >30 years old.
A-41
Maturity of Technique
References
1. Standard for Utility Shielded Power Cables Rated 5 through 46 kV.
ANSI/ICEA S-97-682.
2. Guide for Field Testing of Shielded Power Cable Systems Using Very Low
Frequency (VLF). IEEE Standard 400.2. 2007.
3. Plant Support Engineering: Aging Management Program for Medium-Voltage
Cable Systems for Nuclear Power Plants. EPRI, Palo Alto, CA: 2010. 1020805.
A-42
E-07 Partial Discharge (Off-line)
Uses
Test Description
A prescribed high voltage is applied to the cable system being tested, and the
response of an appropriate PD signal coupling device, connected to the test
object, is monitored/recorded using an appropriate instrument. PD signals
may be coupled from the system being tested using a range of devices including
the following:
1. High-voltage coupling capacitors connected directly to the cable conductor.
2. Radiofrequency current transformers or Rogowski coils applied at the cable
shield ground connections.
3. Sheath interruption couplers installed at cable joints or splices.
4. Inductive-capacitive couplers installed around the cable jacket external to the
cable shield.
Typically, for nuclear plant cable applications, only couplers of the first two types
described are used.
A-43
Acceptance Criteria
Material Applicability
This test method may be used on all cables that have a contiguous metallic
shield. However, the effectiveness of the test is dependent on the cable
insulation and semiconducting materials, the length of the cable being tested,
and the PD detection method used. These points are discussed further in the
Test Consideration section. Partial discharge testing cannot be used on
unshielded cables.
Test Nature
The test can be performed in the plant. Essentially, the test is nondestructive;
however, this statement needs to be qualified because it is dependent on the
applied voltage.
Relative Cost
A-44
Test Considerations
A-45
Complexity of Results Interpretation
Maturity of Technique
Reference
1. Standard for Partial Discharge Test Procedure. Insulated Cable Engineers
Association, Inc. Carrollton, Georgia. ANSI/ICEA T-24-380-2007.
IEEE Guide for Partial Discharge Testing of Shielded Power Cable Systems in a Field
Environment. IEEE Standard 400.3-2006. New York, NY: Institute of Electrical
and Electronic Engineers.
A-46
E-08 Continuity (Loop) Resistance Test
Uses
This test measures the conductor resistance of an installed cable to identify open
conductors, significant conductor damage, and splice and termination problems.
The procedure may also be used to balance the resistance of cables in a phase
having multiple conductors per phase. The test can be used as a preservice or
troubleshooting test.
Test Description
Acceptance Criteria
Expected resistance for a given circuit could be calculated for comparison with
actual circuit values. Comparisons among tests might be more useful in
determining the gradual change in conductor circuit condition. For high-current
circuits, small changes in loop resistance may be indicative of a significant
problem such as a poor connection. The high-resistance connection would be
subject to increased ohmic heating that could lead to insulation failure at the
deteriorated connection. Lower current circuits might not be as sensitive to
changes in loop resistance. Higher loop resistance, however, could result in a
significant voltage drop in the cable that could affect operation of the
connected device.
Material Applicability
The test could be used on nearly any type of cable. For heavy power cables, in
which conductor resistances may be low, a high-current test set might be most
useful for resistance measurement.
Test Nature
A-47
Test Equipment Necessary
Relative Cost
Test Considerations
The test might require that leads be disconnected at both ends of the circuit.
Maturity of Technique
Power Plant Electrical Reference Series, Volume 4, Wire and Cable. EPRI, Palo Alto,
CA: 1988. EL-5036.
A-48
E-09 Differential Insulation Resistance
Uses
Test Description
Acceptance Criteria
There are no acceptance criteria. The test is used to identify locations in the
insulation where deterioration has occurred to allow further assessment to be
performed in that area.
Material Applicability
The test has been successfully used on butyl rubber and EPR insulations. It may
be useful on XLPE and PVC as well.
The test is a forensics laboratory test and may be used on any insulation having
its conductor in place and its insulation outer surface accessible.
Test Nature
The nature of the test is forensic. The cable has been removed from service and is
in the process of being deconstructed.
Insulation resistance meter and a metallic probe (alternately, a wet cotton swab
may be used) are needed.
A-49
Relative Cost
Test Considerations
Maturity of Technique
A-50
M-01 Hardness Test
Uses
Test Description
Acceptance Criteria
Material Applicability
Durometry is useful for evaluating radiation and thermal aging of natural rubber,
NEO, CSPE (Hypalon), EPR, and butyl rubber, thermal aging of PVC, and
radiation aging of silicone rubber. Changes in the hardness of XLPE will be
masked by its crystallinity, making monitoring of aging through durometry
impractical.
A-51
The test is less useful for continuously energized, high-energy power cables in
which significant ohmic heating of the conductor could cause subsurface aging of
the organic materials that might not detectable at the surface.
Test Nature
A durometer is required.
Relative Cost
Test Considerations
The results will characterize the cable material at the sample location only.
Multiple measurements along and around the surface of the cable might be
necessary to characterize the condition of the overall cable. If measurements from
unaged cable insulation or jacket materials are not available, measurements made
at locations not subject to significant thermal and radiation stresses might
provide a reasonable baseline value for comparison with more highly stressed
locations. Durometers will run out of useful range before loss of functional
usefulness for some jacket and insulation materials. In such cases, the Indenter
modulus continues to be sensitive to changes in hardness (see M-003 Indenter
Modulus Testing section).
A-52
Maturity of Technique
Standard Test Method for Rubber Property - Durometer Hardness. ASTM D224-
05. 2010.
A-53
M-02 Tensile Strength and Elongation-at-Break Test
Uses
Tensile tests may be used to assess aging by evaluating tensile strength and/or
elongation-at-break. For most common cable insulation and jacket materials,
elongation-at-break is the most common laboratory test of remaining mechanical
properties. Retention of elongation properties allows the cable jacket and
insulation to be bent and respond to thermal transients without cracking.
Bending a cable causes the material on the outside of the bend to be stretched.
With severe loss of elongation properties, cracking could result when the material
is bent.
Because standard tests must be performed on specimens of 3.93 to 5.9 in. (100 to
150 mm) in length with the conductors removed, the tensile tests must be
performed on segments of cable removed from service. The test is, therefore,
destructive in nature. For small conductor cable, tube samples of the insulation
are tested with the conductor removed. For large-diameter cables, dumbbell
samples can be cut for tensile testing. A special method is used in the program
described in References 1 and 2. In this program, strips approximately 0.08 in.
wide 0.02 in. (2 mm wide 0.5 mm) thick and 2.36 in. (60 mm) long were
tested, greatly increasing the number of test specimens per length of cable.
However, even with this reduction in test specimen size, the test remains
destructive in nature.
Test Description
This test measures the ultimate elongation and strength of an insulation or jacket
material under tensile stress. The test is performed by stretching a dumbbell or
tube sample of insulation or jacket in a test stand with jaws that are separated at a
constant velocity while force is measured. The length of a segment of the sample
is measured before the start of the test. The increase in that length of the
segment of the specimen just before breaking is then determined. The results
are either expressed in the percentage of the original length (absolute elongation)
or in relative terms by giving the ratio or percentage between the result for
specimens subjected to different amounts of accumulated stress to the
elongation of an unaged specimen (relative elongation). For the purposes of
evaluating the retained properties of a cable jacket or insulation, absolute
elongation is more useful.
A-54
Because of its destructive nature, elongation-at-break has not been a readily
usable aging assessment technique for plant cables unless cables that can be
sacrificed are available for removal and testing, which is relatively rare in the
power industry. Where representative cables have been installed specifically for
periodic testing or a representative cable can be removed from service for testing,
elongation-at-break is a well-established, mature technique for evaluating
degradation of cable materials.
Acceptance Criteria
There are no generic acceptance criteria established for all cable polymers. At
minimum, a cable insulation system must be able to withstand the maximum
bending strain at the outer bend surface without cracking. Reference 3 provides a
basis for a retained elongation-at-break of at least 50% as satisfactory for
continued service for in-containment applications. Cables that pass loss-of-
coolant accidents consistently do so with absolute elongations of <20%. With
respect to being able to manipulate cable during maintenance without damage,
the strain for a bend radius of one cable diameter results in an outer surface strain
of 33%. Such a bend radius is much more severe than the recommended
manufacturer's minimum bend radii, which are generally greater than four cable
diameters. A cable material capable of 50% elongation-at-break definitely can
withstand a tight radius bend that would result in a strain at the outer surface
of 33%.
A-55
Material Applicability
Test Nature
The test is destructive and most useful for characterizing cables removed from
service due to failure or because the cable is no longer needed. Relatively large
samples are necessary. Multiple tests of 5.9- to 3.93-in. (100- to 150-mm)
specimens are needed.
Relative Cost
The cost of the test apparatus is significant; the cost of individual tests is
moderate.
Test Considerations
A-56
Complexity of Results Interpretation
Maturity of Technique
References
1. Natural Versus Artificial Aging of Nuclear Power Plant Components. EPRI,
Palo, Alto, CA: 1992. TR-l00245.
2. Natural Versus Artificial Aging of Electrical Components. EPRI, Palo, Alto,
CA: 1997. TR-106845.
3. Initial Acceptance Criteria Concepts and Data for Assessing Longevity of Low-
Voltage Cable Insulations and Jackets. EPRI, Palo, Alto, CA: 2005. 1008211.
A-57
M-03 Indenter Modulus Testing
Uses
Indenter modulus testing is used to assess aging of cable jackets and insulation. A
small anvil is pressed against the wall of the cable while measuring force and
position. At a specific force, the anvil is retracted to prevent damage to the cable.
The slope of the force versus position curve is sensitive to the degree of
embrittlement from thermal and radiation aging for many cable polymers.
Test Description
This test measures the Indenter modulus of a polymer by pressing a small anvil at
constant velocity against the outer surface of a cable or insulated conductor while
measuring the force exerted by the anvil. The Indenter modulus is defined as the
slope of the force versus position curve. The measurement is made through use of
the Indenter polymer aging monitor (Indenter). The results of the test are related
to changes in hardness of the material being tested. Significant increases in the
Indenter modulus occur in many polymers as they age from thermal and
radiation stressors. The Indenter modulus is inversely proportional to elongation-
at-break for most cable polymers.
The Indenter has controls that retract the anvil when a force limit is reached that
prevents damage to the cable material during the test. Additional automatic
controls are provided to prevent overtravel of the anvil should the force limit not
cause retraction.
The nature of the Indenter measurement method allows the Indenter to evaluate
a large spectrum of differences in hardness from very soft materials to those that
are extremely embrittled, giving the device a much broader range than a
durometer (see section M-00l Hardness Test).
Acceptance Criteria
Acceptance criteria for several common cable types have been developed based on
the replication of nuclear environmental qualification accelerated aging [1].
These acceptance criteria are preliminary in nature.
A-58
Material Applicability
Indenter moduli measurements are indicative of the relative aging of NEO and
for thermal and radiation stresses, of silicone rubber for radiation aging, and of
PVC for thermal aging. For certain XLPE and EPR formulations, Indenter
moduli might not change significantly until very near the end of thermal and
radiation life. For these formulations, indenter measurements on XLPE or EPR
will not be useful for evaluating aging because detection of the aging of the
material might occur too late.
Many of the cable types in use other than silicone rubberinsulated cables use
NEO or Hypalon jackets that are amenable to Indenter modulus testing. These
jackets can be used to evaluate the effects of thermal and radiation environments
on the cable, and their condition can be used as a leading indicator of insulation
aging because these jacket materials age more readily than the underlying XLPE
or EPR insulations.
The Indenter can be applied to cables up to 1.57 in. (40 mm) in diameter with
the normal clamp. Larger diameter cables are testable by removing the moving
portion of the clamp and holding the device against the cable surface.
For continuously energized cables with currents near the rated ampacity,
inferences concerning aging of the insulation by using jacket measurements
should be carefully considered, especially if the ambient temperature is low
compared with the conductor temperature (for example, 185194F [8590C]
conductor in a 104F [40C] ambient). In such a case, jacket aging might not age
as fast as insulation aging. Tests performed on the surface of the insulation at a
termination might provide additional insights. Indenter data have not been
developed for specimens that have been aged through ohmic heating of the
conductor.
Where baseline data are not available for the cable being tested, testing of a cable
segment that is located in room temperature environments and not subjected to
high-current loadings will give a reasonable basis for comparison with more
highly stressed cable segments. Indenter measurement on unaged and aged
Hypalon specimens have differences of a factor of 3, making identification of
significant embrittlement relatively easy.
Test Nature
The test is nondestructive and can be performed in situ. Test limits can be
adjusted to ensure that damage is not done to more sensitive materials.
A-59
Test Equipment Necessary
Relative Cost
The Indenter test device is relatively expensive; the cost of individual tests is low.
Test Considerations
The basic test method is easy to learn. Limited training is required to set up the
Indenter for use on specific polymers.
Maturity of Technique
The test method has been used in a number of domestic and foreign power
plants, and implementation practices continue to be developed.
Reference
1. Initial Acceptance Criteria Concepts and Data for Assessing Longevity of Low-
Voltage Cable Insulations and Jackets. EPRI, Palo Alto, CA: 2005. 1008211.
A-60
For Further Information
A-61
M-04 Density Testing
Uses
For most cable polymers, density increases with aging. Standard laboratory
density testing methods require only small samples.
Test Description
As oxidative reactions occur in cable polymers from aging under thermal and
radiation stresses, the density of the materials generally increases. These changes
from the unaged state to the fully aged state are relatively small and generally on
the order of a few percent. However, high-precision density measurements are
possible. Therefore, the trend in the change in density can be used to evaluate
polymer aging. In general, increases in density correlate to a loss of tensile
properties and an increase in hardness of polymers.
The most mature test method is the laboratory method in which a very small
specimen (micrograms to milligrams) is evaluated through use of density gradient
columns. Gradient columns contain salt solutions that have decreasing densities
from bottom to top. A small sample is dropped into the column, and the point at
which it achieves neutral buoyancy provides its density.
Acceptance Criteria
Although there are no specific acceptance criteria for density, correlations with
elongation-at-break are possible. References 1 through 3 provide density results
for insulation and jackets of common cable types from the EPRI/University of
Connecticut Natural Versus Artificial Aging of Nuclear Power Plant
Components program and Sandia National Laboratories studies. These
references also provide elongation data for the same specimens. In the Sandia
study, for a number of thermally aged CSPE jackets, density change
corresponded to progressive decreases in elongation. Reference 4 provides
density data related to accelerated thermal aging for XLPE, butyl rubber, EPR,
and PVC.
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Knowledge of the unaged density value is desirable to be able to determine the
relative change in the property with aging. A density variation measurement from
batch to batch of polymers is possible and would require compensation.
Material Applicability
Provided small specimens can be removed from a cable, there is little limitation
with respect to application to various cable types. The test might be useful in
evaluating cables that have failed in service or that have been removed from
service for other reasons. Results from such evaluations might provide insights
regarding cables that remain in service.
Test Nature
Relative Cost
Test Considerations
The results will characterize the cable at the sample location only. Multiple
samples from one cable or an initial evaluation to determine the worst-case
location of the cable run might be required to make inferences concerning the
remainder of the cable.
A sample must be obtained, which may be the most difficult activity. To perform
the test, only limited training is required. The laboratory procedure can be
standardized.
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Maturity of Technique
Density measurement techniques are mature. Data for use in evaluating results
are becoming increasingly available.
References
1. Natural Versus Artificial Aging of Nuclear Power Plant Components.
Interim Report. EPRI, Palo Alto, CA: 1992. TR-100245.
2. Natural Versus Artificial Aging of Electrical Components. Interim Report 1991-
1995. EPRI, Palo Alto, CA: 1997. TR-106845.
3. Nuclear Energy Plant Optimization (NEPO) Final Report on Aging and
Condition Monitoring of Low-Voltage Cable Materials, SAND 2005-7331.
2005.
4. Improved Conventional Testing of Power Plant Cables. EPRI, Palo Alto,
CA: 1995. TR-105581.
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M0-5 Acoustic Velocity Testing
Uses
Acoustic velocity testing was developed to assess the aging of cable jackets and
insulations nondestructively. As density changes occur in polymers with aging,
the propagation time for sonic waves change.
Test Description
As of this writing, further development work has ceased in favor of other more
readily available test methods.
Acceptance Criteria
Material Applicability
Initial work indicates that the propagation of the sound pulse is independent of
cable configuration.
Test Nature
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Relative Cost
Test Considerations
1. This is a local test that characterizes the cable at the test location only.
Multiple samples along the length of the cable might be necessary to develop
an overall characterization.
2. The test method is currently suitable for laboratory use only. No commercial
device available as yet.
Maturity of Technique
A system was developed by MHI Japan. However, MHI no longer provides in-
plant service using the system.
Reference
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M-06 Thermal Fingerprinting
Uses
Test Description
This test evaluates the shape of the melting curve for cable polymers having
crystalline or semicrystalline structures.
Polymers tend to exhibit melting ranges rather than single melting points,
unlike metals and pure organic compounds of low molecular weight. The melting
range depends on the linearity of the polymer chain, among other variables. This
means that polymers such as cross-linked polyethylene have a much broader
melting range than high-density polyethylene. In the case of XLPE, it extends
from 0C to 106C. The existence of this broad melting range means that
temperatures reached during manufacture of cables from these materials, or use
temperatures due to storage and service conditions leave a fingerprint on the
melting range.
To perform the test, a small sample of the material is placed in a DSC and
heated at l0C/min to a temperature of 150C to obtain the melting curve (heat
flow [mW] versus temperature (C). Changes in heat flow are proportional to the
number of crystals melting at a particular temperature.
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At the end of this exposure, the material is cooled at 104F (40C)/min to 4F
(20C) to quench crystallize the material. This cooling redistributes the crystals
evenly along the melting curve and removes the "recorded thermal history." The
specimen is then reheated at 50F (10C)/min to determine the melting curve of
a quenched specimen. The quenched curve is subtracted from the initial melting
curve to obtain a subtraction curve. The derivative of the subtraction curve is
taken to determine the temperatures to which the material had been exposed
subsequent to manufacture.
Acceptance Criteria
The purpose of the test is to determine the temperature exposure of the cable
polymers; thus, the concept of acceptance criteria does not apply.
Material Applicability
The technique has been successfully performed on XLPE, EPR, and ethylene
propylene diene monomer. The materials under evaluation must have a
crystalline or semicrystalline nature. The technique is not useful for fully
amorphous materials such as CSPE (e.g., Hypalon).
Test Nature
A DSC is required.
Relative Cost
Test Considerations
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Complexity of Results Interpretation
Maturity of Technique
Practicality has been demonstrated. There has been limited commercial usage to
date. The technique is based on mature DSC technology.
Reference
1. Fingerprinting the Thermal History of Polymeric Materials. EPRI, Palo Alto,
CA: 1992. TR-101205.
Improved Conventional Testing of Power Plant Cables. EPRI, Palo Alto, CA:
1996.
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M-07 Nuclear Magnetic Resonance in Solution
Uses
Nuclear magnetic resonance (NMR) testing with the polymer in solution is a test
that allows assessment of the aging of materials that are partially crystalline such
as XLPE. The crystals in the material mask changes in hardness from oxidation
and cross-linking. Melting the crystals and putting the material in solution allows
changes in oxidation and cross-linking to be identified through analysis of the T2
time, the NMR relaxation time.
Test Description
The NMR relaxation time, T2, is related to the mobility of polymer chains.
Because an increase in cross-link density reduces chain mobility, cross-linking
results in decreases in T2, but these decreases are often fairly small and show little
difference between unaged and highly aged specimens, especially when masked
by the crystalline nature of some polymers and fillers such as clay in rubber
compounds. However, when polymers are swollen in a deuterated solvent, the
increased mobility caused by the expanded network tends to significantly increase
T2 values for unaged specimens. Because the solvent is deuterated, swelling also
decreases the density of hydrogen atoms and causes an additional increase in T2.
(The contribution to relaxation from deuterated atoms is significantly less than
that from hydrogen atoms.) With aging, cross-linking leads to a reduction in
solvent uptake and an increase in the concentration of protons so that the T2
values are substantially reduced. When T2 measurements are taken on samples
swelled in a good solvent, the swelling and hydrogen density factors lead to a
significant amplification effect so that the T2 sensitivity to differing levels of
cross-linking (aging) is much greater, and the needed resolution between unaged
and aged specimens is obtained. This method has been successfully used for
NEO, CSPE, EPR, and XLPE [1].
Acceptance Criteria
Material Applicability
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Test Nature
The method requires 8- to 10-mg of material for each test. The solvent is
material specific. Deuterated chloroform (CDCl3) is used for CSPE and NEO.
Benzene-d6 is recommended for XLPE. Cyclohexane-d12 may be used for CPE.
The pretreatments before performing the test vary by polymer [1].
The test is performed using a NMR spectrometer with the capability of heating
the solution during the test.
Relative Cost
The value of T2 indicates the degree of aging. Once the correlation between T2
and elongation-at-break has been established, interpretation is not difficult.
Maturity of Technique
The test method is in the developmental stage and has not been widely used.
Reference
1. Cable Polymer Aging and Condition Monitoring Research at Sandia National
Laboratories Under the Nuclear Energy Plant Optimization (NEPO) Program.
EPRI, Palo Alto, CA: 2005. 1011873.
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M-08 Micro Modulus
Uses
A very small probe is pressed against the surface of a polymer, two steps of load
are applied, the probe displacement is measured at each load, and a modulus is
calculated from the difference in force and difference in displacement. Because
the probe is so small, the modulus of the transverse section can be evaluated
through the depth of a piece of insulation, and the uniformity of degradation
from the outer wall of the insulation to the inner wall can be evaluated.
Test Description
Acceptance Criteria
There are no set acceptance criteria for the micro modulus test. The test is most
useful for determining whether the rate accelerated aging exceeds the point where
oxygen diffusion is too slow to allow uniform aging through the depth of the
material.
Material Applicability
Test Nature
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Test Equipment Necessary
Relative Cost
Test Considerations
Once the specimen has been prepared and mounted in the test rig, the test is
computer controlled, and a modulus profile across the surface of the material is
generated automatically.
The test is a specialty test only available through two laboratories. Personnel
experienced with the preparation of samples and the operation of the test rig are
required.
Maturity of Technique
Reference
1. Cable Polymer Aging and Condition Monitoring Research at Sandia National
Laboratories Under the Nuclear Energy Plant Optimization (NEPO) Program.
EPRI, Palo Alto, CA: 2005. 1011873.
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V-01 Visual Examination
Uses
Visual examination might be used as a screening tool for aging assessment and
can be used as a preliminary evaluation technique in troubleshooting and failure
evaluation. For many cable and termination types, visible signs of degradation are
detectable when significant aging has occurred. Observation of such conditions
generally indicates that further investigation of aging cables subject to similar
service conditions is desirable.
Test Description
Visual examination of cables and terminations can provide insights on
degradation from ambient environments and conditions of the application.
Although degrees of gradual aging are generally not discernable, significant
deterioration in the form of color changes, changes in surface texture, crazing (a
covering of fine surface cracks), cracking, loss of flexibility, surface tackiness, and
hardening are detectable. Observation of such conditions indicates that further
evaluation or corrective action is necessary. Absence of such indications in areas
having more severe normal thermal and/or radiation environments provides a
general indication that low-voltage cable has not experienced severe aging.
Acceptance Criteria
Note: This system of evaluation is for verifying that gross deterioration has not
occurred. If the absence of gross deterioration can be affirmed even in severe
condition applications, inferences concerning the overall adequacy of the low-
voltage cable system are possible. However, to more fully understand the degree
of aging of cables, other condition monitoring techniques capable of determining
lesser degrees of degradation should be considered.
A-74
Material Applicability
Although most cable types have observable characteristics that are indicative of
accumulation of a significant amount of time at elevated stress levels, visual
examination will only be practicable in areas where the cable is available for viewing.
Test Nature
No equipment is necessary.
Relative Cost
Test Considerations
1. Although limited portions of the cable and insulated conductors will be
available for examination, conditions at the terminations of the cable, where
loads and instruments are connected, often are the most severe with regard to
the overall length of the cable. The absence of adverse observations can be
used to infer the overall condition of the cable.
2. If maintenance and test personnel are trained in visual detection of adverse
conditions, feedback concerning cable deterioration might be obtained at
relatively low cost.
3. The application of the technique might be based on management by
exception; that is, only adverse findings are reported. Attention to cables
located in severe normal thermal and radiation environments will provide the
earliest indication of degradation.
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Complexity of Results Interpretation
Maturity of Technique
A-76
V-02 Microscopic Examination
Uses
Test Description
For certain types of cable failures, microscopic examination of the failure site
might provide an indication of the cause. The use of this technique requires that
the location of the fault be known. The faulted area is examined visually with the
aid of a microscope to determine the nature of the faulted area. When electrical
faults occur, the breakdown generally destroys the cause of the fault. Therefore,
examination of the insulation material in the vicinity immediately adjacent to the
fault must be used. Thin layers of material can be microtomed for identification
of inclusions, voids, and other physical defects or damages.
Acceptance Criteria
Material Applicability
The technique is more useful for materials that are not fully opaque because
reflectance and light transmission are important in microscopic examination. The
technique might be of limited use for materials that are carbon black filled.
Test Nature
Relative Cost
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Test Considerations
The test is useful to characterize the vicinity of damage or an electrical fault site.
Maturity of Technique
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