Manual 915 Isotech
Manual 915 Isotech
Manual 915 Isotech
The company is always willing to give technical advice and assistance where appropriate.
Equally, because of the programme of continual development and improvement we reserve the
right to amend or alter characteristics and design without prior notice. This publication is for
information only.
Page 1 of 26
CONTENTS
PAGE NO:
Guarantee
CE Information
4-5
On Arrival
Electricity Supply
Important Note
Figure 1
10
11 -15
Choice of Liquids
16
Changing Liquids
17
Chillers
18
Trouble Shooting
19
20
21 - 22
23
Accessories
24
APPENDIX 1
Using the Isotech High Stability Temperature Controller
25 -26
A-H
Page 2 of 26
GUARANTEE
This instrument has been manufactured to exacting standards and is guaranteed for twelve
months against electrical break-down or mechanical failure caused through defective
material or workmanship, provided the failure is not the result of misuse. In the event of
failure covered by this guarantee, the instrument must be returned, carriage paid, to the
supplier for examination, and will be replaced or repaired at our option.
FRAGILE CERAMIC AND/OR GLASS PARTS ARE NOT COVERED BY THIS
GUARANTEE.
INTERFERENCE WITH, OR FAILURE TO PROPERLY MAINTAIN THIS INSTRUMENT
MAY INVALIDATE THIS GUARANTEE.
RECOMMENDATION
The life of your ISOTECH Instrument will be prolonged if regular maintenance and cleaning
to remove general dust and debris is carried out.
Serial No:.....................................
Date:.............................................
Page 3 of 26
EMC INFORMATION
This product meets the requirements of the European Directive on Electromagnetic
Compatibility (EMC) 89/336/EEC as amended by EC Directive 92/31/EEC and the European
Low Voltage Directive 73/25/EEC, amended by 93/68/EEC. To ensure emission compliance
please ensure that any serial communications connecting leads are fully screened.
The product meets the susceptibility requirements of EN 50082-1, criterion B.
Symbol Identification
Publication
Description
ISO3864
Caution
(Refer to Handbook)
IEC 417
ELECTRICAL SAFETY
This equipment must be correctly earthed.
This equipment is a Class 1 Appliance. A protective earth is used to ensure the conductive
parts can not become live in the event of a failure of the insulation.
The protective conductor of the flexible mains cable which is coloured green/yellow MUST be
connected to a suitable earth.
The blue conductor should be connected to Neutral and the Brown conductor to Live (Line).
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ENVIRONMENTAL RATINGS
Operating Temperature
5-50/C
Relative Humidity
Page 5 of 26
2.
Operators of this equipment should be adequately trained in the handling of hot and
cold items and liquids.
3.
Do not use the apparatus for jobs other than those for which it was designed, ie. the
calibration of thermometers.
4.
Do not handle the apparatus when it is hot (or cold), unless wearing the appropriate
protective clothing and having the necessary training.
5.
6.
Do not dismantle the apparatus without disconnecting it from the supply and leaving
time for it to reach ambient temperatures.
7.
8.
The apparatus is protected by an over temperature circuit, ensure correct settings at all
times.
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ON ARRIVAL
Check List.
You should have the following parts,
1.
2.
3.
4.
Optional accessories are available and will only be present if specified on your order, see page
24.
In the unlikely event of any items arriving damaged please retain the packing materials (which
may need to be inspected later) and then contact your supplier.
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ELECTRICITY SUPPLY
Before connecting to the electricity supply please familiarise yourself with the parts of the
handbook relevant to your model.
Your unit's supply voltage requirement is specified on a plate on the instrument along with the
Serial number.
The apparatus is provided with an approved power cord. If the plug is not suitable for your
location then the plug should be removed and replaced with an appropriate plug.
Take care to ensure that the old plug is disposed of safely.
The cable is colour coded as follows:
COLOUR
FUNCTION
Green/yellow
Brown
Blue
Earth (Ground)
Live (line)
Neutral
Please ensure that your unit is correctly connected to the electricity supply.
THE APPARATUS MUST BE CORRECTLY EARTHED (GROUNDED)
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Connect the drain pipe to the drain tap and the overflow pipe to the side overflow pipe. Place
a suitable container under the overflow pipe. Ensure the tap is shut, i.e. lever at 90 to the tap
body. If the equalising block is to be used it should be placed in position now.
Fill the bath with a suitable liquid, water is probably best for initial testing. Fill the bath until the
level is 10mm below the top of the round central calibration tube
ALWAYS ISOLATE THE BATH FROM THE SUPPLY WHEN CHANGING LIQUIDS
Turn the flow control to the mid position.
FRONT PANEL CONTROLS (See figure 1.)
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FIGURE 1
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A.
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The bath can have its heating rate limited with the Setpoint Ramp Rate feature. This feature is
accessed from the Scroll key. Depress the key until the display shows,
SPrr
On the Upper Display, the lower display will show the current value from OFF (default) to 999.9.
The desired rate is set here with the UP and DOWN keys, the units are /C/min.
When the SPrr is active the controller display will show "RUN", the lower setpoint display will
now automatically update with the current value, known as the working setpoint. The setpoint
can be seen by pressing either the UP and DOWN key.
The Setpoint ramp rate operates when the bath is heating and cooling.
Instrument Address
The controller has a configurable "address" which is used for PC communications. Each
instrument has an address, this allows several instruments to be connected in parallel on the
same communications bus. The default value is 1. This address would only need to be changed
if more than one bath is connected to the same PC port.
To check the Address value press the scroll key until the top display indicates,
Addr
The lower display will show the current value that can be modified with the UP and DOWN keys.
Monitoring the Controller Status
A row of beacons indicate the controllers status as follows,
OP1
REM
Heat Output
This beacon indicates activity on the PC interface
Units
Momentary pressing the Scroll key will show the controller units /C or /F.
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Diagnostic alarms
These indicate that a fault exists in either the controller or the sensor.
Controller Error Messages
The instruments include powerful diagnostics and in the unlikely event of an internal failure, or
a sensor error, one of the following error messages may be displayed.
Display
shows
What it means
What to do about it
EE.Er
Contact Isotech
S.br
Sensor Break:
Input sensor is unreliable or the input
signal is out of range.
Contact Isotech
HW.Er
Hardware error :
Indication that a module is of the wrong
type, missing or faulty
Contact Isotech
LLLL
Contact Isotech
HHHH
Contact Isotech
Err1
Consult Isotech
Err2
Consult Isotech
Err3
Consult Isotech
Err4
Err5
Consult Isotech
Pwr.F
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B.
This device is an important safety feature. It has its own temperature sensor and will isolate the
heater if the temperature exceeds the set temperature. It should be set slightly higher, perhaps
10 - 20C higher than the working temperature or to the maximum safe temperature of the fluid
in use. Which ever is the lowest value. IT MUST BE SET IN THIS WAY TO ENSURE SAFE
USE OF THE BATH. Suitably set it will allow for protection against component failure and also
operator error when setting the controller, either from the front panel or remotely from a
computer.
The over temperature controller is used in conjunction with the Set / Reset Button.
C.
When the bath is first switched on the heater is disabled. When this button is pressed the
heater will become enabled and the light next to the button will become illuminated. If the bath
temperature exceeds the value set in the over temperature controller the heater will no longer
be enabled and the light will turn off.
D.
As mentioned above the light will be lit when the heater is enabled and will be off when the
heater is disabled.
E.
FLOW CONTROL
This controls the flow rate of the liquid. It allows for a wide range of liquid viscosities and
provides easy adjustment. It should initially be set to the mid position and then adjusted whilst
the flow is observed.
The optimum position for a particular liquid at a specific temperature may need to be
determined experimentally. As a general guide the flow should be increased until it becomes
turbulent and then backed off slightly. Generally the stability will be optimum when the flow is
high but stable.
F.
ON / OFF SWITCH
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2.
Set the set point of the temperature controller to the desired value (50.0C).
3.
4.
5.
Press the Set / Reset Button. The bath should now reach and control at the target set
point.
The bath may now be used for calibration, see tutorial.
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CHOICE OF LIQUIDS
The choice of liquid is important. If it is too viscous at the operating temperature then the bath
may not perform correctly. Other criteria also need to be meet, such as safety, operating range
and fume emission for example. Isotech is able to supply a number of fluids for various
temperature ranges, see catalogue.
Unfortunately, there is not one fluid which can be used over the whole operating range of the
bath. Beware of oils that are claimed to work from below ambient to over 100C. Whilst we do
not supply or recommend such liquids. others do. It is our experience that such oils absorb
moisture from the air when used below the dew point. Then at temperatures around 100C this
moisture boils and can lead to the oil spilling from the top of the bath. Even without the boiling
risk the oil is soon spoilt by the ingressions of moisture and the oil has to be replaced regularly,
which can be an expensive task. It will be seen that when changing fluids from say water to oil
that it is important that ALL the water has been removed before adding the oil.
As oils approach their upper operating limit fumes become significant and fume extraction
becomes essential. It is for this reason that the upper limit of the bath is 300C. Isothermal
Technology manufactures a fluidised alumina bath, the Ayries Bath which overcomes the
limitations of oils and may be used to 700C without fuming problems.
Below ambient we use a mixture of methanol and water. Methanol is poisonous and has a low
flash point. It needs to be used very carefully by those suitably trained and aware of the
dangers if handled inappropriately. As local safety requirements vary not only from country to
country but also from organisation to organisation the safety aspects of these fluids should be
determined with the users safety officer.
LIQUID LEVEL
All liquids expand as they are heated and contract when they cool.
The bath has been designed to allow for varying liquid volumes and also features an overflow
system which prevents the liquid from spilling from the top of the bath.
The optimum liquid level with the motor off at the operating temperature is for the liquid to be
level with the top of the calibration tube.
When working below ambient it can be useful to pre chill and store in a thermos flask a quantity
of the operating fluid. This prevents large thermal shocks when the bath is "topped" up and
helps reduce cooling time.
Page 16 of 26
CHANGING LIQUIDS
If possible it is best to plan so that liquids do not need to be frequently changed. This may be
achieved by liquid choice, determining convenient calibration points or having more than one
bath - each with a different liquid to cover the routine calibration range.
To change the liquid,
1.
2.
Ensure the liquid is at a safe handling temperature. Neither too hot nor too cool then
open the drain tap.
3.
Drain the liquid into a clean containers of adequate capacity, properly labelled for future
use.
4.
Clean the bath. Detergent and absorbent paper will assist. If the bath has been used
with an oil it can be helpful to re fill with water and detergent and to allow the mixture to
circulate before draining again.
5.
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Page 18 of 26
TROUBLE SHOOTING
PROBLEM
SOLUTION
No Power
Check Fuse
Bath Overflows
N.B.
If the oil suddenly expands and overflows at 100/C it may have been contaminated with
water and the oil should be replaced after this has been cleaned.
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Note: The RS 422 standard specifies a maximum lead length of 1200M (4000ft). A true RS422
port will be required to realise such lead lengths. The Isotech conversion leads are suitable for
maximum combined lead lengths of 10M that is adequate for most applications.
Connections
For RS232 use simply connect the Isotech cable, a 9 to 25 pin converter is included to suit PCs
with a 25 pin serial converter.
RS422 Connections
Pin
4
5
8
9
1
Connection
Tx+ A
Tx- B
Rx+ A
Rx- B
Common
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CAL NOTEPAD
Cal Notepad can be used to log and display values from the bath and an optional temperature
indicator.
Minimum System Requirements
CNP requires Windows 95 / 98, a minimum of 5Mb of free hard drive space and free serial ports
for the instruments to be connected.
Development
CNP was developed by Isothermal Technology using LabVIEW from National Instruments.
License
Use of the Cal NotePad software program "CNP" is as granted in this license agreement. In using the
CNP
software the user "licensee" is agreeing to the terms of the license. You must read and understand the
terms of this license before using CNP.
1, This license permits licensee to use CNP software on a single computer. The user may make copies
for back up and archival purposes freely as long as the software is only ever in use on a single computer
at any one time. Please enquire about multi-user licenses.
2, CNP is protected by international copyright laws and treaties. CNP must not be distributed to third
parties.
3, CNP must not be reversed engineered, disassembled or de-compiled. Licensee may transfer the
software to a third party provided that no copies or upgrades of CNP are retained.
4, It is the responsibility of the user to ensure the validity of all stored results and printed certificates.
Isothermal Technology Ltd accept no responsibility for any errors caused by inappropriate use, incorrect
set up or any other cause; including defects in the software.
5, Limited Warranty. Isothermal Technology warrants that CNP will perform substantially as described in
this manual for a period of 90 days from receipt. Any distribution media will under normal used be
guaranteed for a period of 90 days.
NO OTHER WARRANTIES, EXCEPT AS STATED ABOVE. The software and documentation is provided
"as is" without warranty of any kind and no other warranties (either expressed or implied) are made with
regard to CNP. Isothermal Technology does not warrant, guarantee or make any representations
regarding the use or results of the use of the software or documentation and does not warrant that the
operation of CNP will be error free.
In no event will Isothermal Technology, its employees, agents or other associated people be liable for
direct, indirect, incidental or consequential damages, expenses, lost profits, business interruption, lost
business information or other damages arising out the use or inability to use CNP. The license fee reflects
this allocation of risk.
CNP is not designed for situations where the results can threaten or cause injury to humans.
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Protocol
The instruments use the "Eurotherm EI BiSynch Protocol"
If required, e.g. for writing custom software the technical details are available from our website
at, www.isotech.co.uk/refer.html
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Page 23 of 26
ACCESSORIES
The following options are available:915/01a
915/01b
915/02
915/03
915/05
915/07
915/08
915/09
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APPENDIX 1
USING THE ISOTECH HIGH STABILITY TEMPERATURE CONTROLLER
i, Isotech High Stability Controller
OPERATING INSTRUCTIONS
The ISOTECH HIGH STABILITY CONTROLLER has been designed to provide superior
stability with ease of use.
CHANGING SET POINT
The set point is modified utilising the three front panel keys.
To modify the set point first press "ALTER" once, the top left digit will flash which indicates that
the digit may be modified by pressing the "SET" key. The digit will step with each press of the
"SET" key. The first digit may be -, 0, 1 or 2 whilst the following digits may be in the range 0 9 which allows an
entry range of -99.99 to 299.99C.
When the required value has been set or to move to the next digit then press the "ENTER" key.
After the fifth digit has been set then pressing "ENTER" will now cause all five digits to flash
showing the new set point or target temperature. To accept this new value press "ENTER"
again the display will now stop flashing. It is only when the display has stopped flashing that the
new set point is activated.
Or if you are unhappy with the new set point value instead of pressing "ENTER" as the display
flashes press "ALTER" which allows the set point to be changed again.
In use there may be a small offset (less than 1C) between the set point and the measured
value this is quite normal. The measured value is to a large extent a measurement system
independent of the control loop. If you are aiming for a particular temperature, for example 50C
and with a set point of 50.00 the actual temperature is found to be 50.06 then the set point may
be offset by 0.06, 49.94 in this case. Remember this is a comparison calibration bath.
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C123.45
C-00.15
C300.45
C-0.15
C100.0
Out of range
A zero is "missing"
A zero is "missing"
RS 232 Connections.
The standard 9 pin D connector is wired as follows,
Pin 2
Pin 3
Pin 5
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